公开(公告)号：KR100676892B1

公开(公告)日：2007-02-02

申请号：KR1020050101238

申请日：2005-10-26

Applicant: 강릉원주대학교산학협력단

Inventor： 경영수 ,  최종섭

IPC: C07C331/20

Abstract: A method for preparing an allyl isothiocyanate is provided to improve the yield of the isothiocyanate, to allow the use of a cost-efficient starting material, and to simplify the processing steps. The method for preparing an allyl isothiocyanate comprises the steps of: mixing an allyl compound with a thiocyanate compound and agitating the resultant mixture to perform a reaction; and heating the reaction mixture after the reaction of the allyl compound with the thiocyanate compound. In a variant, the method for preparing an allyl isothiocyanate comprises the steps of: mixing an allyl compound with a thiocyanate compound and heating the resultant mixture; and agitating the heated mixture to perform a reaction.

Abstract translation: 提供了一种制备异硫氰酸烯丙酯的方法，以提高异硫氰酸酯的产率，允许使用具有成本效益的起始材料，并简化加工步骤。 制备异硫氰酸烯丙酯的方法包括以下步骤：将烯丙基化合物与硫氰酸酯化合物混合并搅拌所得混合物进行反应; 并在烯丙基化合物与硫氰酸盐化合物反应后加热反应混合物。 在一个变体中，用于制备异硫氰酸烯丙酯的方法包括以下步骤：将烯丙基化合物与硫氰酸酯化合物混合并加热所得混合物; 并搅拌加热的混合物以进行反应。