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    폴리헤드랄올리고머릭실세스퀴녹산 치환기를 갖는 전기전도성 고분자 및 그 제조방법
    3.
    发明公开
    폴리헤드랄올리고머릭실세스퀴녹산 치환기를 갖는 전기전도성 고분자 및 그 제조방법 失效
    具有溶解性和电介质特性的聚酯低聚硅烷氧基取代基的电导电聚合物及其制备方法

    公开(公告)号：KR1020040091383A

    公开(公告)日：2004-10-28

    申请号：KR1020030025202

    申请日：2003-04-21

    Applicant: 국방과학연구소

    Inventor： 이문호 ,  백성식 ,  김현철 ,  김근홍 ,  천창환 ,  안준모 ,  권순길

    IPC: C08G73/00

    Abstract: PURPOSE: An electrically conductive polymer having a polyhedral oligomeric silsesquinoxane substituent, its preparation method and a doped electrically conductive polymer material are provided, to obtain new electrically conductive polymer material having solubility and dielectric characteristics by substituting a polar polyhedral oligomeric silsesquinoxane group to the side chain of an electrically conductive polymer. CONSTITUTION: The electrically conductive polymer is represented by the formula 1, wherein 0

    Abstract translation: 目的：提供一种具有多面体低聚硅氧烷奎尼糖取代基的导电聚合物，其制备方法和掺杂的导电聚合物材料，通过将极性多面体低聚硅氧烷基锡烷代替侧链来获得具有溶解性和介电特性的新型导电聚合物材料 的导电聚合物。 构成：导电聚合物由式1表示，其中0 <= x <= 1，n是5-500,000的整数。 优选地，导电聚合物的特性粘度为0.1-3.0dL / g，重均分子量为1,000-10,000,000。 通过使用酸，盐或碘作为掺杂剂来掺杂导电聚合物材料。 导电聚合物是通过反应方案1在溶剂和催化剂的存在下制备的。 优选地，溶剂是酸或有机溶剂，并且催化剂是氧化剂。

    디아미노카바졸 유도체 화합물로부터 합성되는 폴리아조메틴 및 이들의 제조방법
    4.
    发明公开
    디아미노카바졸 유도체 화합물로부터 합성되는 폴리아조메틴 및 이들의 제조방법 失效
    二氨基硼氢化物衍生物，其获得的聚异氰酸酯及其制备方法在有机溶剂或混合有机溶剂中提供优异的溶解性，从而改善电极聚合物的可加工性

    公开(公告)号：KR1020040094468A

    公开(公告)日：2004-11-10

    申请号：KR1020030028256

    申请日：2003-05-02

    Applicant: 국방과학연구소

    Inventor： 이문호 ,  김현철 ,  백성식 ,  김근홍 ,  천창환 ,  안준모 ,  권순길

    IPC: C08G73/02

    Abstract: PURPOSE: Diaminocarbazole derivatives are provided to be advantageously used as intermediates in a polyazomethine preparation. Polyazomethines obtained by using the diaminocarbazole derivatives have excellent solubility in organic solvent or mixed organic solvent with water, thereby improving the processability and applications of the electroconductive polymer material obtained by doping the polyazomethine. CONSTITUTION: The diaminocarbazole derivatives are represented by a formula 1, wherein R is hydrogen, alkyl having C50 or less, hydroxyalkyl, alkylarylhydroxy, arylhydroxy, carboxyalkyl, alkylester, arylester and alkylarylester group. The diaminocarbazole derivatives are produced by: substituting the hydrogen of N-H bond in the carbazole ring with one selected from alkyl, hydroxyalkyl, alkylarylhydroxy, arylhydroxy, carboxyalkyl, alkylester, arylester and alkylarylester group in the presence of sodium hydride or potassium carbonate as a catalyst; dissolving the resulted N-substituted carbazole derivatives into a mixed solvent of acetic acid and anhydride thereof to introduce two nitro groups by using Cu(NO3)2·2.5H2O as a nitrating agent; dissolving the resulted product into ethyl alcohol and hydrochloric acid and adding SnCl2 thereto to reduce the nitro groups to imino groups. Polyazomethines are represented by a formula 2, wherein R is hydrogen, alkyl having C50 or less, hydroxyalkyl, alkylarylhydroxy, arylhydroxy, carboxyalkyl, alkylester, arylester and alkylarylester group; Z is N-R1 or CR2R3, wherein R1, R2 and R3, being independent from each other, are same as defined for R; and n is 2-500000.

    Abstract translation: 目的：提供二氨基咔唑衍生物有利地用作多偶氮甲碱制剂中的中间体。 通过使用二氨基咔唑衍生物获得的多偶氮甲碱在有机溶剂或混合有机溶剂中与水的溶解度优异，从而提高通过掺杂多氮唑啉获得的导电聚合物材料的加工性能和应用。 构成：二氨基咔唑衍生物由式1表示，其中R是氢，C 50或更少的烷基，羟基烷基，烷基芳基羟基，芳基羟基，羧基烷基，烷基酯，芳基酯和烷基芳基酯基团。 二氨基咔唑衍生物的制备方法是：在氢化钠或碳酸钾作催化剂存在下，用选自烷基，羟基烷基，烷基芳基羟基，芳基羟基，羧基烷基，烷基酯，芳基酯和烷基芳基酯基的咔唑环中的N-H键的氢取代; 将得到的N-取代的咔唑衍生物溶解在乙酸及其酸酐的混合溶剂中，通过使用Cu（NO 3）2·2.5H 2 O作为硝化剂引入两个硝基; 将所得产物溶解在乙醇和盐酸中并加入SnCl 2以将硝基还原为亚氨基。 多取代甲酰胺由式2表示，其中R是氢，C 50或更少的烷基，羟基烷基，烷基芳基羟基，芳基羟基，羧基烷基，烷基酯，芳基酯和烷基芳基酯基团; Z是N-R1或CR2R3，其中R1，R2和R3彼此独立地与R定义相同; n为2-500000。

    전기전도성 고분자, 자기특성 산화철 나노입자와전기전도성 고분자의 나노복합체 및 그 제조방법
    7.
    发明公开
    전기전도성 고분자, 자기특성 산화철 나노입자와전기전도성 고분자의 나노복합체 및 그 제조방법 有权
    电导电聚合物，具有两种磁性和电导率的聚合物和磁铁氧化物纳米颗粒的纳米复合物及其制备方法

    公开(公告)号：KR1020040097566A

    公开(公告)日：2004-11-18

    申请号：KR1020030029900

    申请日：2003-05-12

    Applicant: 국방과학연구소

    Inventor： 이문호 ,  전용주 ,  백성식 ,  김현철 ,  김근홍 ,  천창환 ,  안준모 ,  권순길

    IPC: C08G61/02 ,  B82B3/00

    Abstract: PURPOSE: Provided are an electrically conductive polymer, a nanocomposite of the polymer and an iron oxide nanoparticle which has both magnetic property and electrical conductivity and has an excellent processability owing to solubility and its preparation method. CONSTITUTION: The electrically conductive polymer is prepared by polymerizing a monomer X represented by the formula 1 or a monomer Y represented by the formula 2, has a weight average molecular weight of 1,000-10,000,000 and is soluble, wherein Z is an imine group or a vinyl group; Q is S, Se or N-R7; and R1, R2, R3, R4, R5, R6 and R7 are independently H, a hydroxyl group, a halogen atom, a halide, an alkyl group of C1-C50, an alkoxy group, an alkylcarboxyl group, an alkyl ester group, a hydroxyalkyl group, a nitroalkyl group, a cyanoalkyl group, a haloalkyl group, an oxyhaloalkyl group, a cyanohaloalkyl group, an aryl group, an oxyaryl group, a haloaryl group, a nitroaryl group, a cyanoaryl group, an oxyhaloalkylaryl group, a haloalkylaryl group, a nitrohaloalkylaryl group and a cyanohaloalkylaryl group.

    Abstract translation: 目的：提供一种导电聚合物，该聚合物的纳米复合材料和具有磁性和导电性以及由于溶解性而具有优异加工性的氧化铁纳米颗粒及其制备方法。 构成：导电性聚合物通过聚合由式1表示的单体X或由式2表示的单体Y制备，重均分子量为1,000-10,000,000，为可溶的，其中Z为亚胺基或 乙烯基; Q是S，Se或N-R7; R 1，R 2，R 3，R 4，R 5，R 6和R 7独立地为H，羟基，卤素原子，卤素，C 1 -C 50烷基，烷氧基，烷基羧基，烷基酯基， 羟基烷基，硝基烷基，氰基烷基，卤代烷基，氧卤代烷基，氰基卤代烷基，芳基，氧芳基，卤代芳基，硝基芳基，氰基芳基，氧卤代烷基芳基，卤代烷基芳基 基团，硝基卤代烷基芳基和氰基卤代烷基芳基。

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