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公开(公告)号：KR101377337B1
公开(公告)日：2014-03-26
申请号：KR1020110137542
申请日：2011-12-19
Applicant: 서울대학교산학협력단
Abstract: 본 발명은 은 나노 입자를 함유한 양이온성 고분자 나노 섬유 제조에 관한 것으로서, 폴리비닐알코올(polyvinyl alcohol)이 존재하는 수용액 상에 일정량의 은 이온을 전단력(shear force) 하에 녹인 후, 라디칼 개시제(radical initiator)를 도입하여 은 이온의 환원을 유도한 뒤, 양이온성 고분자 단량체를 주입하여 적정 온도와 시간에서 라디칼 매개 분산 중합(radical mediated dispersion polymerization)을 이용하여 은 나노 입자를 함유한 양이온성 고분자 나노 섬유를 제조하는 방법을 제공한다.
본 발명에 따르면, 간단하고 저렴한 공정을 이용하여 은 나노 입자를 함유한 양이온성 고분자 나노 섬유를 용이하게 제조할 수 있으며, 효과적으로 은 나노 입자를 고분자 나노 섬유 내에 포함하기 위하여 추가적인 개질 공정이나 개질제가 요구되지 않는다는 장점을 가진다. 또한 본 발명을 통해 제조될 수 있는 은 나노 입자를 함유한 양이온성 고분자 나노 섬유는 은 나노 입자의 선처리 공정이 필요없을 뿐 아니라, 은 이온을 사용함으로써 제조 과정이 단순하며, 양이온성 고분자 나노 섬유의 종류 및 두께에 제한 없이 제조가 가능하다. 더욱이, 본 발명에서 제조될 수 있는 은 나노 입자를 함유한 양이온성 고분자 나노 섬유는 양이온성 고분자 나노 섬유의 회수가 매우 용이하다는 장점을 갖는다. 그리고 만들어진 은 나노 입자를 함유한 양이온성 고분자 나노 섬유는 기존의 은 나노 입자를 함유한 고분자 나노 섬유보다 더욱 향상되고 지속적인 항균 효과를 나타낼 수 있다.-
公开(公告)号：KR101148411B1
公开(公告)日：2012-05-25
申请号：KR1020090131081
申请日：2009-12-24
Applicant: 서울대학교산학협력단
Abstract: PURPOSE: A manufacturing method of titanium oxide/polymer core/shell nanoparticle is provided to manufacture massively titanium oxide/polymer core/shell nanoparticle through a photopolymerization using only the ultraviolet ray without using additional initiator. CONSTITUTION: The manufacturing method of titanium oxide/polymer core/shell nanoparticle includes following steps.(a) The titanium oxide nanoparticle is dispersed into a solvent.(b) A monomer is injected into the solvent with 'the dispersed titanium oxide'. A physical adsorption of the monomer is induced in the surface of the titanium oxide nanoparticle.(c) The ultraviolet ray is added to the surface of the titanium oxide nanoparticle with the adsorbed monomer. In the surface, a production of electrons and radicals is induced. In the surface, the polymerization of the monomer radical is induced.(d) The titanium oxide/polymer core/shell nanoparticle is collected from the polymerized solution through a precipitation.
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公开(公告)号：KR1020130070298A
公开(公告)日：2013-06-27
申请号：KR1020110137542
申请日：2011-12-19
Applicant: 서울대학교산학협력단
CPC classification number: D01F1/103 , B82B3/00 , D01D5/38 , D01D5/40 , D01F6/14 , D02G3/449 , D06M11/42 , D10B2321/06 , D10B2401/13
Abstract: PURPOSE: A manufacturing method of cationic polymer nano fiber containing silver nano particles is provided to contain silver particles in cationic polymer nano fiber by manufacturing the silver nano particles and cationic polymer nano fiber at the same time with a process without a pre-process of silver nano particles or multiple additional stages. CONSTITUTION: A manufacturing method of cationic polymer nano fiber comprises the steps of: (i) melting silver ions by a strong magnetic mixing; (ii) inducting reduction of the silver ions by putting a radical initiator in the aqueous solution; (iii) polymerizing a monomer on the surface of the silver nano particles by introducing the monomer in the aqueous solution; and (iv) collecting cationic polymer nano fiber containing siver nano particles from the polymeric composition.
Abstract translation: 目的：提供含有银纳米颗粒的阳离子聚合物纳米纤维的制造方法，通过制备银纳米颗粒和阳离子聚合物纳米纤维，在不经过银处理的工艺的同时制备银阳离子聚合物纳米纤维中的银颗粒 纳米颗粒或多个附加阶段。 构成：阳离子聚合物纳米纤维的制造方法包括以下步骤：（i）通过强磁混合熔融银离子; （ii）通过将自由基引发剂引入水溶液中引入银离子的还原; （iii）通过将单体引入水溶液中，使银纳米颗粒的表面上的单体聚合; 和（iv）从聚合物组合物中收集含有纳米颗粒的纳米粒子的阳离子聚合物纳米纤维。
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公开(公告)号：KR1020110065595A
公开(公告)日：2011-06-16
申请号：KR1020090122156
申请日：2009-12-10
Applicant: 서울대학교산학협력단
Abstract: PURPOSE: A producing method of silica/polyrhodanine core-shell nanoparticle using the dispersion polymerization is provided to easily obtain polyrhodanine from the surface of a silica nanoparticle. CONSTITUTION: A producing method of silica/polyrhodanine core-shell nanoparticle comprises the following steps: dispersing silica into a solvent, and adding an initiator into the solvent for absorbing the initiator to the surface of the silica; drying silica nanoparticles absorbed with the initiator, and dispersing into another solvent; injecting a rhodanine monomer into the solvent containing the silica nanoparticles absorbed with the initiator for inducing the polymerization on the surface of the silica; and precipitating the solvent for collecting the silica/polyrhodanine core-shell nanoparticle.
Abstract translation: 目的：提供使用分散聚合的二氧化硅/多罗丹酸核壳纳米颗粒的制备方法，以容易地从二氧化硅纳米颗粒的表面获得聚四氢叶酸。 构成：二氧化硅/聚四氢呋喃核壳纳米颗粒的制备方法包括以下步骤：将二氧化硅分散在溶剂中，并将引发剂加入溶剂中以将引发剂吸收到二氧化硅的表面; 干燥二氧化硅纳米颗粒用引发剂吸收，并分散到另一种溶剂中; 将含有二氧化硅纳米粒子的引发剂注入到含二氧化硅纳米粒子的溶剂中，以诱导二氧化硅表面的聚合; 并沉淀出用于收集二氧化硅/聚四氢呋喃核 - 壳纳米颗粒的溶剂。
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Patent Agency Ranking
公开(公告)号：KR1020130070263A
公开(公告)日：2013-06-27
申请号：KR1020110137500
申请日：2011-12-19
Applicant: 서울대학교산학협력단
Abstract: PURPOSE: An one-pot fabrication method of silver nanoparticles embedded polypyrrole nanotubes is provided to obtain silver nanoparticles embedded polypyrrole nanotubes using silver ions as the oxidizer of chemical oxidation polymerization. CONSTITUTION: A fabrication method of polypyrrole nanotubes includes the following steps of: arranging an anodic aluminum oxide template in a silver cation and iron cation solution, and absorbing silver cations and iron cations on the anodic aluminum oxide template; polymerizing pyrrole monomer on the anodic oxide template by vapor deposition; reducing silver ions from the anodic aluminum oxide template, and generating silver nanoparticles; generating polypyrrole by the chemical oxidation polymerization of the pyrrole monomer; removing the anodic oxide aluminum template, washing the anodic oxide aluminum template with methanol, and collecting polypyrrole nanotubes containing silver nanoparticles.
Abstract translation: 目的：提供一种纳米银纳米粒子纳米管的一锅法制备方法，以银离子作为化学氧化聚合反应的氧化剂，得到银纳米粒子纳米聚酰胺纳米管。 构成：聚吡咯纳米管的制造方法包括以下步骤：在银阳离子和铁阳离子溶液中配置阳极氧化铝模板，并在阳极氧化铝模板上吸收银阳离子和铁阳离子; 通过气相沉积在阳极氧化物模板上聚合吡咯单体; 从阳极氧化铝模板中还原银离子，产生银纳米颗粒; 通过吡咯单体的化学氧化聚合生成聚吡咯; 去除阳极氧化铝模板，用甲醇洗涤阳极氧化铝模板，收集含有银纳米粒子的聚吡咯纳米管。
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6.发明公开
公开(公告)号：KR1020110012122A
公开(公告)日：2011-02-09
申请号：KR1020090069692
申请日：2009-07-29
Applicant: 숭실대학교산학협력단 , 서울대학교산학협력단
CPC classification number: G06Q30/0633 , G06F17/30244 , G06Q20/3276 , H04W4/00 , H04W88/02 , H04W88/08
Abstract: PURPOSE: A mobile communication terminal, a store management server, a shopping service system using a server smart card and a shopping service providing method are provided to enable a mobile communication terminal user to transmit desired information to a store management server, thereby purchasing the product. CONSTITUTION: An information input unit(201) receives an input of an image information about a product. An information transmitting unit(203) transmits the image information to a store management server. A list information receiving unit(205) receives shopping product list information corresponding to the image information from the store management server. A purchasing requesting unit(207) transmits a purchase request information about at least one among products in the shopping product list to a store management server.
Abstract translation: 目的：提供移动通信终端，商店管理服务器，使用服务器智能卡的购物服务系统和购物服务提供方法，以使移动通信终端用户能够将所需信息发送到商店管理服务器，从而购买产品 。 构成：信息输入单元（201）接收关于产品的图像信息的输入。 信息发送单元（203）将图像信息发送到商店管理服务器。 列表信息接收单元（205）从商店管理服务器接收与图像信息对应的购物产品列表信息。 购买请求单元（207）向商店管理服务器发送关于购物商品列表中的产品中的至少一个的购买请求信息。
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公开(公告)号：KR1020110074184A
公开(公告)日：2011-06-30
申请号：KR1020090131081
申请日：2009-12-24
Applicant: 서울대학교산학협력단
CPC classification number: C01G23/04 , B01J19/123 , B82Y30/00 , B82Y40/00 , C01P2004/64 , C08F2/48
Abstract: PURPOSE: A manufacturing method of titanium oxide/polymer core/shell nanoparticle is provided to manufacture massively titanium oxide/polymer core/shell nanoparticle through a photopolymerization using only the ultraviolet ray without using additional initiator. CONSTITUTION: The manufacturing method of titanium oxide/polymer core/shell nanoparticle includes following steps.(a) The titanium oxide nanoparticle is dispersed into a solvent.(b) A monomer is injected into the solvent with 'the dispersed titanium oxide'. A physical adsorption of the monomer is induced in the surface of the titanium oxide nanoparticle.(c) The ultraviolet ray is added to the surface of the titanium oxide nanoparticle with the adsorbed monomer. In the surface, a production of electrons and radicals is induced. In the surface, the polymerization of the monomer radical is induced.(d) The titanium oxide/polymer core/shell nanoparticle is collected from the polymerized solution through a precipitation.
Abstract translation: 目的：提供氧化钛/聚合物核/壳纳米颗粒的制造方法，通过仅使用紫外线的光聚合大规模制造氧化钛/聚合物核/壳纳米颗粒，而不使用额外的引发剂。 构成：氧化钛/聚合物核/壳纳米颗粒的制造方法包括以下步骤：（a）将二氧化钛纳米粒子分散在溶剂中;（b）将单体以“分散的氧化钛”注入溶剂中。 在氧化钛纳米颗粒的表面诱导单体的物理吸附;（c）用吸附的单体将紫外线加入氧化钛纳米颗粒的表面。 在表面上，产生电子和自由基。 在表面上，引发单体自由基的聚合。（d）通过沉淀从聚合溶液中收集氧化钛/聚合物核/壳纳米颗粒。
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公开(公告)号：KR1020110050264A
公开(公告)日：2011-05-13
申请号：KR1020090107170
申请日：2009-11-06
Applicant: 서울대학교산학협력단
CPC classification number: C01B33/12 , B82Y30/00 , B82Y40/00 , C01P2004/64 , C08F2/34
Abstract: PURPOSE: A method for preparing polycation nano particles using vapor deposition polymerization is provided to easily obtain polycation particles in nano sizes based on simple polymerization conditions. CONSTITUTION: The surface of silica nano particles is modified into hydrophobic. A radial initiator is added to the surface of modified silica nano particles is decompressed. A cation monomer is added to the silicon nano particles in which the initiator is added. The monomer is vaporized by increasing temperature. The polymerization of the monomer on the surface of the silicon nano particles is induced. Polycation nano particles are collected.
Abstract translation: 目的：提供使用气相沉积聚合法制备聚阳离子纳米颗粒的方法，以简单的聚合条件容易地获得纳米尺寸的聚阳离子颗粒。 构成：将二氧化硅纳米颗粒的表面改性为疏水性。 在改性二氧化硅纳米颗粒表面加入径向引发剂进行减压。 向其中加入引发剂的硅纳米颗粒中加入阳离子单体。 单体通过升高的温度而蒸发。 诱导单体在硅纳米颗粒表面上的聚合。 收集聚阳离子纳米颗粒。
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公开(公告)号：KR1020140014700A
公开(公告)日：2014-02-06
申请号：KR1020120081382
申请日：2012-07-25
Applicant: 서울대학교산학협력단
CPC classification number: B82B3/0009 , B82B1/00 , C01B32/182 , C01B32/194 , C01G3/02
Abstract: The present invention relates to a method of manufacturing a graphene nano-composite having an urchin-like copper oxide therein by using a simple hydrothermal synthetic method under normal pressure, and provides a method of manufacturing an urchin-like structure made of nanometer size needles through a chemical reaction while stirring copper acetate at a high temperature by using graphene oxide as a stabilizer and a mold. The nano-composite manufactured thereby exhibits an excellent antibacterial property against Staphylococcus, which is a gram positive bacillus, and E. coli, which is a gram negative bacillus, which is caused by the copper oxide nano-structure having a large surface area. According to the present invention, a copper oxide nano-structure having an excellent antibacterial property is easily manufactured by a hydrothermal synthetic method, and has an advantage of being manufactured at an economic manufacturing cost and a simple reaction condition.
Abstract translation: 本发明涉及一种在常压下使用简单的水热合成方法制造其中含有海胆样氧化铜的石墨烯纳米复合材料的方法，并且提供了一种制造由纳米尺寸的针制成的海胆样结构的方法 通过使用石墨烯氧化物作为稳定剂和模具，在高温下搅拌乙酸铜时产生化学反应。 由此生产的纳米复合材料对革兰氏阳性杆菌的葡萄球菌和革兰氏阴性芽孢杆菌具有优异的抗菌性，其是由具有大表面积的氧化铜纳米结构引起的。 根据本发明，通过水热合成方法容易地制造具有优异的抗菌性的氧化铜纳米结构体，具有以经济的制造成本和简单的反应条件制造的优点。
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