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公开(公告)号：KR100933617B1
公开(公告)日：2009-12-23
申请号：KR1020080012876
申请日：2008-02-13
Applicant: 서울대학교산학협력단 , 삼성전기주식회사
IPC: C07F9/6564 , C07F9/02
Abstract: A hardening cyclic phosphagen series compound is provided to produce polymer insulated material having excellent thermal stabililty. A hardening cyclic phosphagen series compound has a structure of the chemical formula (1): N3P3(R^1)x(R^2)y. A method for manufacturing the hardening cyclic phosphagen series compound comprises: a step of reacting R1-OH of the chemical formula III with a cyclotriphosphazene under the presence of NaH; a step of isolating hardening phosphazene; and a step of polymerizing the hardening phosphazene to crosslink. The phosphazene series polymer is obtained by simply heating, heating with AIBN (Azobisisobutyronitrile) or photopolymerizing with DMPA (2,2-dimethoxy- 2-phenyl acetophe-none).
Abstract translation: 提供一种硬化环磷腈系列化合物以生产具有优良热稳定性的聚合物绝缘材料。 固化环磷酸酯系列化合物具有化学式（1）的结构：N3P3（R ^ 1）x（R ^ 2）y。 用于制造固化环磷酸酯系列化合物的方法包括：在NaH存在下使化学式III的R 1 -OH与环三磷腈反应的步骤; 分离硬化磷腈的步骤; 以及聚合硬化磷腈以进行交联的步骤。 磷腈系列聚合物通过简单地加热，用AIBN（偶氮二异丁腈）加热或用DMPA（2,2-二甲氧基-2-苯基丙酮 - 无）光聚合而获得。
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Patent Agency Ranking
公开(公告)号：KR1020090087561A
公开(公告)日：2009-08-18
申请号：KR1020080012876
申请日：2008-02-13
Applicant: 서울대학교산학협력단 , 삼성전기주식회사
IPC: C07F9/6564 , C07F9/02
CPC classification number: C07F9/65815
Abstract: A hardening cyclic phosphagen series compound is provided to produce polymer insulated material having excellent thermal stabililty. A hardening cyclic phosphagen series compound has a structure of the chemical formula (1): N3P3(R^1)x(R^2)y. A method for manufacturing the hardening cyclic phosphagen series compound comprises: a step of reacting R1-OH of the chemical formula III with a cyclotriphosphazene under the presence of NaH; a step of isolating hardening phosphazene; and a step of polymerizing the hardening phosphazene to crosslink. The phosphazene series polymer is obtained by simply heating, heating with AIBN (Azobisisobutyronitrile) or photopolymerizing with DMPA (2,2-dimethoxy- 2-phenyl acetophe-none).
Abstract translation: 提供硬化的环状磷酸酯系化合物以制备具有优异的热稳定性的聚合物绝缘材料。 硬化环状磷酸酯系化合物具有化学式（1）的结构：N 3 P 3（R 1）x（R 2））y。 制备硬化环状磷酸酯系化合物的方法包括：使化学式III的R 1 -OH与环三磷腈在NaH存在下反应的步骤; 分离硬化磷腈的步骤; 以及将硬化磷腈聚合以交联的步骤。 通过简单加热，用AIBN（偶氮二异丁腈）加热或用DMPA（2,2-二甲氧基-2-苯基乙酸酯）无光聚合，得到磷腈系聚合物。
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公开(公告)号：KR1020100120968A
公开(公告)日：2010-11-17
申请号：KR1020090039877
申请日：2009-05-07
Applicant: 서울대학교산학협력단
IPC: C07C15/56 , C07C13/615 , C07C2/38
Abstract: PURPOSE: A porous adamantane-based compound and a manufacturing method thereof are provided to use the compound as an adsorber of contaminants including carbon dioxide and environment hormones. CONSTITUTION: A porous adamantane-based compound has the structure marked with chemical formula I. In the chemical formula I, R1 is a compound selected from the group consisting of phenyl and biphenyl. R2 is selected from the phenyl, the biphenyl, and naphthyl. A manufacturing method of the porous adamantane-based compound comprises a step of reacting a compound marked with chemical formula II with a compound marked with chemical formula III.
Abstract translation: 目的：提供多孔金刚烷基化合物及其制备方法，以使用该化合物作为污染物的吸附剂，包括二氧化碳和环境激素。 构成：多孔金刚烷基化合物具有化学式I的结构。在化学式I中，R 1是选自苯基和联苯的化合物。 R2选自苯基，联苯基和萘基。 多孔金刚烷系化合物的制造方法包括使化学式II标记的化合物与化学式Ⅲ标记的化合物反应的工序。
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公开(公告)号：KR1020100120965A
公开(公告)日：2010-11-17
申请号：KR1020090039873
申请日：2009-05-07
Applicant: 서울대학교산학협력단
IPC: C07F9/6593 , C07F9/6571
CPC classification number: C07F9/65815 , C01B3/0015 , C01B3/0084
Abstract: PURPOSE: A porous phosphagen compound and method for preparing the same are provided to ensure high durability by covalent bond with chemical and thermal stability. CONSTITUTION: A porous phosphagen compound has a structure of chemical formula III. In chemical formula III, R1 is phenoxy, phenyl phenoxy, naphthalene oxy, anilino or phenyl anilino; and R 3 is phenyl, biphenyl or naphthyl. The porous phosphagen compound is prepared by reacting a compound of chemical formula I or II and compound of chemical formula V(Cl-CH_2-R_3-CH_2-Cl) in an organic solvent under the presence of aluminum chloride or iron chloride.
Abstract translation: 目的：提供多孔磷酸酯化合物及其制备方法，以确保通过共价键具有化学和热稳定性的高耐久性。 构成：多孔磷酸盐化合物具有化学式III的结构。 在化学式Ⅲ中，R1是苯氧基，苯氧基苯基，萘氧基，苯胺基或苯基苯胺基; R 3为苯基，联苯基或萘基。 通过使化学式I或II的化合物与化学式V化合物（Cl-CH 2 -R 3 -CH 2 Cl）在有机溶剂中，在氯化铝或氯化铁存在下反应制备多孔磷酸酯化合物。
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公开(公告)号：KR101075258B1
公开(公告)日：2011-10-20
申请号：KR1020090039877
申请日：2009-05-07
Applicant: 서울대학교산학협력단
IPC: C07C15/56 , C07C13/615 , C07C2/38
Abstract: 본발명은다공성아다만테인계화합물과중합체그리고이들의제조방법에관한것이다. 상세하게는 1-브로모아다만테인과페닐할라이드를개질하여다공성고분자의빌딩블록을제조하고, 이들을팔라듐(Ⅱ)(Pd(II))과요오드화구리(CuI) 촉매하에서반응시켜제조하는마이크로포러스(micro porous)한다공성화합물과, 아다만테인유도체와보론산유도체를 Pd(II) 촉매하에서반응시켜제조하는다공성화합물및 그제조방법에관한것이다. 이물질로부터제조된다공성화합물은높은비표면적과작은기공크기를갖는다.
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公开(公告)号：KR101057370B1
公开(公告)日：2011-08-17
申请号：KR1020090039873
申请日：2009-05-07
Applicant: 서울대학교산학협력단
IPC: C07F9/6593 , C07F9/6571
Abstract: 본 발명은 다공성 포스파젠계 화합물 및 이들의 제조방법에 관한 것으로, 상세하게는 반응성 치환체인 방향족 화합물을 시클로트리포스파젠에 도입하여 다공성 고분자의 빌딩블록인 환형 포스파젠계 화합물을 제조하고, 이들을 프리델-크라프트반응으로 중합하여 마이크로포러스(micro porous)한 다공성 포스파젠계 화합물을 제조하는 것이다. 제조된 다공성 포스파젠계 고분자는 높은 비표면적과 작은 기공크기를 갖는다.
다공성물질, 극대비표면적, 포스포젠계 화합물, 시클로트리포스파젠, 마이크로포러스, 가스저장, 오염물 흡착Abstract translation: 本发明多孔磷腈系化合物，涉及它们的制备方法，特别是在在环烷基树磷腈导入的芳香族化合物的反应性取代基的多孔聚合物的环状磷腈化合物的制造积木，和那些弗里德尔 - 牛皮纸反应生产微孔多孔磷腈基化合物。 所制备的多孔磷腈类聚合物具有高比表面积和小孔径。
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