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    올레핀의 산화 및 가암모니아 산화용 촉매의 제조 방법
    2.
    发明公开
    올레핀의 산화 및 가암모니아 산화용 촉매의 제조 방법 有权
    用于催化氧化活性氧化态催化氧化氧化催化剂的制备方法，其制备的催化剂和氧化方法以及用于制备硝酸盐的氧化方法

    公开(公告)号：KR1020040047574A

    公开(公告)日：2004-06-05

    申请号：KR1020030076249

    申请日：2003-10-30

    Applicant: 솔루티아인코포레이티드

    Inventor： 트웨이캐시엘.

    IPC: B01J23/843 ,  B01J23/00 ,  B01J23/02 ,  B01J23/887

    CPC classification number: C07C51/252 ,  B01J23/002 ,  B01J23/8871 ,  B01J23/8876 ,  B01J2523/00 ,  C07C45/34 ,  C07C45/35 ,  C07C253/26 ,  Y02P20/52 ,  C07C47/22 ,  C07C57/04 ,  B01J2523/397 ,  B01J2523/53 ,  B01J2523/54 ,  B01J2523/68 ,  B01J2523/842 ,  C07C255/08

    Abstract: PURPOSE: To provide a catalyst useful for the production of acrylonitrile from propylene, ammonia, and an oxygen-containing gas by using a method for preparing an antimonate-based mixed metal oxide catalyst. CONSTITUTION: The process for preparing an antimonate-based mixed metal oxide catalyst in a catalytically active oxidized state comprises steps of (a) contacting an aqueous Sb2O3 slurry with HNO3 and at least one Me compound, and, optionally, at least one compound selected from X, Q, or R compounds to form a first mixture; (b) heating and drying the first mixture to form a solid product; and (c) calcining the solid product, where the catalyst is represented by the following empirical formula: MeaSbbXcQdReOf, wherein Me is at least one element selected from the group consisting of Fe, Co, Ni, Sn, U, Cr, Cu, Mn, Ti, Th, Ce, Pr, Sm, and Nd; X is at least one element selected from the group consisting of V, Mo, and W; Q is at least one element selected from the group consisting of Li, Na, K, Rb, Cs, Be, Mg, Ca, Sr, Ba, Sc, Y, La, Zr, Hf, Nb, Ta, Re, Ru, Os, Rh, Ir, Pd, Pt, Ag, Au, Zn, Cd, Hg, Al, Ga, In, Tl, Ge, Pb, As, and Se; R is at least one element selected from the group consisting of Bi, B, P, and Te; and a, b, c, d, e, and f respectively denote atomic ratios and are as follows: a is 0.1 to 15, b is 1 to 100, c is 0 to 20, d is 0 to 20, e is 0 to 10, and f is a number taken to satisfy the valence requirements of the metals present in the catalyst in the oxidation state.

    Abstract translation: 目的：通过使用制备锑酸盐系混合金属氧化物催化剂的方法，提供可用于从丙烯，氨和含氧气体制造丙烯腈的催化剂。 构成：用于制备催化活性氧化态的锑酸盐类混合金属氧化物催化剂的方法包括以下步骤：（a）使Sb2O3水溶液与HNO 3和至少一种Me化合物和任选的至少一种选自 X，Q或R化合物以形成第一混合物; （b）加热和干燥第一混合物以形成固体产物; 和（c）煅烧固体产物，其中催化剂由以下经验式表示：MeaSbbXcQdReOf，其中Me是选自Fe，Co，Ni，Sn，U，Cr，Cu，Mn中的至少一种元素 ，Ti，Th，Ce，Pr，Sm和Nd; X是选自V，Mo和W中的至少一种元素; Q是选自Li，Na，K，Rb，Cs，Be，Mg，Ca，Sr，Ba，Sc，Y，La，Zr，Hf，Nb，Ta，Re，Ru中的至少一种元素， Os，Rh，Ir，Pd，Pt，Ag，Au，Zn，Cd，Hg，Al，Ga，In，Tl，Ge，Pb，As和Se; R是选自Bi，B，P和Te中的至少一种元素; a，b，c，d，e，f分别表示原子比，a为0.1〜15，b为1〜100，c为0〜20，d为0〜20，e为0〜 10，f为满足在氧化态的催化剂中存在的金属的化合价要求的数字。

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