公开(公告)号：KR101087032B1

公开(公告)日：2011-11-30

申请号：KR1020100112512

申请日：2010-11-12

Applicant: 신한다이아몬드공업 주식회사 ,  재단법인서울대학교산학협력재단

Inventor： 김신경 ,  정기정 ,  김병기 ,  복은 ,  박정환 ,  홍성현 ,  최성우 ,  김이슬

IPC: C09K11/80 ,  C09K11/02

Abstract: PURPOSE: A method for manufacturing an MASN phosphor is provided to minimize the contamination by carbon generated in sintering since boron nitride is coated to a part of carbon mold and/or carbon punch which are contacted with phosphor raw powder. CONSTITUTION: A method for manufacturing an MASN phosphor comprises the steps of: (S1) injecting the phosphor raw powder required for synthesizing the MASN phosphor represented by M_1-xAlSiN_3:LnX into a carbon mold; (S2) installing the carbon mold within the chamber of an electric discharge plasma sintering apparatus and removing oxygen from the chamber; (S3) sintering the fluorescent raw powder; and (S4) obtaining the phosphor powder by pulverizing the sintered material.

Abstract translation: 目的：提供一种用于制造MASN荧光体的方法，以便在烧结中产生的碳的污染最小化，因为氮化硼被涂覆到与荧光粉原料粉末接触的碳模和/或碳冲头的一部分上。 构成：制造MASN荧光体的方法包括以下步骤：（S1）将由M_1-xAlSiN_3：LnX表示的MASN荧光体合成所需的荧光体原料粉末注入碳模具中; （S2）将碳模具安装在放电等离子体烧结装置的室内并从室中除去氧气; （S3）烧结荧光原料粉末; 和（S4）通过粉碎烧结材料获得荧光体粉末。