公开(公告)号：KR100783490B1

公开(公告)日：2007-12-11

申请号：KR1020060070934

申请日：2006-07-27

Applicant: 전남대학교산학협력단

Inventor： 김찬 ,  윤우연 ,  양갑승

IPC: D01F9/12 ,  D01D5/00 ,  D06C7/04

CPC classification number: D01F9/12 ,  D01D5/0038 ,  D06C7/04 ,  Y02E60/13 ,  Y10S977/842

Abstract: A method for manufacturing a C-type carbon nanofiber is provided to regulate the cross-section of the carbon nanofiber, by electrospinning polyacrylonitrile as a carbon fiber precursor and thermoplastic polymer using a Y-shaped nozzle and removing the thermoplastic polymer through a thermal treatment process. A PAN(polyacrylonitrile) spinning solution and a PMMA(polymethylmethacrylate) spinning solution are respectively prepared. The spinning solutions are electro-spun through a Y-shaped nozzle(2) to produce a nanofiber. The nanofiber is thermally treated at 300-350°C under an air ambience to obtain an insolubilized fiber. The insolubilized fiber is incinerated under a vacuum condition or an inert ambience to produce a carbon nanofiber having a C-type cross-section.

Abstract translation: 提供一种制造C型碳纳米纤维的方法，通过使用Y形喷嘴静电纺丝聚丙烯腈作为碳纤维前体和热塑性聚合物来调节碳纳米纤维的横截面，并通过热处理工艺除去热塑性聚合物 。 分别制备PAN（聚丙烯腈）纺丝溶液和PMMA（聚甲基丙烯酸甲酯）纺丝溶液。 纺丝溶液通过Y形喷嘴（2）进行电纺，以生产纳米纤维。 将纳米纤维在空气气氛下在300-350℃进行热处理，得到不溶纤维。 不溶的纤维在真空条件或惰性气氛下焚烧，生产出具有C型横截面的碳纳米纤维。