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公开(公告)号：KR100722380B1
公开(公告)日：2007-05-28
申请号：KR1020020034519
申请日：2002-06-20
Applicant: 주식회사 포스코 , 학교법인 포항공과대학교
IPC: C08G64/20
CPC classification number: C08G64/34
Abstract: 본 발명은 지방족 폴리카보네이트 중합용 촉매의 제조 방법 및 이를 사용한 지방족 폴리카보네이트의 중합 방법에 관한 것으로서, 상기 촉매의 제조 방법은 디카르복실산 전구체와 아연 전구체를 가압 조건 하에서 산화 반응시키는 공정을 포함한다.
상기 방법으로 제조된 촉매는 단결정 형태로써, 촉매 활성이 높다. 또한 본 발명의 촉매 제조 방법은 기존의 촉매 제조시 사용하던 유기 용매 대신에 물을 사용하여 제조 공정의 환경 친화성을 높일 수 있어, 산업적 응용과 함께 이산화탄소에 의한 대기오염 및 기후 변화 현상을 억제시킬 수 있는 지방족 폴리카보네이프의 공중합용 촉매를 높은 효율과 청정 방법으로 제조할 수 있다.
폴리카보네이트,촉매,공중합,단결정-
2.发明公开
公开(公告)号：KR1020060017891A
公开(公告)日：2006-02-27
申请号：KR1020060002660
申请日：2006-01-10
Applicant: 학교법인 포항공과대학교
IPC: H01L21/31
CPC classification number: H01L21/02225 , H01L21/02142 , H01L21/02601 , H01L21/324
Abstract: 본 발명은 중심-껍질(core-shell) 구조의 나노입자를 이용한 저유전성 절연막의 제조방법 및 이로부터 제조되는 저유전성 절연막에 관한 것으로서, 보다 상세하게는 그물망구조의 유기 고분자 중심 입자; 및 상기 유기 고분자 중심 입자를 둘러싸며, 실세스퀴옥산 전중합체로 이루어진 껍질층을 포함하는 중심-껍질(core-shell) 구조의 나노 입자를 이용한 저유전성 절연막의 제조방법 및 이로부터 제조되는 저유전성 절연막에 관한 것이다.
중심-껍질 구조, 그물망구조 유기 고분자, 실세스퀴옥산, 절연막, 유전상수Abstract translation: 本发明是有机高分子中心的核 - 壳粒子，更具体地涉及网络结构涉及一种低介电的绝缘膜，以产生（核 - 壳），使用该结构的纳米颗粒的低介电绝缘膜的制造方法和由此; 以及使用核壳纳米粒子来制造低介电常数绝缘膜的方法，所述核壳纳米粒子包括由倍半硅氧烷预聚物构成的壳层并且包围有机聚合物核粒子， 去绝缘膜。
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公开(公告)号：KR100378253B1
公开(公告)日：2003-03-29
申请号：KR1020000049241
申请日：2000-08-24
Applicant: 학교법인 포항공과대학교
IPC: H01B3/46
Abstract: PURPOSE: Provided are a low dielectric material, which can be used for preparing an extremely low dielectric thin film and contains an organosilane and silicon oxide aerogel, and a process for producing the low dielectric material. CONSTITUTION: The low dielectric material is produced by a sol-gel reaction of the organosilane, the silicon oxide aerogel, and a tetraalkoxysilane, wherein the weight ratio of the organosilane and the silicon oxide aerogel is 99:1-1:99. And the organosilane is selected from the group consisting of 3-acryloxypropyl trimethoxysilane, 3-acryloxypropyl methylmethoxysilane, 3-glycidoxypropyl methyldimethoxysilane, and etc.
Abstract translation: 目的：提供一种可用于制备极低电介质薄膜并含有有机硅烷和氧化硅气凝胶的低介电材料，以及一种生产低介电材料的方法。 构成：低介电材料由有机硅烷，氧化硅气凝胶和四烷氧基硅烷的溶胶 - 凝胶反应制成，其中有机硅烷和氧化硅气凝胶的重量比为99:1-1:99。 并且有机硅烷选自由3-丙烯酰氧基丙基三甲氧基硅烷，3-丙烯酰氧基丙基甲基甲氧基硅烷，3-缩水甘油氧基丙基甲基二甲氧基硅烷等组成的组
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公开(公告)号：KR100352585B1
公开(公告)日：2002-12-31
申请号：KR1019950066191
申请日：1995-12-29
Applicant: 주식회사 포스코 , 학교법인 포항공과대학교
IPC: G01B11/06
Abstract: PURPOSE: A prism coupler device and a method for controlling the same are provided to measure the thickness and refraction rate in the range from below 1 micro m to 15 micro m in a simple manner without any destruction by using laser beams and optical parts. CONSTITUTION: A prism coupler device includes a light source(20) for projecting helium-neon laser beams with main wavelength of 632.8nm, a polarizer(21) for making the polarization state of the light source to TE or TM mode, a beam splitter(22) and an orifice(23) mounted between the polarizer and a prism(10) for assigning a zero point of synchronous angles, a rotary stage(26) to be driven for changing the synchronous angle, a controller(27) for driving a micro step motor, an input/output interface(28) for the telecommunication between a computer(29) and the controller, the computer for controlling the previous operations entirely, and an ADC board interposed between a detector(25') connected to the beam splitter and the computer.
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公开(公告)号：KR100356373B1
公开(公告)日：2002-10-19
申请号：KR1020000059672
申请日：2000-10-11
Applicant: 학교법인 포항공과대학교 , 주식회사 포스코
IPC: C08G63/64
Abstract: 본 발명은 폴리(알킬렌 카보네이트-델타-발레로락톤) 공중합체 및 그의 제조 방법에 관한 것으로서, 이 제조 방법은 이산화탄소, 알킬렌 옥사이드 및 델타-발레로락톤을 촉매 하에서 삼원 공중합하는 공정을 포함한다. 이 제조 방법으로 제조된 폴리(알킬렌 카보네이트-델타-발레로락톤) 공중합체는 하기 화학식 1을 갖는다.
[화학식 1]
(상기 화학식에서, -OA-는 에틸렌 옥사이드, 프로필렌 옥사이드, 1-부텐 옥사이드, 1,1-디메틸에틸렌 옥사이드, 시클로펜텐 옥사이드, 시클로헥센 옥사이드, 1-페닐에틸렌 옥사이드, 1-비닐에틸렌 옥사이드 및 1-트리플루오로메틸에틸렌 옥사이드로 이루어진 군으로부터 선택되는 알킬렌 옥사이드( )의 개환형 화학 구조를 나타내며,
x와 y는 각기 서로 관계없이 2,000 이하의 정수이고, n은 정수로서 x 및 y와는 n = (zxy)의 관계를 가지며 여기에서 z는 20,000 이하의 정수이다.)
상술한 바와 같이, 본 발명은 상술한 바와 같이, 본 발명은 대기 오염의 주범인 이산화탄소를 사용하여 생분해성 폴리(알킬렌 카보네이트-델타-발레로락톤) 공중합체를 제조할 수 있다. 또한, 본 발명의 폴리(알킬렌 카보네이트-델타-발레로락톤)는 우수한 가수분해 및 생분해 특성을 나타내는 공중합체로서, 범용 고분자 소재로는 물론 의료용 고분자 소재로의 응용과 활용이 기대된다.-
Patent Agency Ranking
公开(公告)号：KR1020020032922A
公开(公告)日：2002-05-04
申请号：KR1020000063685
申请日：2000-10-28
Applicant: 학교법인 포항공과대학교 , 엘지디스플레이 주식회사
IPC: C09K19/56
CPC classification number: G02F1/133723 , B32B7/02 , B32B27/28 , C08G73/14 , G02F1/133788 , Y10T428/10 , Y10T428/1005 , Y10T428/1018 , Y10T428/1023 , Y10T428/31721 , Y10T428/31725
Abstract: PURPOSE: Provided are a light oriented material which is excellent in photo reactivity and has a branched chain, and a liquid crystal display device using the light oriented material. CONSTITUTION: The light oriented material comprises branched diamine derivatives represented by formula 1 having photo reactivity. In the formula 1, a and b are individually integer of 0-4, X1 and X2 are individually selected from the group consisting of -CH2, -CH=, -O-, -COO-, -OOC-, -NHCO-, and -CONH-, R1 and R2 are individually selected from the group consisting of hydrogen, halogen group, cyano group, nitro group, amino group, alkyl group of C1-C100, haloalkyl group, cyanoalkyl group, nitroalkyl group, hydroxyalkyl group, cyanohalo alkyl group, nitrohalo alkyl group, cyanonitroalkyl group, hydroxyhaloalkyl group, cyanohydroxyalkyl group, hydroxynitroalkyl group, aryl group of C6-C100, alkylaryl group, haloaryl group, haloalkylaryl group, nitroaryl group, nitroalkylaryl group, cyanoaryl group, cyanoalkylaryl group, nitroaryl group, nitroalkylaryl group, hydroxyaryl group, hydroxyalkylaryl group, cyanohaloaryl group, and cyanohaloalkylaryl group. The liquid crystal display device consists of the first board and the second board; liquid crystal layer formed between the first board and the second board; and an oriented film comprising the light oriented material, which is formed on the first and the second boards.
Abstract translation: 目的：提供光反应性优异且具有支链的光取向材料，以及使用该光取向材料的液晶显示装置。 构成：光取向材料包括由具有光反应性的式1表示的支链二胺衍生物。 在式1中，a和b分别为0-4的整数，X1和X2分别选自-CH2，-CH =，-O - ， - COO - ， - OOC-，-NHCO-， 和-CONH-，R1和R2分别选自氢，卤素基，氰基，硝基，氨基，C1-C100烷基，卤代烷基，氰基烷基，硝基烷基，羟基烷基，氰基卤素 烷基，硝基卤代烷基，氰基硝基烷基，羟基卤代烷基，氰基羟基烷基，羟基硝基烷基，C6-C100芳基，烷基芳基，卤代芳基，卤代烷基芳基，硝基芳基，硝基烷基芳基，氰基芳基，氰基烷基芳基，硝基芳基， 硝基烷基芳基，羟基芳基，羟基烷基芳基，氰基卤代芳基和氰基卤代烷基芳基。 液晶显示装置由第一板和第二板构成; 形成在第一板和第二板之间的液晶层; 以及包含形成在第一和第二板上的光取向材料的取向膜。
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公开(公告)号：KR1020020028589A
公开(公告)日：2002-04-17
申请号：KR1020000059672
申请日：2000-10-11
Applicant: 학교법인 포항공과대학교 , 주식회사 포스코
IPC: C08G63/64
Abstract: PURPOSE: Provided are a poly(alkylene carbonate-delta-valerolactone) copolymer having excellent biodegradability and a process for producing the copolymer by using carbon dioxide. CONSTITUTION: The poly(alkylene carbonate-delta-valerolactone) copolymer represented by the formula 1 is produced by terpolymerizing the carbon dioxide, alkylene oxide, and delta-valerolactone in the presence of a catalyst, wherein the catalyst is zinc glutarate. The poly(alkylene carbonate-delta-valerolactone) copolymer has a molecular weight of 1,000-2,000,000. In the formula, -O-A- is an open ring type structure of alkylene oxide selected from the group consisting of ethylene oxide, propylene oxide, 1-butene oxide, 1,1-dimethylethylene oxide, and etc., x and y are each integers of less than 2,000, n is an integer, wherein n=(z-x-y), and z is an integer of less than 20,000.
Abstract translation: 目的：提供具有优异生物降解性的聚（碳酸亚烷基酯-δ-戊内酯）共聚物和使用二氧化碳制备共聚物的方法。 构成：由式1表示的聚（碳酸亚烷基酯-δ-戊内酯）共聚物是通过在催化剂存在下使二氧化碳，环氧烷和δ-戊内酯进行三元共聚来制备的，其中催化剂是戊二酸锌。 聚（碳酸亚烷基酯-δ-戊内酯）共聚物的分子量为1,000-2,000,000。 在式中，-OA-是环氧乙烷，环氧丙烷，1-丁烯氧化物，1,1-二甲基环氧乙烷等的环氧烷烃的开环型结构，x和y各自为整数 小于2,000，n是整数，其中n =（zxy），z是小于20,000的整数。
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公开(公告)号：KR1020020021457A
公开(公告)日：2002-03-21
申请号：KR1020000054172
申请日：2000-09-15
Applicant: 주식회사 포스코 , 학교법인 포항공과대학교
IPC: C08G73/00
CPC classification number: C08G73/00 , C08G73/0266 , C08L79/04 , C08L2203/206
Abstract: PURPOSE: Provided is a soluble polyanthranilic acid-based polymer, which is soluble in a water solution and an organic solvent, therefore, which can be used as a coating material for steel plates instead of a chromate coating material. CONSTITUTION: The soluble polyanthranilic acid-based polymer is produced by a process comprising the steps of: mixing anthranilic acid(formula 1) and aniline in the mol% ratio of 1:99-100:0 and dissolving the mixture in an acid solvent at 10-50deg.C; adding an oxidizing agent, dissolved in the acid solvent, to the solution in the molar ratio of 1:5-5:1 at 10-50deg.C and a flow rate of 0.01-10ml/min; performing polymerization at 10-50deg.C and vacuum-drying at 10-100deg.C; adding the dried resultant to a doping solution such as sulfuric acid and stirring for more than 24 hours and then vacuum-drying at 10-100deg.C. The produced soluble polyanthranilic acid-based polymer has a molecular weight of 1,000-2,500,000.
Abstract translation: 目的：提供可溶于水溶液和有机溶剂的可溶性聚邻氨基苯甲酸类聚合物，因此可用作钢板的涂料而不是铬酸盐涂料。 构成：通过包括以下步骤的方法制备可溶性聚邻氨基苯甲酸聚合物：将摩尔％比为1:99-100:0的邻氨基苯甲酸（式1）和苯胺混合，并将该混合物溶解在酸溶剂中 10-50deg.C; 在10〜50℃，摩尔比为1：5-5：1的溶液中加入溶解在酸性溶剂中的氧化剂，流速为0.01〜10 ml / min; 在10-50℃下进行聚合，10-100℃真空干燥; 将干燥的产物加入到诸如硫酸的掺杂溶液中并搅拌超过24小时，然后在10-100℃真空干燥。 生产的可溶性聚邻氨基苯甲酸类聚合物的分子量为1,000-2,500,000。
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公开(公告)号：KR1020020016092A
公开(公告)日：2002-03-04
申请号：KR1020000049241
申请日：2000-08-24
Applicant: 학교법인 포항공과대학교
IPC: H01B3/46
Abstract: PURPOSE: Provided are a low dielectric material, which can be used for preparing an extremely low dielectric thin film and contains an organosilane and silicon oxide aerogel, and a process for producing the low dielectric material. CONSTITUTION: The low dielectric material is produced by a sol-gel reaction of the organosilane, the silicon oxide aerogel, and a tetraalkoxysilane, wherein the weight ratio of the organosilane and the silicon oxide aerogel is 99:1-1:99. And the organosilane is selected from the group consisting of 3-acryloxypropyl trimethoxysilane, 3-acryloxypropyl methylmethoxysilane, 3-glycidoxypropyl methyldimethoxysilane, and etc.
Abstract translation: 目的：提供一种低介电材料，其可用于制备极低电介质薄膜并含有有机硅烷和氧化硅气凝胶，以及制备低电介质材料的方法。 构成：通过有机硅烷，氧化硅气凝胶和四烷氧基硅烷的溶胶 - 凝胶反应制造低电介质材料，其中有机硅烷和氧化硅气凝胶的重量比为99:1-1:99。 有机硅烷选自3-丙烯酰氧基丙基三甲氧基硅烷，3-丙烯酰氧基丙基甲基甲氧基硅烷，3-缩水甘油氧基丙基甲基二甲氧基硅烷等。
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10.发明公开라미네이트필름용폴리에스테르공중합체수지의제조방법및이로부터제조된고분자주쇄에술폰산기측쇄를갖는폴리에스테르공중합체수지 失效用于生产聚烯烃聚合物树脂的方法用于层压薄膜和聚氨酯树脂在其主链中具有磺酸基团
公开(公告)号：KR1020000042534A
公开(公告)日：2000-07-15
申请号：KR1019980058754
申请日：1998-12-26
Applicant: 학교법인 포항공과대학교 , 주식회사 포스코
IPC: C08G63/688
CPC classification number: C08G63/688 , C08L67/00
Abstract: PURPOSE: A process for preparing a polyester copolymer resin for laminate film and a polyester copolymer resin having a sulfonic acid group in a main chain is provided which produces the title compound by controlling the content of diethylene glycol units generated as a side reaction in the manufacture of polyester. CONSTITUTION: A resin is prepared by (a) reacting terephthalic acid derivatives of formula 1, ethylene glycol of formula : HOCH2CH2OH and 5-sulfoisophthalic acid derivatives of formula 3 in the presence of metal acetate at 180 to 205°C, (b) polycondensing the reactant in the presence of metal acetate at 205 to 280°C under reduced pressure of from 100 to 10 torr for about 1 hr, (c) polycondensing at 280°C at a pressure of 1 to 2 torr. In formula, R1,R2 are each independently H or C1-C10 alkyl, M+ is selected from alkali metal ions containing Li+, Na+ or K+. The polymer resin has improved processability and does not cause the problems of environmental pollution.
Abstract translation: 目的：提供一种制备用于层压膜的聚酯共聚物树脂和在主链中具有磺酸基的聚酯共聚物树脂的方法，其通过控制在制备中作为副反应产生的二甘醇单元的含量来产生标题化合物 的聚酯。 构成：通过（a）在金属乙酸盐存在下，在180〜205℃下使式1的对苯二甲酸衍生物，式：HOCH 2 CH 2 OH的乙二醇与式3的5-磺基间苯二甲酸衍生物反应，（b）缩聚 该反应物在金属乙酸盐存在下，在205-280℃，100-10托的减压下约1小时，（c）在280℃，1至2托的压力下进行缩聚。 在式中，R 1，R 2各自独立地为H或C 1 -C 10烷基，M +选自含有Li +，Na +或K +的碱金属离子。 聚合物树脂具有改善的加工性能，不会引起环境污染的问题。
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