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    아조계 금속 착제 반응성 염료, 이의 제조 방법 및 이를포함하는 조성물
    4.
    发明授权
    아조계 금속 착제 반응성 염료, 이의 제조 방법 및 이를포함하는 조성물 失效
    아조계금속착제반응성염료，이의제조방법및이를포함하는조성물

    公开(公告)号：KR100688310B1

    公开(公告)日：2007-03-02

    申请号：KR1020050080366

    申请日：2005-08-30

    Applicant: 한국과학기술연구원 ,  (주)바이오액츠

    Inventor： 김동찬 ,  김동진 ,  박웅서 ,  나종주 ,  고석영 ,  박진우

    IPC: C09B45/00 ,  C09B45/38

    Abstract: Provided is an azo-based metal complex reactive dye, which has advantages of both azo-based metal complex dyes and reactive dyes, and shows an improved sunlight fastness and a high fixation ratio. The azo-based metal complex reactive dye is represented by a formula of MxAyBz, wherein M represents a metal selected from the group consisting of Cr, Co, Fe, Cu and Ni; each of x and y represents 1 or 2, and z is 1, 2 or 3; A is selected from tridendate ligands represented by formulae 7-13; B represents H2O or is selected from tridendate ligands represented by the formulae 7-13; each of R1 and R2 is selected from the group consisting of -OH, -NH2, -COOH, -NHCOCH2COCH3 and -NH-(C6H5); and at least one of R3-R9 is -NHCOCHBrCH2Br or -NHCOCBr=CH2, and each of the remaining substituents of R3-R9 is selected from the group consisting of -H, -NH2, -SO3H, -OH, -COOH, -CH3, -OCH3, -NH-(C6H5), -NH-(C6H5)CH3, -NHSO2-(C6H5), -NHSO2-(C6H5)Cl, -NHSO2-(C6H5)COOH, -NHCOCH3, -NH2CH3, -SO2NH2, -NHSO2CH3, -N(CH3)2, -N(C2H5)2, -NO2, -NHCONH2, -CONH2, -N(C2H4OH)2 and -OC2H5.

    Abstract translation: 本发明提供一种偶氮类金属络合物活性染料，其兼具偶氮类金属络合物染料和活性染料两者的优点，并且显示出改善的日光牢度和高固色率。 偶氮类金属络合物反应性染料由式M x A y B z表示，其中M表示选自Cr，Co，Fe，Cu和Ni的金属; x和y中的每一个代表1或2，并且z是1,2或3; A选自由式7-13表示的十三酸配体; B代表H 2 O或选自式7-13代表的十三配位体; R 1和R 2各自选自-OH，-NH 2，-COOH，-NHCOCH 2 COCH 3和-NH-（C 6 H 5）; 并且R3-R9中的至少一个是-NHCOCHBrCH2Br或-NHCOCBr = CH2，并且R3-R9的其余取代基中的每一个选自-H，-NH2，-SO3H，-OH，-COOH， - （C 6 H 5）CH 3，-NHSO 2 - （C 6 H 5）， - NHSO 2 - （C 6 H 5）Cl，-NHSO 2 - （C 6 H 5）COOH，-NHCOCH 3，-NH 2 CH 3， - -N（CH 2）5，-NO 2，-NHCONH 2，-CONH 2，-N（C 2 H 4 OH）2和-OC 2 H 5。

    생체 분자 표지를 위한 신규 시아닌 화합물 및 그 제조방법
    5.
    发明公开
    생체 분자 표지를 위한 신규 시아닌 화합물 및 그 제조방법 有权
    用于标记生物分子的新型氰胺化合物及其制备方法

    公开(公告)号：KR1020100115301A

    公开(公告)日：2010-10-27

    申请号：KR1020100030228

    申请日：2010-04-02

    Applicant: (주)바이오액츠 ,  한국과학기술연구원

    Inventor： 김동진 ,  김영수 ,  나종주 ,  박진우 ,  김기원

    IPC: C07D403/02 ,  C07D209/04

    CPC classification number: C07D403/06 ,  C07D209/08

    Abstract: PURPOSE: A novel cyanine compound for labeling molecule and method for preparing the same are provided to ensure high stability without additional purification. CONSTITUTION: A novel cyanine compound for labeling molecules is denoted by chemical formula 1. The compound has fluorescence at 500-800 nm wave length. The compound is labeled with bio molecule, nanoparticles or organic compound containing amine group, hydroxyl group, or thiol group. A method for preparing the compound of chemical formula 1 comprises: a step of reacting a compound of chemical formula 4 with a compound of chemical formula 5 or 7 to obtain a compound of chemical formula 6a; a step of reacting the compound of chemical formula 6a with a compound of chemical formula 8 to obtain a compound of chemical formula 9; a step of reacting the compound of chemical formula 9 with a compound of chemical formula 6b to obtain a compound of chemical formula 10; a step of reacting the compound of chemical formula 10 with 1,1'-carbonyldiimidazole or N,N-disuccineimidyl carbonate to obtain a compound of chemical formula 11a or 11b; and a step of reacting the compound of chemical formula 11a or 11b with a compound of chemical formula 12 under the presence of Hunig base.

    Abstract translation: 目的：提供用于标记分子的新颖花青化合物及其制备方法，以确保高稳定性而无需额外纯化。 构成：化学式1表示用于标记分子的新型花青化合物。化合物在500-800nm波长处具有荧光。 该化合物用生物分子，纳米颗粒或含有胺基，羟基或硫醇基的有机化合物进行标记。 制备化学式1的化合物的方法包括：使化学式4的化合物与化学式5或7的化合物反应以获得化学式6a的化合物的步骤; 使化学式6a的化合物与化学式8的化合物反应，得到化学式9的化合物的工序; 使化学式9的化合物与化学式6b的化合物反应，得到化学式10的化合物的工序; 使化学式10的化合物与1,1'-羰基二咪唑或N，N-二琥珀酰亚胺基碳酸酯反应，得到化学式11a或11b的化合物的步骤; 以及使化学式11a或11b的化合物与化学式12的化合物在Hunig碱的存在下反应的步骤。

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