公开(公告)号：KR100376203B1

公开(公告)日：2003-03-15

申请号：KR1020000081696

申请日：2000-12-26

Applicant: 한국에너지기술연구원

Inventor： 박상도 ,  김선욱

IPC: C08B16/00

CPC classification number: Y02P20/544

Abstract: PURPOSE: Provided are a method and a device which substantially increase a reaction rate of hydrolysis using a supercritical water and improve the yield of hydrolysis. CONSTITUTION: The method comprises the steps of (i) heating and pressurizing a raw water containing a small amount of sulfuric acid or sulfate in a heating part(4), (ii) providing the raw water to reactor(8) together with cellulose slurry provided by the slurry pump(10) to effect a hydrolysis, (ii) terminating a reaction by firstly cooling the reactants discharged from the reactor(8) with cooling water provided from cooling water tank(12), (iii) completely terminating a reaction by secondarily cooling the reactants by heat exchanger(13), (iv) passing the reaction product to filter unit(14) to filter an unreacted cellulose, while the filtrate being obtained from a product collecting tank.

Abstract translation: 目的：提供一种显着增加使用超临界水的水解反应速率并提高水解产率的方法和装置。 构成：该方法包括以下步骤：（i）在加热部分（4）中加热和加压含有少量硫酸或硫酸盐的原水，（ii）将原水与纤维素浆料 （10）提供以实现水解，（ii）通过首先用从冷却水罐（12）提供的冷却水冷却从反应器（8）排出的反应物，终止反应，（iii）完全终止反应 通过热交换器（13）二次冷却反应物，（iv）使反应产物通过过滤单元（14）以过滤未反应的纤维素，同时从产物收集罐获得滤液。

公开(公告)号：KR1020020053896A

公开(公告)日：2002-07-06

申请号：KR1020000081696

申请日：2000-12-26

Applicant: 한국에너지기술연구원

Inventor： 박상도 ,  김선욱

IPC: C08B16/00

CPC classification number: Y02P20/544

Abstract: PURPOSE: Provided are a method and a device which substantially increase a reaction rate of hydrolysis using a supercritical water and improve the yield of hydrolysis. CONSTITUTION: The method comprises the steps of (i) heating and pressurizing a raw water containing a small amount of sulfuric acid or sulfate in a heating part(4), (ii) providing the raw water to reactor(8) together with cellulose slurry provided by the slurry pump(10) to effect a hydrolysis, (ii) terminating a reaction by firstly cooling the reactants discharged from the reactor(8) with cooling water provided from cooling water tank(12), (iii) completely terminating a reaction by secondarily cooling the reactants by heat exchanger(13), (iv) passing the reaction product to filter unit(14) to filter an unreacted cellulose, while the filtrate being obtained from a product collecting tank.

Abstract translation: 目的：提供一种使用超临界水显着增加水解反应速率并提高水解产率的方法和装置。 方案：该方法包括以下步骤：（i）在加热部分（4）中加热和加压含有少量硫酸或硫酸盐的原水，（ii）将原水与纤维素浆料一起提供给反应器 由浆料泵（10）提供以进行水解，（ii）通过首先用从冷却水箱（12）提供的冷却水冷却从反应器（8）排出的反应物来终止反应，（iii）完全终止反应 通过热交换器（13）二次冷却反应物，（iv）将过滤器从产品收集罐获得，将反应产物通过过滤器单元（14）以过滤未反应的纤维素。