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公开(公告)号：KR100130188B1
公开(公告)日：1998-04-03
申请号：KR1019930009976
申请日：1993-06-03
Applicant: 한국화학연구원
IPC: C09K3/16
Abstract: Antistatic agent composition having improved flexibilities and hygroscopic properties was prepared. Various kinds of fatty acids and aminoethyl ethanolamine were reacted at 170 deg.C for 3 hours, at 190-200 deg.C for 3-8 hours to synthesize 2-alkyl-1- hydroxyethyl -2-imidazoline, followed by the reaction of dimethyl sulfate to give compound(I). 5 Mol of ethylene oxide was added in monoalkylamine to give compound(II). The antistatic agent composition was prepared from compound(I) and (II) at the ratio of 4:6.
Abstract translation: 制备具有改善的柔性和吸湿性能的抗静电剂组合物。 将各种脂肪酸和氨基乙基乙醇胺在170℃下反应3小时，在190-200℃下反应3-8小时，合成2-烷基-1-羟乙基-2-咪唑啉，然后与 硫酸二甲酯，得到化合物（I）。 在单烷基胺中加入5mol环氧乙烷，得到化合物（II）。 抗静电剂组合物由化合物（I）和（II）以4:6的比例制备。
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公开(公告)号：KR1019940006255B1
公开(公告)日：1994-07-13
申请号：KR1019920003768
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
Abstract: N,N'-diacyldiethylene bishydroxy alkyltriamine methyl sulfate of formula (I) useful as a softening agent for fiber is prepd. by: reacting 2 mole fattic acid and 1 mole diethylene triamine and then adding and reacting with 1 mole water to prepare N,N'-diacyl diethylene triamine of formula (II); reacting with epoxide, e.g. ethylene oxide or propylene oxide; then reacting with dimethyl sulfate. In the formulas, R is C12-C20 alkyl; R1 is H or methyl. The obtd. cpd. has excellent flexibility.
Abstract translation: 可用作纤维软化剂的式（I）的N，N'-二酰基二亚乙基双羟基烷基三胺甲基硫酸盐是制备的。 通过：使2摩尔脂肪酸和1摩尔二亚乙基三胺反应，然后加入并与1摩尔水反应制备式（II）的N，N'-二酰基二亚乙基三胺; 与环氧化物反应，例如 环氧乙烷或环氧丙烷; 然后与硫酸二甲酯反应。 式中R为C 12 -C 20烷基; R1是H或甲基。 有限公司 CPD。 具有极好的灵活性。
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公开(公告)号：KR1019930019921A
公开(公告)日：1993-10-19
申请号：KR1019920003768
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
Abstract: 본 발명은 섬유유연제 N,N′-디아실디에틸렌비스히도록시알킬트리아민메틸설페이트의 제조방법에 관한것으로서 이미다졸린을 가수분해하여 얻어지는 디아미도아민을 에폭시화반응 및 사차화반응시켜 기존의 섬유유연제보다 유연성이 우수한 섬유유연제를 제조하였으며, 이미다졸린계유연제보다 약 7∼22%유연성이 향상되는 효과가 있다.
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Patent Agency Ranking
公开(公告)号：KR100078216B1
公开(公告)日：1994-10-13
申请号：KR1019920003768
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
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公开(公告)号：KR1019940006256B1
公开(公告)日：1994-07-13
申请号：KR1019920003769
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
Abstract: The fiber softening agent composition is composed of dialkyl imidazoline methyl sulfate of formula (I) as the imidazoline based fiber softening agent component, and N,N'-diacyldiethylene bishydroxy alkyltriamine methyl sulfate of formula (II) as the diamide based fiber softening agent component. The comprising ratio of (I) to (II) is 3:7. The said dialkyl is C12-C20 acyl, and the hydroxy alkyl is hydroxy ethyl or hydroxy propyl. In the formulas, R is C12-C20 alkyl, R1 is H or methyl. The obtd. fiber softening agent has good flexibility and improved antistatic property.
Abstract translation: 纤维软化剂组合物由作为咪唑啉系纤维软化剂组分的式（I）的二烷基咪唑啉甲基硫酸盐和作为二酰胺类纤维软化剂成分的式（II）的N，N'-二酰基二亚乙基双羟基烷基三胺甲基硫酸盐 。 （I）〜（II）的比例为3:7。 所述二烷基是C 12 -C 20酰基，羟基烷基是羟基乙基或羟基丙基。 式中R为C 12 -C 20烷基，R 1为H或甲基。 有限公司 纤维软化剂具有良好的柔韧性和抗静电性能。
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公开(公告)号：KR100078215B1
公开(公告)日：1994-10-13
申请号：KR1019920003769
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
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公开(公告)号：KR1019930019922A
公开(公告)日：1993-10-19
申请号：KR1019920003769
申请日：1992-03-07
Applicant: 한국화학연구원
IPC: D06M13/256
Abstract: 본 발명은 이미다졸린계 섬유유연제와 디아미드계 유연제를 3:7의 조성물로서 뛰어난 유연성을 나타낼뿐아니라, 대전성도 디아미드계 유연제보다 우수한 효과가 있으며 이미다졸린계 : 디아미드계=3:7의 조성물의 유연성이 향상되는 효과가 있다.
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