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公开(公告)号：KR100447939B1
公开(公告)日：2004-09-08
申请号：KR1020020038326
申请日：2002-07-03
IPC: C09K3/00
Abstract: PURPOSE: A composition for removing advertising stickers and labels is provided, to allow the stickers and labels to be removed cleanly and easily by weakening the adhesive strength between the stickers or labels and a board or a wall. CONSTITUTION: The composition comprises 5-22 wt% of an adhesive rigid resin which has a glass transition temperature of 40-130 deg.C and is soluble in the used solvent; and 78-95 wt% of a mixture of a high boiling point organic solvent and a low boiling point organic solvent whose boiling points are different each other. Preferably the adhesive rigid resin is polystyrene, poly(styrene-co-maleic anhydride), polyacrylonitrile, poly(styrene-co-acrylonitrile), poly(vinyl chloride-co-vinyl acetate), carboxyl group-containing poly(vinyl chloride-co-vinyl acetate), poly(methyl acrylate-co-ethyl acrylate), carboxyl group-containing poly(methyl acrylate-co-ethyl acrylate), poly(methyl methacrylate-co-vinyl acetate), or carboxyl group-containing poly(methyl methacrylate-co-vinyl acetate). Preferably the solvent mixture comprises 20-90 wt% of a high boiling point organic solvent and 10-80 wt% of a low boiling point organic solvent.
Abstract translation: 目的：提供一种用于去除广告标签和标签的组合物，以便通过减弱标签或标签与板或墙之间的粘合强度来干净且容易地去除标签和标签。 构成：该组合物包含5-22重量％的玻璃化转变温度为40-130℃且可溶于所用溶剂的粘合剂硬质树脂; 和78-95重量％的沸点彼此不同的高沸点有机溶剂和低沸点有机溶剂的混合物。 优选地，粘合剂硬质树脂是聚苯乙烯，聚（苯乙烯 - 马来酸酐共聚物），聚丙烯腈，聚（苯乙烯-co-丙烯腈），聚（氯乙烯 - 共 - 乙酸乙烯酯），含羧基的聚（氯乙烯 - 乙烯基乙酸酯），聚（丙烯酸甲酯 - 共 - 乙基丙烯酸酯），含羧基的聚（丙烯酸甲酯-co-乙基丙烯酸酯），聚（甲基丙烯酸甲酯 - 共 - 乙酸乙烯酯）或含羧基的聚 甲基丙烯酸酯 - 共 - 乙酸乙烯酯）。 优选溶剂混合物包含20-90重量％的高沸点有机溶剂和10-80重量％的低沸点有机溶剂。
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公开(公告)号：KR100442113B1
公开(公告)日：2004-07-30
申请号：KR1020020010607
申请日：2002-02-27
Applicant: 한국화학연구원 , 히포메디칼 주식회사
IPC: C09J133/00
Abstract: PURPOSE: A composition for the adhesion of cellulose, a method for preparing a medical cotton pad and a medical cotton pad prepared by the method are provided, to improve the water and blood absorptive power by maximizing the crosslinking efficiency. CONSTITUTION: The composition comprises 0.5-1.5 wt% of a poly(acrylic acid)-based resin; 0.4-0.9 wt% of liquid ammonia (28%); 0.01-0.06 wt% of chitosan; 0.6-1.7 wt% of acetic acid; and water. Preferably the poly(acrylic acid)-based resin is a poly(acrylic acid-co-maleic anhydride) copolymer. The method comprises the steps of soaking 1 parts by weight of cotton into 3-8 parts by weight of the composition; placing the soaked cellulose cotton on a polished stainless plate and compressing the cotton by using a rubber roller with a pressure of 0.5-2 kgf/cm¬2 3-10 times for 3-40 sec; and drying it with a hot wind of 40-80 deg.C for 0.5-6 hours.
Abstract translation: 目的：提供一种用于纤维粘合的组合物，一种制备医用化妆棉的方法以及通过该方法制备的医用化妆棉垫，以通过最大化交联效率来提高水和血液的吸收能力。 构成：组合物包含0.5-1.5重量％的聚（丙烯酸）基树脂; 0.4-0.9重量％的液氨（28％）; 0.01-0.06重量％的壳聚糖; 0.6-1.7重量％的乙酸; 和水。 优选聚（丙烯酸）基树脂是聚（丙烯酸 - 共 - 马来酸酐）共聚物。 该方法包括将1重量份棉花浸入3-8重量份组合物中的步骤; 将浸透的纤维素棉放置在抛光的不锈钢板上，并通过使用压力为0.5-2kgf / cm 2的橡胶辊压缩棉花; 3-10次，3-40秒; 并用40-80℃的热风干燥0.5-6小时。
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公开(公告)号：KR1020030071078A
公开(公告)日：2003-09-03
申请号：KR1020020010607
申请日：2002-02-27
Applicant: 한국화학연구원 , 히포메디칼 주식회사
IPC: C09J133/00
Abstract: PURPOSE: A composition for the adhesion of cellulose, a method for preparing a medical cotton pad and a medical cotton pad prepared by the method are provided, to improve the water and blood absorptive power by maximizing the crosslinking efficiency. CONSTITUTION: The composition comprises 0.5-1.5 wt% of a poly(acrylic acid)-based resin; 0.4-0.9 wt% of liquid ammonia (28%); 0.01-0.06 wt% of chitosan; 0.6-1.7 wt% of acetic acid; and water. Preferably the poly(acrylic acid)-based resin is a poly(acrylic acid-co-maleic anhydride) copolymer. The method comprises the steps of soaking 1 parts by weight of cotton into 3-8 parts by weight of the composition; placing the soaked cellulose cotton on a polished stainless plate and compressing the cotton by using a rubber roller with a pressure of 0.5-2 kgf/cm¬2 3-10 times for 3-40 sec; and drying it with a hot wind of 40-80 deg.C for 0.5-6 hours.
Abstract translation: 目的：提供通过该方法制备的用于纤维素粘合的组合物，制备医用棉垫的方法和医用棉垫，以通过最大化交联效率来提高水和吸收吸收力。 组成：该组合物包括0.5-1.5重量％的基于聚（丙烯酸）的树脂; 0.4-0.9重量％的液氨（28％）; 0.01-0.06重量％的壳聚糖; 0.6-1.7重量％的乙酸; 和水。 优选地，基于聚（丙烯酸）的树脂是聚（丙烯酸 - 共 - 马来酸酐）共聚物。 该方法包括以下步骤：将1重量份棉花浸泡在组合物的3-8重量份中; 将浸泡的纤维素棉放置在抛光的不锈钢板上，并使用压力为0.5-2kgf / cm 3的橡胶辊3-10次，压制棉花3-40秒; 并用40-80℃的热风干燥0.5-6小时。
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公开(公告)号：KR100419852B1
公开(公告)日：2004-02-25
申请号：KR1020010060650
申请日：2001-09-28
Applicant: 한국화학연구원
IPC: C08F8/36
Abstract: PURPOSE: A chelate resin for adsorbing a specific heavy metal ion and its preparation method are provided, to improve the adsorption property by increasing the hydrophilicity and adding unshared electron pairs to the structure. CONSTITUTION: The chelate resin comprises a side chain of a spherical polystyrene copolymer, where the side chain is a phenyl ring has an acetic acid group adjoining linearly to a sulfone amide structure chain as a functional group, and is represented by the formula 1, wherein A is H, Na or K. The method comprises the steps of reacting a spherical polystyrene copolymer which is prepared by the suspension copolymerization of styrene using divinyl benzene as a crosslinking agent, with chlorosulfonic acid to prepare a chlorosulfonated copolymer resin; and reacting the obtained chlorosulfonated copolymer resin with iminodiacetic acid.
Abstract translation: 目的：提供一种吸附特定重金属离子的螯合树脂及其制备方法，通过增加亲水性和向结构中添加非共享电子对来改善吸附性能。 组成：螯合树脂包含球形聚苯乙烯共聚物的侧链，其中侧链是苯环，具有与磺酰胺结构链线性相邻的乙酸基团作为官能团，并且由式1表示，其中 A是H，Na或K.该方法包括以下步骤：使用二乙烯基苯作为交联剂通过苯乙烯的悬浮共聚制备的球形聚苯乙烯共聚物与氯磺酸反应以制备氯磺化共聚物树脂; 并使得到的氯磺化共聚物树脂与亚氨基二乙酸反应。
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公开(公告)号：KR100419851B1
公开(公告)日：2004-02-25
申请号：KR1020010060649
申请日：2001-09-28
Applicant: 한국화학연구원
IPC: C08F8/36
Abstract: PURPOSE: A chelate resin for adsorbing specific heavy metal ions and its preparation method are provided, to improve the adsorbing property to specific heavy metal ions by introducing a sulfonyl dithiocarbamic acid group into the phenyl ring of a spherical polystyrene as a chelate functional group and thereby improving the hydrophilicity and the coordinating property. CONSTITUTION: The chelate resin is represented by the formula 1, wherein A is H, K or Na. The method comprises the steps of preparing a spherical polystyrene by suspension polymerization of styrene using a divinylbenzene as a crosslinking agent, and reacting the spherical polystyrene with chlorosulfonic acid to obtain the chlorosulfonated copolymer represented by the formula 2; aminating the copolymer of the formula 2 by using liquid ammonia to prepare the sulfonamide group-containing copolymer represented by the formula 3; and reacting the copolymer of the formula 3 with carbon disulfide to introduce a dithiocarboxylic group into the copolymer and neutralizing the obtained one.
Abstract translation: 目的：提供一种用于吸附特定重金属离子的螯合树脂及其制备方法，以通过将磺酰基二硫代氨基甲酸基团引入作为螯合官能团的球形聚苯乙烯的苯环来提高对特定重金属离子的吸附性能 改善亲水性和配位性。 构成：螯合树脂由式1表示，其中A是H，K或Na。 所述方法包括以下步骤：通过使用二乙烯基苯作为交联剂使苯乙烯悬浮聚合来制备球形聚苯乙烯，并且使球形聚苯乙烯与氯磺酸反应以获得由式2表示的氯磺化共聚物; 通过使用液氨将式2的共聚物胺化以制备式3所示的含磺酰胺基团的共聚物; 和使式3的共聚物与二硫化碳反应以将二硫代羧酸基团引入共聚物中并中和得到的二硫代羧酸基团。
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Patent Agency Ranking
公开(公告)号：KR1020030027417A
公开(公告)日：2003-04-07
申请号：KR1020010060650
申请日：2001-09-28
Applicant: 한국화학연구원
IPC: C08F8/36
Abstract: PURPOSE: A chelate resin for adsorbing a specific heavy metal ion and its preparation method are provided, to improve the adsorption property by increasing the hydrophilicity and adding unshared electron pairs to the structure. CONSTITUTION: The chelate resin comprises a side chain of a spherical polystyrene copolymer, where the side chain is a phenyl ring has an acetic acid group adjoining linearly to a sulfone amide structure chain as a functional group, and is represented by the formula 1, wherein A is H, Na or K. The method comprises the steps of reacting a spherical polystyrene copolymer which is prepared by the suspension copolymerization of styrene using divinyl benzene as a crosslinking agent, with chlorosulfonic acid to prepare a chlorosulfonated copolymer resin; and reacting the obtained chlorosulfonated copolymer resin with iminodiacetic acid.
Abstract translation: 目的：提供一种用于吸附特定重金属离子的螯合树脂及其制备方法，通过增加亲水性和向结构中添加非共享电子对来提高吸附性能。 构成：螯合树脂包含球形聚苯乙烯共聚物的侧链，其中侧链是苯环具有与作为官能团的砜酰胺结构链线性邻接的乙酸基团，并且由式1表示，其中 A是H，Na或K.该方法包括使用二乙烯基苯作为交联剂将通过苯乙烯的悬浮共聚制备的球形聚苯乙烯共聚物与氯磺酸反应以制备氯磺化共聚物树脂的步骤; 并使得到的氯磺化共聚物树脂与亚氨基二乙酸反应。
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公开(公告)号：KR1020060022181A
公开(公告)日：2006-03-09
申请号：KR1020040070985
申请日：2004-09-06
Applicant: 한국화학연구원 , 에이케이켐텍 주식회사
CPC classification number: C08F8/36 , C08F279/06 , C08K5/0025 , C08L51/04
Abstract: 본 발명은 중금속이온 흡착용 티올기 함유 슬폰산계 킬레이트 수지에 관한 것으로, 더욱 상세하게는 스티렌과 메틸메타크릴레이트를 단량체로 사용하고 디비닐벤젠을 가교제로 사용하여 중합된 구상(球狀)의 공중합체를 골격구조로 하고, 골격구조에서 볼 때 측쇄 길이가 긴 스티렌과 측쇄 길이가 짧은 메틸메타크릴레이트의 단위구조 각각에 슬폰산기와 티올기를 관능기로 배치시켜 이종(異種) 관능기 간의 간섭을 최소화하고 관능기 간의 킬레이트 능력이 개선되도록 일정 공간을 확보해 줌으로써, 슬폰산기에 대해 낮은 흡착능을 보이는 Hg
2+ 이온에 대한 흡착능을 보완하고, 기존에 우수한 흡착능을 보인 특정의 중금속이온들에 대해서도 킬레이트 형성능력을 보다 개선하는 티올기 함유 슬폰산계 킬레이트 수지에 관한 것이다.
티올 관능기, 슬폰산 관능기, 킬레이트 수지, 중금속이온 흡착능-
公开(公告)号：KR100512332B1
公开(公告)日：2005-09-05
申请号：KR1020030060863
申请日：2003-09-01
Applicant: 한국화학연구원 , 에이케이켐텍 주식회사
IPC: C08G61/02
Abstract: 본 발명은 특정 중금속이온 흡착용 술폰산기 함유 킬레이트 수지에 관한 것으로서, 더욱 상세하게는 구상(球狀)의 폴리스티렌 공중합체의 페닐 측쇄에는 N-메틸술폰아미드 결합구조의 공간자(spacer)가 도입되어 있고, 연이어서 술폰산기가 킬레이트 관능기로 도입되어 있어 보다 친수성을 강화시킨 구조를 이루고 있고, 술폰산 관능기 주위에는 산소 또는 질소 원자의 비공유 전자쌍들을 한층 풍부하게 해줌으로써 특정 중금속이온들에 대한 흡착특성이 우수한 특정 중금속이온 흡착용 술폰산기 함유 킬레이트 수지에 관한 것이다.
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公开(公告)号：KR1020050024759A
公开(公告)日：2005-03-11
申请号：KR1020030060864
申请日：2003-09-01
Applicant: 한국화학연구원 , 에이케이켐텍 주식회사
IPC: C08G61/02
Abstract: PURPOSE: Provided is a phosphorylated poly(styrene-co-divinylbenzene)-based chelate resin which is excellent in chelate adsorption power to a certain heavy metal ion, and a preparing method thereof. CONSTITUTION: The phosphorylated poly(styrene-co-divinylbenzene)-based chelate resin is represented by the formula 1, wherein a spacer of an ethylene benzyl sulfone linkage structure is introduced onto a phenyl ring, and successively, a phosphono functional group is introduced thereonto, and is prepared by the method comprising the steps of: reacting a phenyl ring in a spherical copolymer resin of styrene and divinylbenzene, with chloromethyl, followed by thiolating with thiourea/aqueous alkali solution to prepare a thiol group-containing copolymer resin of the formula 2; reacting the obtained copolymer resin with chloroethanol to convert into a hydroxyethyl benzyl thioether group, followed by chlorination to prepare a chloroethyl benzyl thioether linkage structure-containing copolymer resin of the formula 3; and reacting the obtained copolymer resin with triethylphosphite/aqueous alkali solution. In the formula 1-3, A represents a hydrogen atom or an alkali metal atom.
Abstract translation: 目的：提供对某种重金属离子的螯合吸附力优异的磷酸化聚（苯乙烯 - 共 - 二乙烯基苯）螯合树脂及其制备方法。 构成：磷酸化聚（苯乙烯 - 共 - 二乙烯基苯）螯合树脂由式1表示，其中将乙烯苄基砜键合结构的间隔基引入苯环上，然后将膦酰基官能团引入其上 并且通过包括以下步骤的方法制备：使苯基苯乙烯和二乙烯基苯的球形共聚物树脂中的苯环与氯甲基反应，然后与硫脲/碱性水溶液硫醇化，制备含硫醇基的共聚物树脂，式 2; 使得到的共聚物树脂与氯乙醇反应，转化为羟乙基苄基硫醚基，然后氯化制备含有式3的含氯乙基苄基硫醚键合结构的共聚物树脂; 并使得到的共聚物树脂与亚磷酸三乙酯/碱性水溶液反应。 在式1-3中，A表示氢原子或碱金属原子。
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公开(公告)号：KR1020040003581A
公开(公告)日：2004-01-13
申请号：KR1020020038325
申请日：2002-07-03
IPC: C11D3/26
Abstract: PURPOSE: A composition for removing a poster is provided, to improve the film strength of a paper poster and the permeation of the composition, thereby allowing the poster to be removed cleanly and easily. CONSTITUTION: The composition comprises 3-20 wt% of an aqueous polymer bonded with carboxyl groups or amide groups; 1-15 wt% of a paper penetrating agent selected from silicates, phosphates, caustic soda and acetic acid solution; 0.5-30 wt% of a permeation adjuvant selected from an alcohol and a surfactant; and 35-95.5 wt% of water. Preferably the aqueous polymer is a copolymer of dicarboxylic acid-based monomers selected from maleic anhydride, succinic acid, fumaric acid and itaconic acid, and acrylic acid, methacrylic acid or acrylamide; and the surfactant is a nonionic surfactant whose HLB (hydrophilic lipophilic balance) value is 9-18.
Abstract translation: 目的：提供用于去除海报的组合物，以提高纸张海报的膜强度和组合物的渗透性，从而允许海报被干净且容易地清除。 构成：组合物包含3-20重量％的与羧基或酰胺基键合的水性聚合物; 1-15重量％的选自硅酸盐，磷酸盐，苛性钠和乙酸溶液的纸张渗透剂; 0.5-30重量％的选自醇和表面活性剂的渗透助剂; 和35-95.5重量％的水。 优选地，水性聚合物是选自马来酸酐，琥珀酸，富马酸和衣康酸的二羧酸系单体和丙烯酸，甲基丙烯酸或丙烯酰胺的共聚物; 表面活性剂是HLB（亲水亲油平衡）值为9-18的非离子表面活性剂。
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