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公开(公告)号:KR100902414B1
公开(公告)日:2009-06-11
申请号:KR1020070132507
申请日:2007-12-17
Applicant: 한국화학연구원
IPC: C09K11/55
Abstract: A barium-magnesium phosphate-based phosphor is provided to ensure high brightness under 200~400 nm excitation and good chromatic purity, and to be useful for an emitting device for the ultraviolet excitation light emitting diode. A method for manufacturing a barium-magnesium phosphate-based phosphor comprises the steps of: manufacturing a mixture by weighting a barium precursor, magnesium precursor, phosphoric acid precursor, manganese precursor and europium precursor in a range represented by formula 1: Ba_(1-x)Mg_(1-y)P_2O_7:xEu, yMn; drying the mixture at 100~150 °C; oxidizing and heat-treating the dried mixture at 800~1100 °C; and pulverizing the mixture, then reducing and heat-treating the mixture at 800~1100 °C in a reducing atmosphere of 1~20 volume % hydrogen. In the chemical formula 1, 0
Abstract translation: 提供了一种磷酸钡镁磷光体,以确保在200〜400nm激发下的高亮度和良好的色纯度,并且可用于紫外激发发光二极管的发射装置。 一种制造磷酸钡镁的荧光体的方法包括以下步骤:通过在由式1表示的范围内加权钡前体,镁前体,磷酸前体,锰前体和铕前体制备混合物:Ba(1- x)Mg_(1-y)P_2O_7:xEu,yMn; 在100〜150℃下干燥混合物; 在800〜1100℃下对干燥的混合物进行氧化和热处理; 粉碎混合物,然后在1〜20体积%氢气的还原气氛中,在800〜1100℃下还原和热处理该混合物。 在化学式1中,0