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公开(公告)号:KR100427260B1
公开(公告)日:2004-04-17
申请号:KR1020010030713
申请日:2001-06-01
Applicant: 한국화학연구원
IPC: C01B33/12
Abstract: PURPOSE: A preparation method of micron-size silica is provided which is economical by controlling particle size distribution and shape of silica and using an ordinary crusher such as ball mill or vibration mill. CONSTITUTION: The preparation method of micron-size silica is characterized in that silica particles are wet crushed under the existence of a water system medium using a crushing medium selected from balls, rods and pebbles, wherein the silica particle, water system medium and crushing medium are contained in a volume ratio of 20 to 40 : 20 to 40 : 40 to 80 vol.%, the silica particles are synthesized in a wet process and has a moisture content of 60 to 80 wt.% and an average particle diameter of 300 to 340 micrometers, the water system medium is one or more mediums selected from water, alcohols and mineral oil, the balls are alumina balls having a diameter of 5 to 10 mm, the wet crushing treatment is performed under the conditions that crushing time is 0.5 to 3 hours, rotation speed of the ball mill is 60 revolutions per minute, and vibration number of the vibration mill is 1000 vibrations per minute, and the micron-size silica prepared by the preparation method has a maximum particle diameter less than 100 micrometers and an average particle diameter of 0.8 to 12.8 micrometers.
Abstract translation: 目的:通过控制二氧化硅的粒度分布和形状以及使用普通的破碎机如球磨机或振动磨机来提供经济的微米级二氧化硅的制备方法。 构成:微米级二氧化硅的制备方法,其特征在于,使用选自球,棒和卵石的粉碎介质,在水系介质存在下湿法粉碎二氧化硅颗粒,其中二氧化硅颗粒,水系介质和粉碎介质 以体积比20〜40:20〜40:40〜80体积%的比例含有时,二氧化硅粒子以湿式法合成,水分量为60〜80重量%,平均粒径为300 水系介质为选自水,醇类和矿物油中的1种以上的介质,球为直径5〜10mm的氧化铝球,湿式粉碎处理在粉碎时间为0.5 至3小时,球磨机的转速为60转/分钟,振动磨机的振动次数为1000次/分钟,并且通过制备方法制备的微米级二氧化硅具有最大颗粒 直径小于100微米,平均粒径为0.8至12.8微米。
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公开(公告)号:KR1020020091906A
公开(公告)日:2002-12-11
申请号:KR1020010030713
申请日:2001-06-01
Applicant: 한국화학연구원
IPC: C01B33/12
CPC classification number: C01B33/18 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62
Abstract: PURPOSE: A preparation method of micron-size silica is provided which is economical by controlling particle size distribution and shape of silica and using an ordinary crusher such as ball mill or vibration mill. CONSTITUTION: The preparation method of micron-size silica is characterized in that silica particles are wet crushed under the existence of a water system medium using a crushing medium selected from balls, rods and pebbles, wherein the silica particle, water system medium and crushing medium are contained in a volume ratio of 20 to 40 : 20 to 40 : 40 to 80 vol.%, the silica particles are synthesized in a wet process and has a moisture content of 60 to 80 wt.% and an average particle diameter of 300 to 340 micrometers, the water system medium is one or more mediums selected from water, alcohols and mineral oil, the balls are alumina balls having a diameter of 5 to 10 mm, the wet crushing treatment is performed under the conditions that crushing time is 0.5 to 3 hours, rotation speed of the ball mill is 60 revolutions per minute, and vibration number of the vibration mill is 1000 vibrations per minute, and the micron-size silica prepared by the preparation method has a maximum particle diameter less than 100 micrometers and an average particle diameter of 0.8 to 12.8 micrometers.
Abstract translation: 目的:提供微米级二氧化硅的制备方法,通过控制二氧化硅的粒度分布和形状,并使用普通的破碎机如球磨机或振动磨,是经济的。 构成:微米级二氧化硅的制备方法的特征在于,使用选自球,棒和鹅卵石的破碎介质,在水系介质存在下将二氧化硅颗粒湿法压碎,其中二氧化硅颗粒,水系介质和破碎介质 的体积比为20〜40:20〜40:40〜80体积%,二氧化硅粒子以湿法合成,水分含量为60〜80重量%,平均粒径为300 至340微米,水系介质为选自水,醇和矿物油的一种或多种介质,球为直径为5至10mm的氧化铝球,在破碎时间为0.5的条件下进行湿式破碎处理 至3小时,球磨机的转速为60转/分钟,振动磨的振动次数为每分钟1000次振动,通过制备方法制备的微米级二氧化硅具有最大粒子 直径小于100微米,平均粒径为0.8至12.8微米。
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公开(公告)号:KR1019950017837A
公开(公告)日:1995-07-20
申请号:KR1019930026918
申请日:1993-12-08
Applicant: 한국화학연구원
IPC: C04B35/18
Abstract: 본발명은 고순도 초미립 알루미나의 제조방법에 관한 것으로서, 더욱 상세하게는 나트륨 성분을 함유한 수산화알루미늄에 규석분을 첨가하여 소성하고 소성물중 나트륨 흡착 규석분을 체분리하고 염산수용액 분위기 하에서 세정분쇄함으로써 알루미나중 나트륨 성분의 함량이 적고 순도가 높아서 내연기관의 점화전 등의 전자부품의 절연재료의 원료로 사용되는 고순도 초미립 알루미나의 제조 방법에 관한 것이다.
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公开(公告)号:KR1020000008357A
公开(公告)日:2000-02-07
申请号:KR1019980028142
申请日:1998-07-13
Applicant: 한국화학연구원
IPC: C09J103/12 , C09J11/04
CPC classification number: C09J103/02
Abstract: PURPOSE: A multi-wall paper manufactured by mixing starch, clay, silica sol with water is provided which improves the strength degradation of reclaimed corrugated board. CONSTITUTION: A mixture of 3-3.8 weight% of starch, 0.1-0.5 weight% of clay with a particle of 0.1-2 micro meter, 0.1-0.5 weight% of silica sol with a particle of 3-200 nanometers is stirred with 95.2-96.8 weight% of water uniformly to give a slurry adhesive, which is sprayed on the layer of a multi-wall paper with a thickness of 1-4 g/square meter, pressed with the pressure of 2-8 kg/square meter for 1-4 min, and dried at 90-150°C to give a multi-wall paper. Corn, potato and tapioca starch can be used as an organic adhesive ingredient, but corn starch is preferable in the economic and efficiency aspect. The compound improves the adhesive strength of interlayer of the multi-wall paper, the bursting strength and the compressed strength compared with a conventional single spraying process of non-gelatinized starch.
Abstract translation: 目的:提供将淀粉,粘土,硅溶胶与水混合制成的多壁纸,改善了再生瓦楞纸板的强度退化。 构成:将3-3.8重量%的淀粉,0.1-0.5重量%的粘土,0.1-2微米的颗粒,0.1-0.5重量%的具有3-200纳米颗粒的硅溶胶的混合物与95.2 -96.8重量%的水均匀,得到浆料粘合剂,喷涂在厚度为1-4克/平方米的多层纸层上,压力为2-8公斤/平方米, 1-4分钟,并在90-150℃下干燥,得到多壁纸。 玉米,马铃薯和木薯淀粉可以用作有机粘合剂成分,但在经济和效率方面优选玉米淀粉。 与常规的非糊化淀粉单喷雾方法相比,该复合物提高了多壁纸的中间层的粘合强度,破裂强度和压缩强度。
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公开(公告)号:KR1020110050175A
公开(公告)日:2011-05-13
申请号:KR1020090107041
申请日:2009-11-06
Applicant: 한국화학연구원 , 에이비씨나노텍 주식회사
CPC classification number: C09D11/52 , C08K5/07 , C08K5/16 , C09D11/30 , H01B1/22 , H05K1/00 , H05K3/00
Abstract: PURPOSE: An ink composition for forming circuits is provided to ensure excellent dispersion stability, to perform thermal process at a low temperature, and to easily form electrode wiring patterns. CONSTITUTION: An ink composition for forming circuits comprises a copper-glycine composite of chemical formula 1. In chemical formula 1, M is Cu, R1 and R2 are different or the same and represent C3-C7 linear or branched alkyl group in which one or more halogens are substituted or unsubstituted. A method for forming copper circuits comprises the steps of: applying the ink composition for copper circuits to a material; and heat-treating the ink composition to form copper nanoparticle circuits from the copper-glycine composite.
Abstract translation: 目的:提供用于形成电路的油墨组合物,以确保优异的分散稳定性,在低温下进行热处理,并容易地形成电极布线图案。 构成:用于形成电路的油墨组合物包括化学式1的铜 - 甘氨酸复合物。在化学式1中,M是Cu,R 1和R 2是不同的或相同的,代表C 3 -C 7直链或支链烷基,其中一个或 更多的卤素是取代或未取代的。 一种形成铜电路的方法包括以下步骤:将铜电路用油墨组合物施加到材料上; 并对该油墨组合物进行热处理以从铜 - 甘氨酸复合物形成铜纳米颗粒回路。
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公开(公告)号:KR100332214B1
公开(公告)日:2002-04-12
申请号:KR1019990020004
申请日:1999-06-01
Applicant: 한국화학연구원
Abstract: 본발명은제지의보류및 탈수향상제에관한것으로서, 더욱상세하게는제지생산공정에서적용되는보류및 탈수향상제를제조함에있어음이온성폴리실리식산을무기원료로하고양이온성폴리아크릴아미드를유기원료로하여혼성(hybrid)결합시켜제조함으로써, 지료중에함유되어있는미세분의보류를증가시키고지료중의물을용이하게제거하여제지생산공정의경제성과생산성을크게향상시킬수 있는제지의보류및 탈수향상제에관한것이다.
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公开(公告)号:KR100142923B1
公开(公告)日:1998-07-15
申请号:KR1019940016708
申请日:1994-07-12
Applicant: 한국화학연구원
Abstract: 본 발명은 제지용 피치 콘트롤제(Pitch Controlling Agent)와 그의 제조방법에 관한 것으로서, 더욱 상세하게는 활석광물을 건식 미분쇄처리하여 얻은 활석분체의 입자표면을 물로 세정하고 염산으로 1차 개질처리한 다음 보류향상제 또는 분산제 등으로 2차 개질처리하여 제조됨으로써, 피치 제거효과가 높은 새로운 제지용 피치 콘트롤제와 그의 제조방법에 관한 것이다.
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公开(公告)号:KR1019960006232B1
公开(公告)日:1996-05-11
申请号:KR1019930026918
申请日:1993-12-08
Applicant: 한국화학연구원
IPC: C04B35/18
Abstract: The high purity and ultrafine alumina is prepared by (a) mixing sodium-containing aluminum hydroxide with nature silica stone powder and firing, (b) separating sodium-adsorbed silica stone powder with sieving, (c) milling the separated powder in the wet ball mill and 5% hydrochloric acid solution to remove sodium on the surface of alumina and to diminish the particle size of alumina up to 1 micrometer.
Abstract translation: 高纯度和超细氧化铝的制备方法是:(a)将含有氢氧化铝的氢氧化钠与天然石英石粉混合并焙烧,(b)用筛分法分离吸附的二氧化硅石粉,(c)在湿球中研磨分离的粉末 研磨和5%盐酸溶液以除去氧化铝表面上的钠,并将氧化铝的粒径降低至1微米。
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公开(公告)号:KR101055625B1
公开(公告)日:2011-08-10
申请号:KR1020090107041
申请日:2009-11-06
Applicant: 한국화학연구원 , 에이비씨나노텍 주식회사
Abstract: 본 발명은 하기 화학식 1의 구리-글리신 복합물을 포함하는 배선용 잉크 조성물과 이를 기재에 인쇄한 후 열처리하여 구리배선을 형성시키는 방법에 관한 것이다.
[화학식 1]
[상기 화학식 1에서, M은 Cu이고, R
1 및 R
2 는 서로 상이하거나 동일할 수 있으며, 할로겐이 하나 이상 치환되거나 치환되지 않은 C3-C7의 선형 또는 분지형의 알킬기이다.]
본 발명에 따른 배선용 잉크 조성물은 종래의 금속 나노입자를 계면활성제 또는 덮개리간드와 함께 분산용매에 분산시키는 잉크 조성물보다 분산 안정성이 우수한 장점이 있다. 또한 낮은 온도에서 열처리 공정을 수행할 수 있는 장점이 있으며, 잉크젯 인쇄방법에 적합하여 전극배선 패턴을 용이하게 형성할 수 있다.
배선용 잉크, 구리 화합물, 구리 복합물, 잉크젯 프린팅, 도전성 잉크, 구리 전구체, 전극 배선 패턴, RFID
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