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公开(公告)号:US12098314B2
公开(公告)日:2024-09-24
申请号:US15733469
申请日:2019-02-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Shantanu R. Ranade , Alexander J. Kugel , Kai U. Claussen , Rachna Khurana , Dean M. Moren , William H. Sikorski, Jr. , Erik M. Townsend
IPC: C09J7/50 , C09D183/02 , C09J5/04 , C09J7/20 , C09J7/30 , C09J7/35 , C08K3/10 , C08K5/14 , C08K5/1535
CPC classification number: C09J7/50 , C09D183/02 , C09J5/04 , C09J7/20 , C09J7/30 , C09J7/35 , C08K3/10 , C08K5/14 , C08K5/1535 , C09J2301/408 , C09J2301/416
Abstract: Curable adhesive films, primers for adhesion of curable adhesive films, and adhesive systems comprising adhesive films and primers are provided. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising a blend of: a) a first film-forming polymer or oligomer; b) a first species comprising first unsaturated free-radically polymerizable groups, which may be a) or a species other than a); and c) a first transition metal cation; and II) a primer for adhesion of a curable adhesive free-standing film to a first substrate comprising an oxidizing agent. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising an outer surface bearing embossed air bleed channels capable of aiding in escape of air during application of the outer surface to a primed substrate; and II) a primer comprising components that initiate cure of the curable adhesive free-standing film.
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公开(公告)号:US20240400865A1
公开(公告)日:2024-12-05
申请号:US18698451
申请日:2022-08-18
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Amanda K. Leone , Bryan T. Whiting , Kai U. Claussen , William H. Moser
IPC: C09J4/00 , B32B37/12 , C08F220/18 , C08F220/28 , C09J5/00 , C09J133/08 , C09J133/14
Abstract: A photopolymerizable composition comprises at least one free-radically polymerizable compound; at least one organic photoactivatable reducing agent precursor; at least one reducible transition metal compound comprising at least one of cobalt, copper, iron, manganese, nickel, or vanadium; at least one organic peroxide; and at least one photoinitiator. The at least one photoinitiator does not comprise an organic peroxide. Methods of bonding and sealing, and an at least partially polymerized composition are also disclosed.
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公开(公告)号:US20210102097A1
公开(公告)日:2021-04-08
申请号:US15733470
申请日:2019-02-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Shantanu R. Ranade , Alexander J. Kugel , Kai U. Claussen , Rachna Khurana , Dean M. Moren , William H. Sikorski, Jr. , Erik M. Townsend
Abstract: Curable adhesive films, primers for adhesion of curable adhesive films, and adhesive systems comprising adhesive films and primers are provided. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising a blend of: a) a first film-forming polymer or oligomer; b) a first species comprising first unsaturated free-radically polymerizable groups, which may be a) or a species other than a); and c) a first transition metal cation; and II) a primer for adhesion of a curable adhesive free-standing film to a first substrate comprising an oxidizing agent. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising an outer surface bearing embossed air bleed channels capable of aiding in escape of air during application of the outer surface to a primed substrate; and II) a primer comprising components that initiate cure of the curable adhesive free-standing film.
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4.
公开(公告)号:US20190046419A1
公开(公告)日:2019-02-14
申请号:US16078069
申请日:2017-02-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kai U. Claussen , Johannes M. Leykauff , Christine Lienau , Reinhold Hecht , Peter Braun , Markus Mikulla
Abstract: The invention relates to a kit of parts for preparing a glass ionomer composition for dental use, the kit comprising a Paste A and a Paste B, Paste A comprising water, acid-reactive inorganic filler A, phyllo silicate(s), Paste B comprising water, poly-acid, non acid-reactive filler B, optionally chelating agent. The invention also relates to a hardenable composition obtainable by combining the pastes of the kit or parts and to the use of such a composition as or for preparing a dental cement, dental filling mater ial, dental core build up material or dental root channel filling material.
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公开(公告)号:US12163070B2
公开(公告)日:2024-12-10
申请号:US15733470
申请日:2019-02-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Shantanu R. Ranade , Alexander J. Kugel , Kai U. Claussen , Rachna Khurana , Dean M. Moren , William H. Sikorski, Jr. , Erik M. Townsend
IPC: C09J7/50 , C08K3/10 , C08K5/14 , C08K5/1535 , C09D183/02 , C09J5/04 , C09J7/20 , C09J7/30 , C09J7/35
Abstract: Curable adhesive films, primers for adhesion of curable adhesive films, and adhesive systems comprising adhesive films and primers are provided. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising a blend of: a) a first film-forming polymer or oligomer; b) a first species comprising first unsaturated free-radically polymerizable groups, which may be a) or a species other than a); and c) a first transition metal cation; and II) a primer for adhesion of a curable adhesive free-standing film to a first substrate comprising an oxidizing agent. In some embodiments, an adhesive system comprises: I) a curable adhesive free-standing film comprising an outer surface bearing embossed air bleed channels capable of aiding in escape of air during application of the outer surface to a primed substrate; and II) a primer comprising components that initiate cure of the curable adhesive free-standing film.
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公开(公告)号:US20230404859A1
公开(公告)日:2023-12-21
申请号:US18037642
申请日:2021-11-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kai U. Claussen , Hassan Sahouani , Silke D. Mechernich
Abstract: The invention relates to a dental composition comprising a polymerizable component not comprising an acidic moiety, and microcapsules comprising a first component of a non water-soluble redox-initiator system, and a pH-sensitive inorganic component, the microcapsules not comprising a polymeric material. The invention also relates to the use of certain microcapsules for preparing a curable dental composition and to a process of curing a dental composition, as well as a device for storing the dental composition.
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公开(公告)号:US20210102095A1
公开(公告)日:2021-04-08
申请号:US15733471
申请日:2019-02-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Shantanu R. Ranade , Alexander J. Kugel , Kai U. Claussen , Rachna Khurana , Dean M. Moren , William H. Sikorski, JR. , Erik M. Townsend
Abstract: Curable adhesive free-standing films and adhesive systems comprising such films are provided. In some embodiments, a curable adhesive free-standing film comprises a blend of: a) a first film-forming polymer or oligomer; b) a first species comprising first unsaturated free-radically polymerizable groups, which may be a) or a species other than a); c) a first transition metal cation; d) a reducing agent; and no oxidizing agent. In some embodiments, an adhesive system comprises: I) a first curable adhesive free-standing film as described preceding; and II) a second curable adhesive free-standing film comprising a blend of: e) a second film-forming polymer or oligomer; f) a second species comprising second unsaturated free-radically polymerizable groups, which may be e) or may be a species other than e); and g) an oxidizing agent. In some embodiments, the curable adhesive free-standing films may be pressure sensitive adhesives prior to cure. Methods of use are provided.
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8.
公开(公告)号:US10799429B2
公开(公告)日:2020-10-13
申请号:US16078069
申请日:2017-02-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kai U. Claussen , Johannes M. Leykauff , Christine Lienau , Reinhold Hecht , Peter Braun , Markus Mikulla
Abstract: The invention relates to a kit of parts for preparing a glass ionomer composition for dental use, the kit comprising a Paste A and a Paste B, Paste A comprising water, acid-reactive inorganic filler A, phyllo silicate(s), Paste B comprising water, poly-acid, non acid-reactive filler B, optionally chelating agent. The invention also relates to a hardenable composition obtainable by combining the pastes of the kit or parts and to the use of such a composition as or for preparing a dental cement, dental filling material, dental core build up material or dental root channel filling material.
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公开(公告)号:US20220211611A1
公开(公告)日:2022-07-07
申请号:US17595217
申请日:2020-05-27
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kai U. Claussen , Silke D. Mechernich , Hassan Sahouani
Abstract: The invention relates to a microcapsule comprising a hollow or porous core, the hollow or porous core being composed of a crosslinked polymeric material and containing a component to be released, a shell, the shell being composed of a polymeric material containing a component, which is able to produce gas upon exposure to acid. The microcapsule can be used for formulating dental materials.
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公开(公告)号:US20200368117A1
公开(公告)日:2020-11-26
申请号:US16967937
申请日:2019-02-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kai U. Claussen , Silke D. Mechernich , Mareike Richter , Reinhold Hecht , Manfred Ludsteck , Simone Jurjevic
IPC: A61K6/889 , A61C5/00 , A61C7/00 , A61K6/17 , C08F222/10
Abstract: The invention relates to a microcapsule comprising a hollow or porous core, the hollow or porous core being composed of a polymeric material and containing a component of a redox-initiator system, a shell, the shell being composed of a pH-sensitive material. The microcapsule can be used for formulating dental materials.
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