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公开(公告)号:US11584823B2
公开(公告)日:2023-02-21
申请号:US16467570
申请日:2017-12-05
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael A. Kropp , Matthew J. Kryger
Abstract: A curable, one-part epoxy/thiol resin composition comprising: an epoxy resin component comprising an epoxy resin having at least two epoxide groups per molecule; a thiol component comprising a polythiol compound having at least two primary thiol groups; a nitrogen-containing catalyst for the epoxy resin; and a substituted barbituric acid soluble in the one-part epoxy/thiol resin composition.
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公开(公告)号:US20210317254A1
公开(公告)日:2021-10-14
申请号:US17265023
申请日:2019-09-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kolby L. White , Joseph D. Rule , Michael A. Kropp , Matthew J. Kryger , Zachary J. Thompson , Richard B. Ross
IPC: C08G18/28 , C08G18/00 , C08G18/20 , C08G18/22 , C08G18/32 , C08G18/42 , C08G18/48 , C08G18/50 , C08G18/79 , C08G18/80 , C09D175/08 , C09J175/08 , B32B7/12 , B32B37/12
Abstract: The present disclosure provides a polymeric material including a polymerized reaction product of a polymerizable composition including components and has a solids content of 90% or greater. The components include a uretdione-containing material including a reaction product of a diisocyanate reacted with itself; a first hydroxyl-containing compound; an optional second hydroxyl-containing compound having a single OH group, wherein; and an epoxy component. The first hydroxyl-containing compound has more than one OH group and the optional second hydroxyl-containing compound is a primary alcohol or a secondary alcohol. The present disclosure also provides a two-part composition, in which the polymeric material is included in the first part and the second part includes at least one amine. Further, a method of adhering two substrates is provided, including obtaining a two-part composition; combining at least a portion of the first part with at least a portion of the second part to form a mixture; disposing at least a portion of the mixture on a first substrate; and contacting a second substrate with the mixture disposed on the first substrate. The disclosure also provides a polymeric material and a method of making a two-part composition. Advantageously, two-part compositions according to the present disclosure can be used as coatings and adhesive systems with handling and performance similar to existing two-part urethane systems, but with less sensitivity to water.
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公开(公告)号:US20250136546A1
公开(公告)日:2025-05-01
申请号:US18683434
申请日:2022-08-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Hae-Seung Harry Lee , Steven R. Austin , Matthew J. Kryger
IPC: C07C323/52 , B32B5/18 , B32B7/14 , B32B15/04 , B32B15/20 , C09J181/02
Abstract: A primer compound is provided that can be used as an adhesion promoter on various substrates, particularly metal-containing substrates. Articles containing a metal-containing substrate and a primer layer, which includes the primer compound, positioned adjacent to the substrate are also provided. The articles often include an adhesive layer with the primer layer positioned between the metal-containing substrate and the adhesive layer. The primer compound has a diketone group that can form chelates with various metals through coordination chemistry plus a thiol group that can react with components in the adhesive layer.
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公开(公告)号:US11988304B2
公开(公告)日:2024-05-21
申请号:US17280026
申请日:2019-09-23
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Matthew J. Kryger
CPC classification number: F16L13/103 , C09J5/06 , F16L13/11
Abstract: Apparatus and method for joining two tubular elements (14, 22) at a joint using an adhesive that is non-flowable at ambient temperatures but flowable at an elevated temperature. A ring (12) of uncured, non-flowable adhesive is placed around the male end of a male (14)/female (22) pipe interface. Upon exposure to elevated temperatures, the ring (12) melts and flows down into the interface, and cures.
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公开(公告)号:US20240124639A1
公开(公告)日:2024-04-18
申请号:US18264594
申请日:2022-02-07
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kolby L. White , Gregory P. Sorenson , Matthew J. Kryger
IPC: C08F283/10 , C09J151/08
CPC classification number: C08F283/10 , C09J151/08
Abstract: A two-part curable composition is provided that includes a first part that includes an oxamido-containing compound and a second part that includes an epoxy resin. The oxamido-containing compound includes at least one first segment derived from a first polyamine and at least one second segment derived from a second polyamine that is different than the first polyamine. The oxamido-containing compound has at least two amino (—NH2) groups that can react with the epoxy resin in the second part of the curable composition. Each part of the curable composition is flowable, often at room temperature or slightly above room temperature, and can be mixed to form a cured composition having structural bonding performance.
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公开(公告)号:US20240117221A1
公开(公告)日:2024-04-11
申请号:US18257312
申请日:2021-12-15
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Matthew J. Kryger , Chase M. O'Brien , Dennis C. Ngo , Eric R. Amann
IPC: C09J5/00 , C09J11/04 , C09J163/00
CPC classification number: C09J5/00 , C09J11/04 , C09J163/00 , C09J2463/00
Abstract: Methods of bonding a male element and a female element, the method including applying an adhesive composition to at least the male element, the male element including a first metal; inserting at least a portion of the male element into the female element thereby forming an external interface between the male element and the female element, the female element including a second metal; and curing the adhesive composition to form an adhesive bond between the male element and the female element, wherein the first metal and the second metal are not the same, wherein the external interface of the male element and female element is covered by the cured adhesive composition and the adhesive composition covering the external interface of the male element and female element limits corrosion of at least a portion of the male element, the female element, or both.
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公开(公告)号:US11655327B2
公开(公告)日:2023-05-23
申请号:US17265023
申请日:2019-09-16
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kolby L. White , Joseph D. Rule , Michael A. Kropp , Matthew J. Kryger , Zachary J. Thompson , Richard B. Ross
IPC: C08G18/28 , B32B7/12 , B32B37/12 , C08G18/00 , C08G18/20 , C08G18/32 , C08G18/42 , C08G18/48 , C08G18/50 , C08G18/79 , C08G18/80 , C09D175/08 , C09J175/08 , C08G18/22
CPC classification number: C08G18/2825 , B32B7/12 , B32B37/12 , C08G18/003 , C08G18/2063 , C08G18/227 , C08G18/325 , C08G18/3228 , C08G18/3234 , C08G18/4238 , C08G18/4808 , C08G18/4854 , C08G18/5024 , C08G18/798 , C08G18/8016 , C08G18/8064 , C09D175/08 , C09J175/08 , B32B2037/1269 , C08G2170/90
Abstract: The present disclosure provides a polymeric material including a polymerized reaction product of a polymerizable composition including components and has a solids content of 90% or greater. The components include a uretdione-containing material including a reaction product of a diisocyanate reacted with itself; a first hydroxyl-containing compound; an optional second hydroxyl-containing compound having a single OH group, wherein; and an epoxy component. The first hydroxyl-containing compound has more than one OH group and the optional second hydroxyl-containing compound is a primary alcohol or a secondary alcohol. The present disclosure also provides a two-part composition, in which the polymeric material is included in the first part and the second part includes at least one amine. Further, a method of adhering two substrates is provided, including obtaining a two-part composition; combining at least a portion of the first part with at least a portion of the second part to form a mixture; disposing at least a portion of the mixture on a first substrate; and contacting a second substrate with the mixture disposed on the first substrate. The disclosure also provides a polymeric material and a method of making a two-part composition. Advantageously, two-part compositions according to the present disclosure can be used as coatings and adhesive systems with handling and performance similar to existing two-part urethane systems, but with less sensitivity to water.
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公开(公告)号:US12018114B2
公开(公告)日:2024-06-25
申请号:US17265049
申请日:2019-09-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Kolby L. White , Matthew J. Kryger , Joseph D. Rule , Michael A Kropp , Adrian T. Jung
IPC: C08G18/22 , B32B7/12 , B32B37/12 , C08G18/28 , C08G18/32 , C08G18/42 , C08G18/48 , C08G18/50 , C08G18/78 , C08G18/79 , C08G18/80 , C08G59/40 , C08G59/50 , C09D175/12 , C09J175/12
CPC classification number: C08G18/227 , B32B7/12 , B32B37/12 , C08G18/2825 , C08G18/3206 , C08G18/3218 , C08G18/3253 , C08G18/4238 , C08G18/4854 , C08G18/5024 , C08G18/7831 , C08G18/798 , C08G18/8038 , C08G59/4021 , C08G59/5013 , C09D175/12 , C09J175/12 , B32B2037/1269 , C08G2190/00
Abstract: The present disclosure provides a polymeric material including a polymerized reaction product of a polymerizable composition including components, and a thermally activatable amine curative, and has a solids content of 90% or greater. The components include a uretdione-containing material including a reaction product of a diisocyanate reacted with itself; a first hydroxyl-containing compound; and an optional second hydroxyl-containing compound having a single OH group. The first hydroxyl-containing compound has more than one OH group and the optional second hydroxyl-containing compound is a primary alcohol or a secondary alcohol. The present disclosure also provides a two-part composition, in which a polymeric material is included in the first part and the second part includes at least one liquid amine. Further, a method of adhering two substrates is provided, including obtaining a two-part composition; combining at least a portion of the first part with at least a portion of the second part to form a mixture; disposing at least a portion of the mixture on a first substrate; and contacting a second substrate with the mixture disposed on the first substrate. The disclosure also provides a polymeric material and a method of curing a two-part composition. Advantageously, two-part compositions according to the present disclosure can be used as coatings and adhesive systems having a two-step cure with handling and performance similar to existing two-part urethane systems, but with less sensitivity to water.
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公开(公告)号:US20220162376A1
公开(公告)日:2022-05-26
申请号:US17440976
申请日:2019-03-25
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Li Yao , Michael A. Kropp , Matthew J. Kryger , Wayne S. Mahoney , Mario A. Perez , Shuang Wu , Lingjie Tong , Ahmad Shaaban , Adrian T. Jung , Jeremy M. Higgins , Ying Lin
IPC: C08G59/66 , C08G59/24 , C08K5/37 , C08K3/22 , C08K7/18 , C08K9/06 , C09J163/00 , H01M50/233 , H01M10/653
Abstract: A curable composition includes a first part comprising an epoxy resin; and a second part comprising a multifunctional, functional thiol containing compound. The curable composition further includes an inorganic filler present in an amount of at least 20 weight %, based on the total weight of the curable composition. The multifunctional, functional thiol containing compound comprises an ether in the backbone thereof.
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公开(公告)号:US20210403634A1
公开(公告)日:2021-12-30
申请号:US16467570
申请日:2017-12-05
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Michael A. Kropp , Matthew J. Kryger
Abstract: A curable, one-part epoxy/thiol resin composition comprising: an epoxy resin component comprising an epoxy resin having at least two epoxide groups per molecule; a thiol component comprising a polythiol compound having at least two primary thiol groups; a nitrogen-containing catalyst for the epoxy resin; and a substituted barbituric acid soluble in the one-part epoxy/thiol resin composition.
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