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1.发明申请公开(公告)号：US20160033470A1
公开(公告)日：2016-02-04
申请号：US14851281
申请日：2015-09-11
Inventor： Wayne F. Reed
CPC classification number: G01N33/442 , B01J19/0006 , B01J19/0033 , B01J2219/00063 , B01J2219/00177 , B01J2219/00186 , B01J2219/002 , C08F2/001 , G01N1/32 , G01N21/05 , G01N21/253 , G01N21/47 , G01N21/49 , G01N21/53 , G01N21/64 , G01N21/82 , G01N33/44 , G01N2021/054 , G01N2021/4742 , G01N2021/4769 , G01N2021/8411 , Y02P20/582
Abstract: A method of monitoring the evolution of polymer and/or colloid stimuli responsiveness during synthesis of polymers and/or colloids, including postpolymerization modifications on natural and synthetic polymers, includes providing a reactor in which the polymers and/or colloids are synthesized; and providing a means of monitoring the stimuli responsiveness of the polymers and/or colloids during said synthesis. Preferably, the method also includes monitoring the evolution of the characteristics of the polymers and/or colloids during said synthesis. Preferably, evolution of polymer and/or colloid stimuli responsiveness is correlated to the evolution of the properties of the polymers and/or colloids themselves. Also, preferably the conditions of the fluid in the reactor in which the synthesis occurs is determined. The determination can be by detection, choice of materials and temperature conditions, for example, and combinations thereof. The method and instrumentation disclosed can lead to optimization and control of processes and synthetic and modification strategies leading to polymers and colloids with desired stimuli responsiveness.
Abstract translation: 监测合成聚合物和/或胶体期间聚合物和/或胶体刺激响应性的方法，包括天然和合成聚合物的后聚合改性，包括提供其中合成聚合物和/或胶体的反应器; 并且提供在所述合成期间监测聚合物和/或胶体的刺激响应性的手段。 优选地，该方法还包括在所述合成期间监测聚合物和/或胶体的特性的演变。 优选地，聚合物和/或胶体刺激反应性的演变与聚合物和/或胶体本身的性质的演变相关。 此外，优选确定发生合成的反应器中的流体的条件。 该测定可以通过检测，材料的选择和温度条件，例如及其组合。 所公开的方法和仪器可以导致优化和控制过程和合成和修饰策略，导致具有期望的刺激反应性的聚合物和胶体。
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公开(公告)号：US11835500B2
公开(公告)日：2023-12-05
申请号：US15518658
申请日：2015-10-13
Inventor： Wayne F. Reed
IPC: C08F2/00 , B01J19/24 , B01J19/00 , B01F33/81 , B01F33/80 , G01N30/78 , B01J4/00 , B01F35/21 , B01F35/71 , C12M1/34 , G01N1/38 , G01N15/02 , G01N15/00
CPC classification number: G01N30/78 , B01F33/811 , B01F35/2132 , B01F35/2133 , B01F35/7176 , B01J4/00 , B01J19/0093 , B01J19/245 , C12M1/34 , B01D2313/08 , B01F33/834 , B01J2219/00813 , B01J2219/00867 , B01J2219/00871 , B01J2219/00889 , B01J2219/00894 , B01J2219/00952 , B01J2219/00968 , B01J2219/00997 , G01N1/38 , G01N15/02 , G01N2015/0092
Abstract: Disclosed herein is a device and method for changing the conditions of a solution flowing in a serial path. In particular, disclosed herein is a device that includes a chemical reactor, a first system, and a second system that are each serial to one another. Each of the first system and the second system include a mixing chamber, a solvent reservoir, a solvent pump, and one or more detectors. Also disclosed herein is a method for changing the condition of a solution that includes flowing a liquid sample in a path, serially mixing the sample with at least two discrete solvents while it flows through the path, and detecting the condition of the sample after it is mixed with each solvent.
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公开(公告)号：US20170234842A1
公开(公告)日：2017-08-17
申请号：US15518658
申请日：2015-10-13
Inventor： Wayne F. Reed
CPC classification number: G01N30/78 , B01D2313/08 , B01F13/1016 , B01F15/0022 , B01F15/00227 , B01F15/0243 , B01F2013/1052 , B01J4/00 , B01J19/0093 , B01J19/245 , B01J2219/00813 , B01J2219/00867 , B01J2219/00871 , B01J2219/00889 , B01J2219/00894 , B01J2219/00952 , B01J2219/00968 , B01J2219/00997 , C12M1/34 , G01N1/38 , G01N15/02 , G01N2015/0092
Abstract: Disclosed herein is a device and method for changing the conditions of a solution flowing in a serial path. In particular, disclosed herein is a device that includes a chemical reactor, a first system, and a second system that are each serial to one another. Each of the first system and the second system include a mixing chamber, a solvent reservoir, a solvent pump, and one or more detectors. Also disclosed herein is a method for changing the condition of a solution that includes flowing a liquid sample in a path, serially mixing the sample with at least two discrete solvents while it flows through the path, and detecting the condition of the sample after it is mixed with each solvent.
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4.发明授权公开(公告)号：US09568462B2
公开(公告)日：2017-02-14
申请号：US14851281
申请日：2015-09-11
Inventor： Wayne F. Reed
IPC: C08F2/00 , A61L2/28 , G01N33/00 , C40B30/10 , G01N33/44 , B01J19/00 , G01N21/25 , G01N21/53 , G01N21/82 , G01N1/32 , G01N21/05 , G01N21/64 , G01N21/47 , G01N21/84
CPC classification number: G01N33/442 , B01J19/0006 , B01J19/0033 , B01J2219/00063 , B01J2219/00177 , B01J2219/00186 , B01J2219/002 , C08F2/001 , G01N1/32 , G01N21/05 , G01N21/253 , G01N21/47 , G01N21/49 , G01N21/53 , G01N21/64 , G01N21/82 , G01N33/44 , G01N2021/054 , G01N2021/4742 , G01N2021/4769 , G01N2021/8411 , Y02P20/582
Abstract: A method of monitoring the evolution of polymer and/or colloid stimuli responsiveness during synthesis of polymers and/or colloids, including postpolymerization modifications on natural and synthetic polymers, includes providing a reactor in which the polymers and/or colloids are synthesized; and providing a means of monitoring the stimuli responsiveness of the polymers and/or colloids during said synthesis. Preferably, the method also includes monitoring the evolution of the characteristics of the polymers and/or colloids during said synthesis. Preferably, evolution of polymer and/or colloid stimuli responsiveness is correlated to the evolution of the properties of the polymers and/or colloids themselves. Also, preferably the conditions of the fluid in the reactor in which the synthesis occurs is determined. The determination can be by detection, choice of materials and temperature conditions, for example, and combinations thereof. The method and instrumentation disclosed can lead to optimization and control of processes and synthetic and modification strategies leading to polymers and colloids with desired stimuli responsiveness.
Abstract translation: 监测合成聚合物和/或胶体期间聚合物和/或胶体刺激响应性的方法，包括天然和合成聚合物的后聚合改性，包括提供其中合成聚合物和/或胶体的反应器; 并且提供在所述合成期间监测聚合物和/或胶体的刺激响应性的手段。 优选地，该方法还包括在所述合成期间监测聚合物和/或胶体的特性的演变。 优选地，聚合物和/或胶体刺激反应性的演变与聚合物和/或胶体本身的性质的演变相关。 此外，优选确定发生合成的反应器中的流体的条件。 该测定可以通过检测，材料的选择和温度条件，例如及其组合。 所公开的方法和仪器可以导致优化和控制过程和合成和修饰策略，导致具有期望的刺激反应性的聚合物和胶体。
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