Process for the preparation of triazine carbamates
    1.
    发明公开
    Process for the preparation of triazine carbamates 审中-公开
    Verfahren zur Herstellung von Triazincarbamaten

    公开(公告)号:EP2995613A1

    公开(公告)日:2016-03-16

    申请号:EP14184020.7

    申请日:2014-09-09

    Inventor: Flood, Lawrence

    CPC classification number: C07D251/24 C07D251/18 C07D251/54 C07D251/70

    Abstract: This invention relates to a process for the preparation of triazine carbamates by reacting a mixture of an aminotriazine A having at least two amino groups per molecule, an organic carbonate C, and a base B selected from the group consisting of alkoxides, and arylalkoxides of metals M, which may be alkali or earth alkali metals, and a solvent S which is a monohydric alcohol solvent R 2 OH or a mixture of solvents that comprises a monohydric alcohol R 2 OH, and a monohydric alcohol R 3 OH, or a mixture of solvents that comprises a monohydric alcohol R 2 OH with a further solvent selected from the group consisting of ether, alcohol, and hydrocarbon solvents, and adding to the products of the said reaction, an acid or a solution of an acid in a solvent.

    Abstract translation: 本发明涉及一种通过使每分子具有至少两个氨基的氨基三嗪A与有机碳酸酯C和碱金属B的混合物的混合物制备三嗪的方法,所述碱金属选自醇盐和金属的芳基烷氧基化物 M,其可以是碱金属或碱土金属,以及溶剂S,其是一元醇溶剂R 2 OH或包含一元醇R 2 OH和一元醇R 3 OH的溶剂混合物,或 包含一元醇R 2 OH与另外的选自醚,醇和烃溶剂的溶剂的溶剂,并将酸或溶液中的酸或酸的溶液加入到所述反应产物中。

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