1.
    发明专利
    未知

    公开(公告)号:DE2653346A1

    公开(公告)日:1978-06-01

    申请号:DE2653346

    申请日:1976-11-24

    Applicant: BASF AG

    Abstract: Pure halonaphthalic acid anhydrides are prepared from haloacenaphthenes by oxidation with nitric acid in a mixture of aliphatic carboxylic acid, water and nitric acid in the presence of vanadate, with or without further metal salts, at an elevated temperature and the reaction product is isolated and subjected to an oxidative after-treatment with hypochlorite in aqueous solution at a pH of from 9 to 12 at an elevated temperature. The products are intermediates for the manufacture of optical brighteners.

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