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公开(公告)号:DE2456961A1
公开(公告)日:1976-06-16
申请号:DE2456961
申请日:1974-12-03
Applicant: BASF AG
Inventor: EBERHARD PETER DR
IPC: C07D317/26 , C07D319/06 , C07D325/00
Abstract: Benzil monoketals of formula (I; X=CO) are prepd. by oxidising the corresp. benzoin ketals of formula (II; X=CHOH), (where R1 and R2 are H, 1-6C alkyl, 1-6C alkoxy or 2-6C alkoxyalkyl and Z is a divalent gp. of an aliphatic 2-8C diol) with DMSO in the presence of an acylating agent (III) in a polar solvent, pref. DMSO and/or DMF, at -10 to +100 degrees C. (I) are used as photo-initiators, and are obtd. in high yields, e.g. >90% of theoretical, economically, without causing pollution problems.
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公开(公告)号:DE3063972D1
公开(公告)日:1983-08-04
申请号:DE3063972
申请日:1980-07-17
Applicant: BASF AG
Inventor: HUPFER LEOPOLD DR , GRAF FRITZ DR , EBERHARD PETER DR , WICKENHAEUSER GERHARD DR , SCHLUETER LOTHAR DR
IPC: C07D233/58 , C07D233/54
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公开(公告)号:DE3061668D1
公开(公告)日:1983-02-24
申请号:DE3061668
申请日:1980-04-21
Applicant: BASF AG
Inventor: EBERHARD PETER DR , HUPFER LEOPOLD DR , GRAF FRITZ DR , SCHULTE WOLFGANG DR
IPC: C07D233/54 , C07D233/58
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