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公开(公告)号：US3787299A
公开(公告)日：1974-01-22
申请号：US3787299D
申请日：1971-03-22
Applicant: BASF AG
CPC classification number: C25B3/10
Abstract: Process for the electrochemical condensation of carboxylic acids in a solvent, in which the electrolyte is caused to flow at a rate of from 0.05 to 2 m/sec between pairs of electrodes which are impermeable to liquids and are spaced from 0.1 to 2 mm apart.
Abstract translation: 在溶剂中电化学缩合羧酸的方法，其中使电解液以对液体不渗透的电极对之间以0.05至2m / sec的速率流动并且间隔0.1至2mm。
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2.发明授权An electrocoating composition containing an acid binder present as the salt of an arylamine, alkynyl amine, quaternary ammonium hydroxide or phosphonium hydroxide 失效含有酸性粘合剂的电动组合物作为亚氨基胺的盐，烷基胺，季铵氢氧化铵或氢氧化磷
公开(公告)号：US3819548A
公开(公告)日：1974-06-25
申请号：US20470171
申请日：1971-12-03
Applicant: BASF AG
CPC classification number: C09D5/4484 , Y10S524/901
Abstract: In an electrocoating process acid binders which are present at least partly in the form of their salts with basic compounds are used and the basic compounds used for salt formation consist of the extent of 0.1 to 50 percent of the neutralization equivalent of the acid binder of at least one arylamine and/or alkynylamine and/or quaternary ammonium hydroxide and/or phosphonium hydroxide with at least one aromatic ligand, and other conventional additives and non-basic corrosion inhibitors may be contained in the aqueous solution or dispersion of the coating composition. The process is suitable for the production of particularly corrosion-resistant coatings on metal articles.
Abstract translation: 在电涂工艺中，使用至少部分以其与碱性化合物形式的盐形式存在的酸结合剂，用于形成盐的碱性化合物的组成范围为在酸性粘合剂的中和当量的0.1至50％ 可以在涂料组合物的水溶液或分散体中含有至少一种芳基胺和/或炔基胺和/或具有至少一种芳族配体的氢氧化季铵和/或氢氧化鏻以及其它常规添加剂和非碱性缓蚀剂。 该方法适用于生产金属制品上特别耐腐蚀的涂层。
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公开(公告)号：US3783112A
公开(公告)日：1974-01-01
申请号：US3783112D
申请日：1971-05-10
Applicant: BASF AG
CPC classification number: C25B3/10
Abstract: PROCESS FOR THE PRODUCTION OF SEBACIC ACID DIESTERS FROM ADIPIC ACID MONOESTERS OF HIGHER ALCOHOLS BY ELECTROCHEMICAL CONDENSATION IN METHANOLIC SOLUTION USING CONTINUOUS OR INTERMITTENT FLOW OF CURRENT, IN WHICH A SATURATED MONOOR POLYVALENT ETHER OR A LOWER ALKANOIC ACID IS ADDED TO THE REACTION MIXTURE.
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Patent Agency Ranking
公开(公告)号：ZA754625B
公开(公告)日：1976-07-28
申请号：ZA754625
申请日：1975-07-18
Applicant: BASF AG
IPC: C07C69/157 , C07C69/76 , C07D215/20 , C07D213/69 , C07D215/32 , C07D307/20 , C07D307/78 , C07D307/83 , C25B3/23 , C25B3/29 , C23B , C07C
Abstract: 1507920 Esters BASF AG 18 July 1975 [19 July 1974] 30186/75 Heading C2C [Also in Division C7] In electrochemical manufacture of an aromatic or heterocyclic ester by anodic acyloxylation of an aromatic or heterocyclic compound with an alkanoic acid, electrolysis is carried out in the presence of a conducting salt where R 1 , R 2 , and R 3 are the same or different and are H or alkyl, at least one being alkyl, and R 4 is H or C 1 -C 6 alkyl. The aromatic compound may be a benzene derivative, a naphthalene, anthracene, phenanthrene, acenaphthene, acenaphthylene, tetracene, perylene or chrysene; the heterocyclic compound may be quinoline or benzofuran; substituent groups on the aromatics may be alkyl, aryl, alkoxy, aryloxy, halogen, acyloxy, acylamino, cyano, nitro, or sulphonate; examples are given. Alkanoic acids mentioned are formic, acetic, propionic, butyric, valeric, isovaleric, and caproic; said salt may be made by reacting a suitable amine with such acid and may be trimethylammonium formate, acetate or propionate; triethyl ammonium formate, acetate or propionate, tri-n-butylammonium acetate, dimethylammonium formate, acetate or propionate, or diethylammonium acetate. The anode may be graphite, PbO 2 , Pt or Au, and the cathode graphite, Fe, steel or Pb; the electrode spacing may be 0À25-2 mm. and the C.D. 0À1- 30 A/dm. 2 ; a charge of 0À4-1À5 F/mole causes monoacyloxylation, and >2F/mole a higher degree. The electrolyte may comprise 5-60 wt. per cent aromatic or heterocyclic compound, 5-70% alkanoic acid, 1-20% of the salt and 0-50% of an inert co-solvent; everything apart from the product may be removed afterwards by distillation.
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公开(公告)号：ZA7504625B
公开(公告)日：1976-07-28
申请号：ZA7504625
申请日：1975-07-18
Applicant: BASF AG
IPC: C07D215/20 , C07C69/157 , C07C69/76 , C07D213/69 , C07D215/32 , C07D307/20 , C07D307/78 , C07D307/83 , C25B3/00 , C25B3/02 , C25B3/10 , C23B , C07C
CPC classification number: C25B3/02
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公开(公告)号：NO752427L
公开(公告)日：1976-01-20
申请号：NO752427
申请日：1975-07-04
Applicant: BASF AG
IPC: C07C69/157 , C07D215/20 , C07C69/76 , C07D213/69 , C07D215/32 , C07D307/20 , C07D307/78 , C07D307/83 , C25B3/23 , C25B3/29 , C25B
Abstract: 1507920 Esters BASF AG 18 July 1975 [19 July 1974] 30186/75 Heading C2C [Also in Division C7] In electrochemical manufacture of an aromatic or heterocyclic ester by anodic acyloxylation of an aromatic or heterocyclic compound with an alkanoic acid, electrolysis is carried out in the presence of a conducting salt where R 1 , R 2 , and R 3 are the same or different and are H or alkyl, at least one being alkyl, and R 4 is H or C 1 -C 6 alkyl. The aromatic compound may be a benzene derivative, a naphthalene, anthracene, phenanthrene, acenaphthene, acenaphthylene, tetracene, perylene or chrysene; the heterocyclic compound may be quinoline or benzofuran; substituent groups on the aromatics may be alkyl, aryl, alkoxy, aryloxy, halogen, acyloxy, acylamino, cyano, nitro, or sulphonate; examples are given. Alkanoic acids mentioned are formic, acetic, propionic, butyric, valeric, isovaleric, and caproic; said salt may be made by reacting a suitable amine with such acid and may be trimethylammonium formate, acetate or propionate; triethyl ammonium formate, acetate or propionate, tri-n-butylammonium acetate, dimethylammonium formate, acetate or propionate, or diethylammonium acetate. The anode may be graphite, PbO 2 , Pt or Au, and the cathode graphite, Fe, steel or Pb; the electrode spacing may be 0À25-2 mm. and the C.D. 0À1- 30 A/dm. 2 ; a charge of 0À4-1À5 F/mole causes monoacyloxylation, and >2F/mole a higher degree. The electrolyte may comprise 5-60 wt. per cent aromatic or heterocyclic compound, 5-70% alkanoic acid, 1-20% of the salt and 0-50% of an inert co-solvent; everything apart from the product may be removed afterwards by distillation.
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公开(公告)号：NO752427A
公开(公告)日：1976-01-20
申请号：NO752427
申请日：1975-07-04
Applicant: BASF AG
IPC: C07D215/20 , C07C69/157 , C07C69/76 , C07D213/69 , C07D215/32 , C07D307/20 , C07D307/78 , C07D307/83 , C25B3/00 , C25B3/02 , C25B3/10 , C25B
CPC classification number: C25B3/02
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