公开(公告)号：PL350827A1

公开(公告)日：2003-02-10

申请号：PL35082700

申请日：2000-03-17

Applicant: BASF AG

Inventor： SCHOENHERR MICHAEL ,  KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.

公开(公告)号：DE19913995A1

公开(公告)日：2000-10-05

申请号：DE19913995

申请日：1999-03-29

Applicant: BASF AG

Inventor： SCHOENHERR MICHAEL ,  KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15 ,  C07B63/00 ,  C07D295/04 ,  C07C305/06

Abstract: The invention relates to an improved method for the preparation of granular N-alkyl ammonium acetonitrile salts of formula (I) R R N R -CR R -CN Y in which R to R are hydrogen or organic rests and Y is a sulfate or hydrogen sulfate anion; from an aqueous solution of the compound of formula (II) R R N R -CR R -CN R O-SO2-O in which R is C1 to C4 alkyl. According to the invention the aqueous solution is evaporated at a temperature of between 80 and 250 DEG C and a pressure of between 10 mbar and 2 bar so as to obtain a melt and said melt is then left to solidify. During or after evaporation usual carrier materials and/or auxiliaries can be added. Lastly the resulting solidified compound (I) is given the desired granular form.

公开(公告)号：DE50005416D1

公开(公告)日：2004-04-01

申请号：DE50005416

申请日：2000-03-17

Applicant: BASF AG

Inventor： SCHOENHERR MICHAEL ,  KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.

公开(公告)号：HU0200282A2

公开(公告)日：2002-07-29

申请号：HU0200282

申请日：2000-03-17

Applicant: BASF AG

Inventor： KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR ,  SCHOENHER MICHAEL

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.

公开(公告)号：TR200102806T2

公开(公告)日：2002-04-22

申请号：TR200102806

申请日：2000-03-17

Applicant: BASF AG

Inventor： SCHOENHERR MICHAEL ,  KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.

公开(公告)号：AT260244T

公开(公告)日：2004-03-15

申请号：AT00912618

申请日：2000-03-17

Applicant: BASF AG

Inventor： SCHOENHERR MICHAEL ,  KINDER HANS-JUERGEN ,  MUNDINGER KLAUS ,  SCHUERMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.