公开(公告)号：ID30453A

公开(公告)日：2001-12-06

申请号：ID20012349

申请日：2000-03-17

Applicant: BASF AG

Inventor： SCHONHERR M ,  KINDER HANS-JURGEN ,  MUNDINGER KLAUS ,  SCHURMANN GREGOR

IPC: C07D295/14 ,  C07C253/30 ,  C07C253/32 ,  C07C255/25 ,  C07D295/15

Abstract: Improved process for the preparation of granular N-alkylammoniumacetonitrile salts Iwhere R1 to R5 are hydrogen or organic radicals, and Y- is a sulfate or hydrogensulfate anion,from an aqueous solution of the compound IIwhere R6 is C1- to C4-alkyl,which comprises evaporating this aqueous solution at a temperature of from 80° C. to 250° C. and a pressure of from 10 mbar to 2 bar to give a melt, then allowing the melt to solidify, where, during or following the evaporation, customary carrier materials and/or auxiliaries can be added, and the resulting solidified compound I is converted into the desired granular form.