PROCESS FOR THE PREPARATION OF DRY POLYCAPROLACTAM GRANULES

    公开(公告)号:DE3470546D1

    公开(公告)日:1988-05-26

    申请号:DE3470546

    申请日:1984-10-12

    Applicant: BASF AG

    Abstract: Dry polycaprolactam granules containing from 8 to 13% by weight of caprolactam and its oligomers are prepared by a method in which a caprolactam melt is extruded, the extrudates are cooled to 100 DEG -150 DEG C., left at this temperature until the polycaprolactam has substantially crystallized, and then immediately granulated, and the granules are left in a stream of inert gas, in the absence of molecular oxygen, for from 1 to 4 hours at from 100 DEG to 150 DEG C., and are then cooled.

    6.
    发明专利
    未知

    公开(公告)号:DE3730538A1

    公开(公告)日:1989-03-30

    申请号:DE3730538

    申请日:1987-09-11

    Applicant: BASF AG

    Inventor: WEHR RUDOLF DR

    Abstract: A TiO2-containing polycaprolactam contains, based on TiO2, less than 0.1% by weight of 100 DEG C. water solubles and from 2 to 15% by weight of monomeric caprolactam and oligomers thereof, based on polycaprolactam.

    8.
    发明专利
    未知

    公开(公告)号:DE3338294A1

    公开(公告)日:1985-05-02

    申请号:DE3338294

    申请日:1983-10-21

    Applicant: BASF AG

    Abstract: Dry polycaprolactam granules containing from 8 to 13% by weight of caprolactam and its oligomers are prepared by a method in which a caprolactam melt is extruded, the extrudates are cooled to 100 DEG -150 DEG C., left at this temperature until the polycaprolactam has substantially crystallized, and then immediately granulated, and the granules are left in a stream of inert gas, in the absence of molecular oxygen, for from 1 to 4 hours at from 100 DEG to 150 DEG C., and are then cooled.

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