Prepn of n-substituted xylylenediamines

    公开(公告)号:DE1808789A1

    公开(公告)日:1970-06-11

    申请号:DE1808789

    申请日:1968-11-14

    Applicant: BASF AG

    Abstract: N-substd. xylylene diamines (I) are prepd. by reaction at 20-200 degrees (pref. 60-100 degrees) of xylylene halides. (II) with primary or secondary amines or diamines (III) in a mol. ratio III:II= 1-5:1. Starting materials II are the o-, m- and pref. compds. The reaction is favourably influenced by the presence of tert. amines as acid absorbing agents, e.g. pyridine, NEt3. N-Me-piperidine, NMe2.CH2CH2OH. In examples p II was reacted with aniline. N-Me-aniline, o-toluidine, cyclohexylamine. Yields are 60-70% of theory of high purity. Operation is simple and economical. The products are starting materials for the prepn. of plant protection products, dyes, polyamides, plastics and lacquers.

    4.
    发明专利
    未知

    公开(公告)号:DE1908966A1

    公开(公告)日:1970-09-03

    申请号:DE1908966

    申请日:1969-02-22

    Applicant: BASF AG

    Abstract: 1292910 Rendering textile materials absorptive BADISCHE ANILIN- & SODA-FABRIK AG 20 Feb 1970 [22 Feb 1969] 8184/70 Heading D1P Textile materials are rendered absorptive and rewettable by treatment with one or more surphito betaines of the general formula where R 1 is a C 8-17 aliphatic hydrocarbon radical, R 2 and R 3 are alkyl radicals having up to 5 C atoms, A is -NH- r -O-, X is a alkylene radical having up to 5 C atoms, and n is 0 or 1. Textile materials which may be treated are those containing organic fibres, e.g. cotton, regenerated cellulose, cellulose ester, polyamide., polyester, polyacrylonitrile, polyolefin, wool and silk. The sulphito betaines are preferably applied from aqueous solution by dipping padding or spraying so that the textile retains less than 1 % (preferably 0.005- 0.5%) of its dry weight of the substance applied. The treated textile may then be rinsed in water and dried.

Patent Agency Ranking