公开(公告)号：US3860623A

公开(公告)日：1975-01-14

申请号：US33229173

申请日：1973-02-14

Applicant: BASF AG

Inventor： ZANKER FRITZ ,  MANGOLD DIETRICH

IPC: C07C265/00 ,  B01J31/00 ,  C07C20060101 ,  C07C67/00 ,  C07C241/00 ,  C07C263/04 ,  C07C265/04 ,  C07C119/04

CPC classification number: C07C263/04 ,  C07C2601/14 ,  C07C265/04 ,  C07C265/10

Abstract: New and valuable process for the production of isocyanates by reaction of carbamyl halides with aliphatic olefins.

Abstract translation: 通过氨基甲酰卤与脂族烯烃的反应生产异氰酸酯的新的和有价值的方法。

公开(公告)号：HU186694B

公开(公告)日：1985-09-30

申请号：HU164883

申请日：1983-05-12

Applicant: BASF AG

Inventor： GOETZ NORBERT ,  GIRKENSON BJOERN ,  ZANKER FRITZ

IPC: C07D265/30 ,  C07D295/023

Abstract: 1. A process for the preparation of 2,6-dimethylmorpholine containing a high proportion of the cis-isomer by cyclization of diisopropanolamine with sulfuric acid, working up the reaction mixture with sodium hydroxide solution, and distilling and drying the crude product obtained, wherein diisopropanolamine containing from 0 to 20 percent of water, and excess 90 to 120 percent strength sulfuric acid are simultaneously metered in such a manner into the reaction space, while stirring but without cooling, that the temperature of the reaction medium increases to 85 to 170 degrees C, and the reaction mixture is then heated at 150 to 190 degrees C for 1 to 25 hours while water is distilled off.

公开(公告)号：CA1207771A

公开(公告)日：1986-07-15

申请号：CA427731

申请日：1983-05-09

Applicant: BASF AG

Inventor： GOETZ NORBERT ,  GIRGENSOHN BJOERN ,  ZANKER FRITZ

IPC: C07D265/30 ,  C07D295/023

Abstract: 2,6-Dimethylmorpholine containing a high proportion of the cis compound is prepared by cyclization of diisopropanolamine (1,1'-iminobispropan-2-ol) in the presence of sulfuric acid, with simultaneous addition of the components and full utilization of the heat of reaction.

公开(公告)号：HU174885B

公开(公告)日：1980-04-28

申请号：HUBA002885

申请日：1973-03-01

Applicant: BASF AG

Inventor： ZANKER FRITZ ,  MANGOLD DIETRICH

IPC: C07C265/00 ,  B01J31/00 ,  C07C20060101 ,  C07C67/00 ,  C07C241/00 ,  C07C263/04 ,  C07C265/04 ,  C07C119/042

Abstract: New and valuable process for the production of isocyanates by reaction of carbamyl halides with aliphatic olefins.