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公开(公告)号：JP2014139190A
公开(公告)日：2014-07-31
申请号：JP2014031226
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , DESIRAJU GAUTAM R , RAHUL BANERJEE , BHATT PRASHANT M
IPC: C07D231/44 , A01N25/00 , A01N25/04 , A01N25/14 , A01N47/02 , A01P5/00 , A01P7/00 , A01P7/04 , A61K31/415 , A61P33/10 , A61P33/14
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl, and a method for producing said crystalline transformation, and also a composition for combating pests and parasites.SOLUTION: Use of a novel crystalline transformation IV of fipronyl of formula I below that exists in a triclinic crystalline system having center symmetric space group P-1. Said fipronyl is dissolved into acetone and crystallized to obtain crystalline transformation IV, and which is used, as it is (crystalline transformation IV), as a composition for controlling pests. High purity fipronyl of said crystalline transformation IV is a raw material for converting to crystalline transformation IV by further tempering the crystalline transformation IV at 90 to 100°C, or to crystalline transformation V by tempering at 100 to 130°C.
Abstract translation: 要解决的问题：提供呋喃尼基的新型结晶转化及其生产所述结晶转化的方法，以及用于防治害虫和寄生虫的组合物。解决方案：使用存在下述式I的呋喃基的新结晶转化IV 具有中心对称空间群P-1的三斜晶系。 将所述氟虫酰基溶于丙酮中并结晶，得到结晶转化IV，并将其作为（结晶转化IV）用作防治害虫的组合物。 所述结晶转变IV的高纯度fipronyl是通过在90至100℃进一步回火结晶转变IV或通过在100至130℃回火的结晶转变V而转化为结晶转变IV的原料。
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公开(公告)号：JP2014139188A
公开(公告)日：2014-07-31
申请号：JP2014031221
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , GAUTAM R DESIRAJU , RAHUL BANERJEE , PRASHANT M BHATT
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl of the formula below that was found and of which characteristics were determined, and a novel method for producing said crystalline transformation with high yield while excluding the production of other crystalline transformed forms, also a mixture and composition for killing insects and parasites comprising said crystalline transformation, and a method of their use for combating pests and parasites.SOLUTION: A crystalline transformation of fipronyl that has a particular X-ray powder diffraction chart, and undergoes, at 105°C to 145°C, phase transformation to two other crystalline transformations respectively having melting points of 196 to 197°C and 202 to 203°C.
Abstract translation: 要解决的问题：为了提供下面所公开的下列式子基的新型结晶转变，其特征是确定的，以及一种新的制备高产率的结晶转化同时排除其它结晶转化形式的生产的新方法 用于杀死昆虫和包含所述结晶转化的寄生虫的混合物和组合物及其用于防治害虫和寄生虫的方法。解决方案：具有特定X射线粉末衍射图的fipronyl的结晶转化并在105° C至145℃，相转变为分别具有196至197℃和202至203℃的熔点的两个其它结晶转化。
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公开(公告)号：JP2014141494A
公开(公告)日：2014-08-07
申请号：JP2014031217
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , STEFAN SCHERER , ANTTI OJALA , GAUTAM R DESIRAJU , RAHUL BANERJEE , PRASHANT M BHATT
IPC: C07D231/38 , A01N47/02 , A01P7/04 , A61K9/10 , A61K31/415 , A61P33/00 , A61P33/10 , A61P33/14
CPC classification number: A01N43/56 , A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a fipronyl crystal allowing easy filtration and drying with less dust in a production procedure and a composition which is blended with the crystal, has formulation stability and is for insecticidal and parasiticidal mixtures.SOLUTION: A solid fipronyl is present as a monoclinic system having a center-symmetry space group C2/c, shows a specific reflection in an X-ray powder diffraction diagram recorded at 25°C by using Cu-Kα radiation rays and contains at least 85 wt.% of a crystal transformation I of fipronyl. A method of producing the crystal transformation I comprises dissolving a solid fipronyl different from the crystal transformation I in a solvent selected from one or more of alcohols, acetonitrile(AN), dimethylsulfoxide(DMSO), one or more of benzene derivatives, etc. and crystallizing from the resultant solution. When the solvent is AN, crystallization is carried out at 40°C or lower. When the solvent is DMSO, crystallization is carried out at 80°C or lower.
Abstract translation: 要解决的问题：提供一种氟虫腈基晶体，其允许在制备方法中容易地过滤和干燥较少的粉尘，并且与晶体混合的组合物具有制剂的稳定性，并且是杀虫剂和杀寄生虫剂的混合物。解决方案：存在固体氟虫基 作为具有中心对称空间群C2 / c的单斜晶系，通过使用Cu-Kα射线在25℃记录的X射线粉末衍射图中显示特定的反射，并含有至少85重量％的结晶 氟吡酮的转化I。 制造晶体转变I的方法包括将不同于晶体转变I的固体氟虫酰基溶解在选自醇，乙腈（AN），二甲基亚砜（DMSO），一种或多种苯衍生物等中的一种或多种的溶剂中，以及 从所得溶液中结晶。 当溶剂为AN时，在40℃或更低温度下进行结晶。 当溶剂为DMSO时，在80℃或更低温度下进行结晶。
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公开(公告)号：JP2014139189A
公开(公告)日：2014-07-31
申请号：JP2014031222
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , DESIRAJU GAUTAM R , RAHUL BANERJEE , BHATT PRASHANT M
IPC: C07D231/44 , A01N25/04 , A01N25/12 , A01N47/02 , A01P5/00 , A01P7/04 , A61K31/415 , A61P33/10 , A61P33/14
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystal-transformed fipronil and an insecticidal and a parasiticidal composition.SOLUTION: A fipronil of a triclinic-system crystal transformation V is obtained by crystallizing a solid-form fipronil of formula (I) with dimethylsulfoxide at 100-150°C or acetonitrile at 60-81°C as solvent. A combination of the fipronil with an other insecticidal or parasiticidal compound provides an insecticidal or a parasiticidal composition having a synergistic effect against a specified target of an insect, an acarid or a parasite. The fipronil can be used as a mixture with a fungicidal compound.
Abstract translation: 要解决的问题：提供新型晶体转化的氟虫腈和杀虫剂和杀寄生虫剂组合物。解决方案：通过用二甲基亚砜结晶式（I）的固体形式的氟虫腈获得三斜晶系的晶体转变V的氟虫腈 100-150℃或乙腈在60-81℃作为溶剂。 氟虫腈与其他杀虫剂或杀寄生虫化合物的组合提供对昆虫，螨虫或寄生虫的特定靶标具有协同效应的杀虫剂或杀寄生虫剂组合物。 氟虫腈可以与杀真菌化合物混合使用。
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公开(公告)号：BRPI0718715B8
公开(公告)日：2021-03-23
申请号：BRPI0718715
申请日：2007-11-05
Applicant: BASF SE
Inventor： CLAUDE TARANTA , GAUTAM R DESIRAJU , GERHARD COX , HEIDI EMILIA SAXELL , PETER ERK , PRASHANT M BHATT , RAHUL BANERJEE , THOMAS KRÖHL
Abstract: modificação cristalina iv de fipronil contendo acetona cocristalizada, fipronil sólido, processos para preparar as modificações cristalinas iv, v e i, mistura pesticida ou parasiticida e composição pesticida ou parasiticida. a presente invenção diz respeito a uma modificação cristalina de fipronil, a um processo para a preparação do mesmo, às misturas e composições pesticidas e parasiticidas compreendendo a dita modificação cristalina e ao seu uso para combater pragas e parasitas.
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Patent Agency Ranking
公开(公告)号：BRPI0718715B1
公开(公告)日：2021-03-09
申请号：BRPI0718715
申请日：2007-11-05
Applicant: BASF SE
Inventor： CLAUDE TARANTA , GAUTAM R DESIRAJU , GERHARD COX , HEIDI EMILIA SAXELL , PETER ERK , PRASHANT M BHATT , RAHUL BANERJEE , THOMAS KRÖHL
Abstract: modificação cristalina iv de fipronil contendo acetona cocristalizada, fipronil sólido, processos para preparar as modificações cristalinas iv, v e i, mistura pesticida ou parasiticida e composição pesticida ou parasiticida. a presente invenção diz respeito a uma modificação cristalina de fipronil, a um processo para a preparação do mesmo, às misturas e composições pesticidas e parasiticidas compreendendo a dita modificação cristalina e ao seu uso para combater pragas e parasitas.
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公开(公告)号：CR10702A
公开(公告)日：2009-04-28
申请号：CR10702
申请日：2009-04-01
Applicant: BASF SE
Inventor： SANDRA LOHR , MICHAEL KEIL , JAN HENDRIK WEVERS , PETER ERK , HEIDI EMILIA SAXELL , GERHARD HAMPRECHT , WERNER SEITZ , GUIDO MAYER , BERND WOLF , GERHARD COX , ALFRED MICHEL , CYRILL ZAGAR , ROBERT REINHARD , BERND SIEVERNICH , THOMAS SCHMIDT , JOACHIM GEBHARDT
IPC: A01N43/48 , C07D239/54
Abstract: Hidratos de 2-cloro-5-[3,6-dihidro-3-metil-2,6-dioxo-4-(trifluorometil)-1-(2h)-pirimidinil]-4-fluor-N-[[metil-(1-metiletil)amino]sulfonil]benzamida. Tambien un proceso para la preparacion de estos hidratos y formulaciones destinadas a la fitoprotecion que comprenden hidratos de feniluracilo I.
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公开(公告)号：BR112013006073B1
公开(公告)日：2022-07-05
申请号：BR112013006073
申请日：2011-09-13
Applicant: BASF SE
Inventor： WEN XU , HEIDI EMILIA SAXELL , PAUL NEESE , WALTER WEISHAAR , WILLIAM MAURICE FLETCHER , RAINER BERGHAUS , TATJANA LEVY , CEDRIC DIELEMAN , DOUGLAS D ANSPAUGH , KARA BENTON , PAUL CH KIERKUS
Abstract: COMPOSIÇÕES, MÉTODO PARA PREPARAR UMA MISTURA EM TANQUE, USO DO ADJUVANTE, KIT DE PARTES, FORMULAÇÃO PESTICIDA, HIDRATOS CRISTALINOS E MÉTODOS PARA PROTEGER PLANTAS, PARA CONTROLAR INSETOS E PARA PROTEÇÃO DE MATERIAL DE PROPAGAÇÃO DE PLANTAS. A presente invenção refere-se a composições que compreendem um pesticida de piripiropeno de fórmula (I) ou (II) e um adjuvante. A presente invenção também se refere a métodos para preparar e aplicar tais composições, assim como diversos usos das mesmas, e, finalmente, sementes que compreendem a dita composição. A invenção também se refere a uma formulação pesticida aquosa que compreende um composto pesticida de fórmula I, conforme definido na reivindicação I, sob a forma de partículas finas suspensas em um líquido aquoso.
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公开(公告)号：PT2117297E
公开(公告)日：2012-02-08
申请号：PT08708832
申请日：2008-02-08
Applicant: BASF SE
Inventor： ERK PETER , BRATZ MATTHIAS , ISRAELS RAFEL , HEIDI EMILIA SAXELL
IPC: A01N25/00 , A01N43/653 , A01N47/24 , A01N47/34 , C07D417/06
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公开(公告)号：CR10704A
公开(公告)日：2009-04-29
申请号：CR10704
申请日：2009-04-01
Applicant: BASF SE
Inventor： THOMAS SCHMIDT , SANDRA LOHR , MICHAEL KEIL , JAN HENDRIK WEVERS , PETER ERK , HEIDI EMILIA SAXELL , GERHARD HAMPRECHT , WERNER SEITZ , GUIDO MAYER , BERND WOLF , GERHARD COX , ALFRED MICHEL , CYRILL ZAGAR , ROBERT REINHARD , BERND SIEVERNICH , JOACHIM GEBHARDT
IPC: A01N43/48 , C07D239/54
Abstract: Forma cristalina de 2-cloro-5-[3,6-dihidro-3-metil-2,6-dioxo-4-(trifluorometil)-1-(2H)pirimidinil]-4-fluoro-N-[[metil(1-metiletil)amino]sulfonil]benzamida. Tambien un proceso para la preparacion de esta forma cristalina y formulaciones fitoprotectoras que comprenden esta forma cristalina de feniluracilo.
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