2.
    发明专利
    未知

    公开(公告)号:AT549379T

    公开(公告)日:2012-03-15

    申请号:AT03717301

    申请日:2003-04-15

    Applicant: BASF SE

    Abstract: A process for preparing perylene-3,4:9,10-tetracarboxylic dianhydride, comprising: dimerizing a naphthalene-1,8-dicarboximide of the formula IIa; reoxidizing the resulting alkali metal salt of the leuco form of the perylene-3,4:9,10-tetracarboxylic diimide of the formula Ia; hydrolyzing the diimide to the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid in the presence of an inert organic solvent, of an alkali metal base and of water; and subjecting the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid to the action of an aqueous inorganic acid to convert it into perylene-3,4:9,10-tetracarboxylic dianhydride; wherein R3 is cyclohexyl or phenyl which may each be substituted by up to three C1-C4-alkyl radicals, and the dimerizing is in a substantially homogeneous reaction medium consisting essentially of an apolar aprotic organic solvent and an alkali metal base.

    3.
    发明专利
    未知

    公开(公告)号:DE502005007702D1

    公开(公告)日:2009-08-27

    申请号:DE502005007702

    申请日:2005-01-15

    Abstract: A process for preparing terylene-3,4:11,12-tetracarboximides I where the variables are each defined as follows: R, R' are each independently hydrogen; if desired substituted alkyl or cycloalkyl; R 1 is hydrogen or alkyl; R 2 is hydrogen; alkyl; if desired substituted aryl or hetaryl, by reacting a perylene-3,4-dicarboximide II in the presence of a base-stable, high-boiling organic solvent and of an alkali metal or alkaline earth metal base, with a naphthalene-1,8-dicarboximide III in which X is hydrogen, bromine or chlorine.

Patent Agency Ranking