Method for producing bispyrrolidine compounds

    公开(公告)号:US11345680B2

    公开(公告)日:2022-05-31

    申请号:US16766678

    申请日:2018-11-13

    Applicant: BASF SE

    Abstract: The present application relates to a method for preparing compounds of the formula I in which, in a first step, γ-butyrolactone is reacted with diamines of the formula II to form bisamides of the formula Ill, with the amide function of the bisamides of the formula Ill then undergoing partial or complete catalytic hydrogenation in step II) to form bispyrrolidine compounds of the formula I.

    Method for flotation of a silicate-containing iron ore with a cationic collector

    公开(公告)号:US12275019B2

    公开(公告)日:2025-04-15

    申请号:US17606997

    申请日:2020-04-27

    Applicant: BASF SE

    Abstract: The invention relates to a method for manufacturing a concentrate enriched in iron mineral content from an ore, which contains an iron mineral and silicate, by reverse flotation, which method comprises the step of (c) adding a compound of formula I wherein R1 is C9-C22 alkyl or alkenyl, which is linear or branched, R2 is H, C1-C4 alkyl, which is linear or branched, R3 is —X—NH2, H or C1-C4 alkyl, which is linear or branched, and X is C2-C4 alkylene, which is linear or branched, or a salt of a protonated compound of formula I and an anion, to a prepared aqueous pulp of the ore and optionally one or more flotation auxiliaries to obtain an aqueous mixture. Furthermore, a method for manufacturing a specific group of compounds of formula I, i.e. compounds of formula 1-X wherein R1 is C9-C15 alkyl, which is linear or branched, R2 is H, R3 is —X—NH2 and X is C2-C4 alkylene, which is linear or branched, is disclosed.

    METHOD FOR FLOTATION OF A SILICATE-CONTAINING IRON ORE WITH A CATIONIC COLLECTOR

    公开(公告)号:US20220212204A1

    公开(公告)日:2022-07-07

    申请号:US17606997

    申请日:2020-04-27

    Applicant: BASF SE

    Abstract: The invention relates to a method for manufacturing a concentrate enriched in iron mineral content from an ore, which contains an iron mineral and silicate, by reverse flotation, which method comprises the step of (c) adding a compound of formula I wherein R1 is C9-C22 alkyl or alkenyl, which is linear or branched, R2 is H, C1-C4 alkyl, which is linear or branched, R3 is —X—NH2, H or C1-C4 alkyl, which is linear or branched, and X is C2-C4 alkylene, which is linear or branched, or a salt of a protonated compound of formula I and an anion, to a prepared aqueous pulp of the ore and optionally one or more flotation auxiliaries to obtain an aqueous mixture. Furthermore, a method for manufacturing a specific group of compounds of formula I, i.e. compounds of formula 1-X wherein R1 is C9-C15 alkyl, which is linear or branched, R2 is H, R3 is —X—NH2 and X is C2-C4 alkylene, which is linear or branched, is disclosed.

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