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    processos para a preparação contínua dos succinatos de dialquila c1-c3 e para a separação do efluente do reator
    3.
    发明专利
    processos para a preparação contínua dos succinatos de dialquila c1-c3 e para a separação do efluente do reator 未知

    公开(公告)号：BR112015027995A2

    公开(公告)日：2017-07-25

    申请号：BR112015027995

    申请日：2014-05-07

    Applicant: BASF SE

    Inventor： GABRIELE IFFLAND ,  GABRIELE IFFLAND ,  JENS WITTENBERG ,  JENS WITTENBERG ,  STEFANIE DEMMING ,  STEFANIE DEMMING ,  STEPHAN FREYER ,  STEPHAN FREYER ,  SUMAN THOTLA ,  SUMAN THOTLA ,  TILL CHRISTIAN BRÜGGEMANN ,  TILL CHRISTIAN BRÜGGEMANN ,  WOLFGANG SIEGEL ,  WOLFGANG SIEGEL ,  YVONNE HOELZL ,  YVONNE HOELZL

    IPC: C07C67/08

    Abstract: resumo “processos para a preparação contínua dos succinatos de dialquila c1-c3 e para a separação do efluente do reator“ a presente invenção se refere a um processo para a preparação contínua dos succinatos de dialquila c1-c3, reagindo o ácido succínico com um alcanol c1-c3 na presença de um catalisador de esterificação acídica heterogênea de leito fixo em um reator tubular, a uma temperatura no intervalo a partir de 60 a 100º c, em que uma mistura, que compreende o ácido succínico, alcanol c1-c3, succinato de monoalquila c1-c3, succinato de dialquila c1-c3 e água, é formada em um estágio de mistura e alimentada para a entrada do reator tubular, e em que de 5 a 75% da taxa de fluxo de saída do reator tubular são diretamente reciclados para o estágio de mistura como uma corrente de reciclagem, e a proporção molar de alcanol c1-c3 para o ácido succínico adicionado à zona de mistura, e não incluindo o alcanol c1-c3 e ácido succínico na corrente de reciclagem, está no intervalo a partir de 2,0 a 9,5. a presente invenção ainda se refere a um processo para a separação do efluente do reator de uma esterificação do ácido succínico com um alcanol c1-c3 para fornecer os succinatos de dialquila c1-c3 através da destilação, em que a separação é realizada em uma coluna de parede dividida em que o alcanol c1-c3 e a água são removidos em um estiramento superior da coluna, o succinato de dialquila c1-c3 é removido em um estiramento lateral da coluna, e em que o succinato de monoalquila c1-c3 e o ácido succínico são removidos em um estiramento inferior da coluna.

    Fermentative production of non-volatile microbial metabolism products in solid form
    7.
    发明专利
    Fermentative production of non-volatile microbial metabolism products in solid form 未知

    公开(公告)号：AU2006289083B2

    公开(公告)日：2011-08-25

    申请号：AU2006289083

    申请日：2006-09-06

    Applicant: BASF SE

    Inventor： OSKAR ZELDER ,  EDZARD SCHOLTEN ,  MARKUS POMPEJUS ,  MATTHIAS BOY ,  STEPHAN FREYER ,  MARKUS LOHSCHEIDT

    IPC: C12P19/14 ,  A23L7/104 ,  A23L35/00 ,  C12P13/08 ,  C12P13/14

    Abstract: The invention relates to a method for production of at least one non-volatile microbial metabolism product in solid form by sugar-based microbial fermentation, wherein a microbial strain producing the required metabolism product is cultivated with a sugary liquid medium with a monosaccharide content of more than 20 wt. %, based on the total weight of the liquid medium, the volatile components of the fermentation brew are mostly removed, the sugary liquid medium being produced by: a1) milling a starch source selected from cereal grains, a2) liquefying the milled material in an aqueous liquid in the presence of at least one starch-digesting enzyme and subsequent saccharification using at least one saccharifying enzyme, wherein the liquefying is carried out with addition of a partial amount of the milled material to the aqueous fluid continuously or batch-wise. The invention further relates to a solid formulation obtained by the above method of a non-volatile microbial metabolism product and the use of such a solid formulation as additive or supplement to animal or human food or for textile, leather, cellulose, paper or surface treatments.

    Fermentative production of non-volatile microbial metabolism products in solid form
    9.
    发明专利
    Fermentative production of non-volatile microbial metabolism products in solid form 未知

    公开(公告)号：ZA200802925B

    公开(公告)日：2009-06-24

    申请号：ZA200802925

    申请日：2008-04-03

    Applicant: BASF SE

    Inventor： EDZARD SCHOLTEN ,  MARKUS POMPEJUS ,  STEPHAN FREYER ,  MARKUS LOHSCHEIDT ,  ZELDER OSKAR ,  MATTHIAS BOY

    IPC: A23L7/104 ,  A23L35/00 ,  C12P20090101

    Abstract: The present invention relates to a method for the production of at least one nonvolatile microbial metabolite in solid form by sugar-based microbial fermentation, in which process a microorganism strain which produces the desired metabolites is grown using a sugar-containing liquid medium with a monosaccharide content of more than 20% by weight based on the total weight of the liquid medium, and the volatile constituents of the fermentation liquor are subsequently largely removed, the sugar-containing liquid medium being prepared by: a1) milling selected starch feedstock from cereal grains; and a2) liquefying the millbase in an aqueous liquid in the presence of at least one starch-liquefying enzyme, followed by saccharification using at least one saccharifying enzyme, where, for liquefaction purposes, at least a portion of the millbase is liquefied by continuous or batchwise addition to the aqueous liquid. Furthermore, the invention relates to a solid formulation, of a nonvolatile microbial metabolite, obtainable by the method according to the invention; and to the use of such a solid formulation as additive or supplement for human or animal nutrition or for the treatment of textiles, leather, cellulose, paper or surfaces.

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