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    2,2{40 ,4,4{40 -tetrachloro-5,5{40 -diamino-diphenyl ether
    1.
    发明授权
    2,2{40 ,4,4{40 -tetrachloro-5,5{40 -diamino-diphenyl ether 失效
    2,2 {40,4,4 {40-TETRACHLORO-5,5 {40-DIAMINO-DIPHENYL ETHER

    公开(公告)号：US3673123A

    公开(公告)日：1972-06-27

    申请号：US3673123D

    申请日：1970-02-27

    Applicant: BAYER AG

    Inventor： TACKE PETER ,  BINSACK RUDOLF ,  WEISSEL OSKAR

    IPC: C08G69/42 ,  C08L75/00 ,  C07C93/14

    CPC classification number: C08G69/42 ,  C08L75/00

    Abstract: The 2,2'',4,4''-tetrachloro-5,5''-diamino-diphenyl ether which is useful as starting material for the production of polyamides and polyurethanes and which may be obtained by the reduction of the corresponding dinitro compound.

    Abstract translation: 2,2'，4,4'-四氯-5,5'-二氨基二苯基醚，可用作生产聚酰胺和聚氨酯的原料，可通过还原相应的二硝基化合物而得到。

    8.
    发明专利
    未知

    公开(公告)号：FR1242941A

    公开(公告)日：1960-10-07

    申请号：FR803267

    申请日：1959-08-21

    Applicant: BAYER AG

    Inventor： RAUE RODERICH ,  MUELLER WERNER ,  WEISSEL OSKAR ,  COENEN MAX ,  PSAAR HUBERTUS

    IPC: C07D209/08 ,  C07D209/18 ,  C07D403/06 ,  C08K5/3445 ,  C09B23/10 ,  D01F1/10

    Abstract: The Specification relates to methine dyes of the general formula: wherein R1 is hydrogen, chlorine, bromine, alkyl, alkoxy, hydroxy alkoxy, amino, acetylamino, benzoylamino, nitro, sulphonamido, alkylsulphonamido, alkyl sulphonyl, alkylsulphonylamino, phenylsulphonylamino, phenyl or carbalkoxy, or represents a fused-on benzene ring, R3 is hydrogen or alkyl, R41 is a cyano, acyl or carbalkoxy group and R5 is the residue of a 5-pyrazolone, cyanacetic acid or an alkyl ester, substituted alkyl ester or amide thereof, or of malonic acid dinitrile, the residue R5 being free from sulphonic acid groups and all the said alkyl and alkoxy groups containing from 1 to 5 carbon atoms. The dyes are prepared by condensing a compound R5H2 with a 3;3-dimethyl-2-methylene -indoline-o -aldehyde having also an o -cyano, acyl or carbalkoxy substituent (R41), preferably in an alkaline medium. An emulsifying agent such as polyoxyethylene oleyl ether also may be present. In the case where R5 is the residue of a 5-pyrazolone, the dyes may be prepared by reacting a 3;3-dimethyl-2-methylene-indoline having an o -cyano, acyl or carbalkoxy substituent (R41) with a 5-pyrazolone having in its 4-position a -CHO or =CH-N(alkyl)2 group, preferably in an acidic medium. Dyes are specified wherein the substituent R1 in the indoline component is methyl, methoxy, carbomethoxy or chlorine. Pyrazolone components are specified having a 1-phenyl, chlorophenyl, dichlorophenyl, nitrophenyl, or methylphenyl substituent and a 3-methyl or carboxylic acid, ester or amide substituent. The group R41 may be cyano, benzoyl or carbethoxy. Specification 929,394 is referred to.

    9.
    发明专利
    未知

    公开(公告)号：FR1228155A

    公开(公告)日：1960-08-26

    申请号：FR788173

    申请日：1959-03-03

    Applicant: BAYER AG

    Inventor： COENEN MAX ,  WEISSEL OSKAR

    IPC: C09B23/01 ,  C09B23/02 ,  C09B23/06 ,  C09B23/08 ,  C09B23/10 ,  C09B23/14 ,  D06P5/00 ,  G03C1/12

    Abstract: Cyanine dyes are prepared by reacting a 2-cyanmethylene-indoline of the formula wherein n is 0 or 1, A is an ortho phenylene or ortho naphthalene residue, R is H or CN, X is a dialkylated carbon atom and Y is N-alkyl, with a 1; 3; 3-trialkyl-2-methylene-indoline-o -aldehyde, an indole-3-aldehyde or a p-di-substituted aminobenzaldehyde in the presence of an acidic condensing agent. Examples are given of the preparation of trimethine dyes by reacting a 1-methyl- or 1-ethyl-3; 3-dimethyl-2-cyanmethylene-indoline which may have methyl, methoxy, chloro, carbomethoxy or phenyl substituents in the benzene ring, with a 1; 3; 3-trimethyl-2-methylene-indoline-o -aldehyde which may have methyl, methoxy, or chloro substituents in the benzene ring, or with 1-ethyl-3; 3-dimethyl-5-ethoxy-2-methylene-indoline-10-aldehyde. Other 2-methylene-indoline-w-aldehyde starting materials are referred to including ones having in the 5-position a nitro, carboxylic amido or ester, cyano, acylamino, alkylsulphonylamino, arylsulphonylamino or sulphonamido substituent. In Example 11, an a -g -dicyano-pentamethine dye is prepared from 1; 3; 3-trimethyl-2-(a -g -dicyano-propenylidene)-indoline and 1; 3; 3-trimethyl-2-methylene-indoline-o -aldehyde. In Example 12, a dimethine dye is prepared from 1; 3; 3-trimethyl-2-cyanmethylene - indoline and 1 - methyl - 2 - phenyl - indole-3-aldehyde. In Example 13, a styryl dye is prepared from 1; 3; 3-trimethyl-2-cyanmethylene - indoline and p - dimethylamino - benzaldehyde; reference is made to using p-(N-methyl - N - phenylamino) - or p - (N - methyl - N - (p1 - methoxyphenyl) - amino) benzaldehydes. The reactions may be carried out in benzene, ligroin, cyclohexane, chloroform, chlorobenzene, acetone or acetic acid as solvent, and with phosphorus oxychloride, thionyl chloride, acetyl chloride, acetic anhydride, sulphuric acid or phosphoric acid as acidic condensing agent. Specifications 823,520 and 897,195 are referred to.

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