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    Process for the manufacture of piperidine derivatives
    1.
    发明授权
    Process for the manufacture of piperidine derivatives 失效
    制备哌啶衍生物的方法

    公开(公告)号：US3879399A

    公开(公告)日：1975-04-22

    申请号：US39489373

    申请日：1973-09-06

    Applicant: CIBA GEIGY AG

    Inventor： ZONDLER HELMUT ,  PFLEIDERER WOLFGANG

    IPC: C08G59/50 ,  C07D29/06

    CPC classification number: C08G59/506

    Abstract: 3-( gamma -aminopropyl)-piperidines can be manufactured by hydrogenating certain bis-cyanoethylated aldimines in the presence of a catalyst and preferably in the presence of an organic solvent. The hydrogenation can be executed at temperatures up to 200*C either without application of pressure or under pressure. Cyclisation occurs with a primary amin being split off. The piperidine derivatives, obtainable according to this invention are suitable as curing agents for epoxy resins.

    Abstract translation: 3-（γ-氨基丙基） - 哌啶可以通过在催化剂存在下，优选在有机溶剂的存在下氢化某些双氰基乙基化的醛亚胺来制备。 氢化可以在高达200℃的温度下进行，无需施加压力或压力。 原发性氨基被分裂时发生环化。

    HETEROCYCLIC SUBSTITUTED DIHALOISONICOTINICACIDAMIDES FOR PROTECTING PLANTS AGAINST MICROORGANISMS
    9.
    发明专利
    HETEROCYCLIC SUBSTITUTED DIHALOISONICOTINICACIDAMIDES FOR PROTECTING PLANTS AGAINST MICROORGANISMS 未知

    公开(公告)号：AU622640B2

    公开(公告)日：1992-04-16

    申请号：AU3114989

    申请日：1989-03-08

    Applicant: CIBA GEIGY AG

    Inventor： ZONDLER HELMUT ,  MEYER ALFRED ,  ECKHARDT WOLFGANG ,  KUNZ WALTER

    IPC: A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/58 ,  A01N43/60 ,  A01N43/653 ,  C07D213/81 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14 ,  C07D413/14 ,  A01N43/56 ,  A01N43/84

    Abstract: Novel substituted isonicotinic acid amides of the general formula in which X in ortho/ortho'-position are equal and represent fluorine, chlorine, bromine or iodine; Q1 is unsubstituted pyridimin-4-yl, or pyrimidin-4-yl substituted by R1, R2 and R3; Q2 is unsubstituted pyrimidin-2-yl, or pyrimidin-2-yl substituted by R1, R2 and R3; Q3 is unsubstituted pyrimidin-5-yl, or pyrimidin-5-yl substituted by R1, R2 and R3; Q4 is pyridin-2-yl, pyridin-3-yl or pyridin-4-yl each of which is unsubstituted or substituted by R1, R2 and R3; Q5 is pyridazin-3-yl or pyridazin-4-yl each of which is unsubstituted or substituted by R1, R2 and R3; Q6 is unsubstituted pyrazin-2-yl, or pyrazin-2-yl substituted by R1, R2 and R3; R1, R2, R3 are hydrogen, halogen, C1-C6alkyl, C1-C6haloalkyl having from 1 to 3 halogen atoms, C1-C6alkoxy, C2-C6alkoxyalkyl, C1-C6thioalkyl, C1-C6haloalkoxy having from 1 to 5 halogen atoms, C3-C6alkenyloxy, C3-C6alkynyloxy, C3-C6thioalkenyl, C3-C6cycloalkyl, C3-C6cycloalkyl substituted by methyl, or nitro, cyano, the radical CH(OR4)2 or COOR4 in which R4 is C1-C4alkyl; also phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl; or phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl each substituted at least once by C1-C3alkyl, C1-C3-alkoxy, C1-C3haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano; and also N(R5)R6 in which R5 and R6, independently of one another, are each C1-C6alkyl; and furthermore piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl, or piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl each substituted by C1-C3alkyl, C1-C3alkoxy, C1-C3haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano. The novel active ingredients have plant-protecting properties and are suitable especially for the preventive protection of plants against attack by phytopathogenic microorganisms such as fungi, bacteria and viruses.

    PROCESS FOR PRODUCING PYRIMIDYL-/NAPHTYL/ALKYL/-AMINE DERIVATIVES AND INSECTICIDE, ACARICIDE AND FUNGICIDE COMPOSITIONS CONTAINING THEM AS ACTIVE COMPONENTS
    10.
    发明专利
    PROCESS FOR PRODUCING PYRIMIDYL-/NAPHTYL/ALKYL/-AMINE DERIVATIVES AND INSECTICIDE, ACARICIDE AND FUNGICIDE COMPOSITIONS CONTAINING THEM AS ACTIVE COMPONENTS 未知

    公开(公告)号：HUT58300A

    公开(公告)日：1992-02-28

    申请号：HU266691

    申请日：1991-08-09

    Applicant: CIBA GEIGY AG

    Inventor： KRISTIANSEN ODD ,  ZONDLER HELMUT ,  MUELLER URS

    IPC: A01N43/54 ,  C07D239/42 ,  C07D239/46 ,  C07D239/47 ,  C07D239/48

    Abstract: Compounds of the formula I in which: R1 denotes hydrogen, C1-C5-alkyl which is unsubstituted or substituted by halogen or C1-C3-alkoxy or S(O)p-C1-C3-alkyl; C2-C7-alkenyl which is unsubstituted or substituted by halogen; C3-C7-cycloalkyl; halogen; or C2-C4-alkynyl; R2 denotes hydrogen, hydroxyl, C1-C5-alkyl which is unsubstituted or substituted by halogen or C1-C3-alkoxy, C1-C4-alkoxy, S(O)p-C1-C4-alkyl, halogen, nitro, cyano, amino, NHR3, N(R3)R9 or N=C(R9)R10; R3 denotes hydrogen; C1-C5-alkyl; benzyl; -CO-R6 or -S-R7; R4 and R8 independently of one another denote hydrogen; C1-C5-alkyl which is unsubstituted or substituted by halogen or C1-C3-alkoxy; or C3-C7-cycloalkyl; R5 denotes halogen, C1-C3-alkyl, C1-C3-alkoxy, C2-C6-alkoxyalkyl, C1-C3-haloalkyl, C1-C3-alkylthio, C1-C3-haloalkoxy, C1-C3-haloalkylthio, CN, NO2 or an -X-phenyl group occurring once on the naphthyl ring, which is unsubstituted or mono- to trisubstituted by identical or different halogen, C1-C3-alkyl or C1-C3-alkoxy substituents; R6 denotes C1-C5-alkyl; phenyl which is unsubstituted or substituted by halogen and/or C1-C3-alkyl; R7 denotes phenyl or benzyl, which are unsubstituted or mono- or disubstituted in the ring by identical or different halogen, nitro or cyano substituents; or C1-C5-alkyl which is unsubstituted or substituted by halogen or cyano; R9 denotes C1-C5-alkyl, R10 denotes hydrogen or C1-C5-alkyl, R13 denotes hydrogen; C1-C4-alkyl which is unsubstituted or substituted by halogen or C1-C3-alkoxy; cyclopropyl; halogen; C1-C3-alkoxy; C1-C3-alkylthio or -N(C1-C3-alkyl)2; X denotes oxygen or sulfur; m denotes 1, 2 or 3; n denotes 0, 1, 2 or 3 and p denotes 0, 1 or 2. The novel active substances have useful biocidal properties. They can be employed in plant protection for preventing the infestation of crop plants by pests and for controlling these pests.

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