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1.发明申请COMPOSITIONS CONTAINING POLYHYDROXYOXOALUMINUM CATIONS AND MANUFACTURE THEREOF 审中-公开含有聚羟基氧铝粉的组合物及其制造方法
公开(公告)号：WO2012148481A1
公开(公告)日：2012-11-01
申请号：PCT/US2011/066018
申请日：2011-12-20
Applicant: COLGATE-PALMOLIVE COMPANY , VAUGHN, John , PAPPAS, Iraklis , PAN, Long
Inventor： VAUGHN, John , PAPPAS, Iraklis , PAN, Long
CPC classification number: C01F7/026 , A61K8/26 , A61K8/28 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01F7/002 , C01F7/56 , C01P2002/86 , C01P2002/87
Abstract: A composition comprising a polyhydroxyoxoaluminum cation detectable at 76 ppm by 27 Al NMR that is present in a relative abundance on a 27 Al NMR spectrograph that is greater than any other polyhydroxyoxoaluminum cation detectable by 27 Al NMR. Also, disclosed are methods of making the composition.
Abstract translation: 包含通过27Al NMR在76ppm下可检测的聚羟基氧代铝阳离子的组合物，其在27Al NMR光谱仪上的相对丰度存在，其大于可通过27Al NMR检测的任何其它聚羟基氧代铝阳离子。 此外，公开了制备组合物的方法。
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公开(公告)号：WO2015072970A1
公开(公告)日：2015-05-21
申请号：PCT/US2013/069653
申请日：2013-11-12
Applicant: COLGATE-PALMOLIVE COMPANY
Inventor： PAN, Long , YUAN, Shaotang , PAPPAS, Iraklis , VAUGHN, John , MASTERS, James G.
CPC classification number: G01N27/44782 , A61K8/19 , A61K8/26 , A61K8/27 , A61K8/28 , A61K8/44 , A61K2800/58 , A61K2800/74 , A61K2800/805 , A61Q15/00 , D06M13/005
Abstract: Methods of estimating the suitability of a candidate antiperspirant material by measuring the zeta potential of the material.
Abstract translation: 通过测量材料的ζ电位来估计候选止汗材料的适用性的方法。
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公开(公告)号：WO2012061280A2
公开(公告)日：2012-05-10
申请号：PCT/US2011/058559
申请日：2011-10-31
Applicant: COLGATE-PALMOLIVE COMPANY , PAPPAS, Iraklis , VAUGHN, John , PAN, Long
Inventor： PAPPAS, Iraklis , VAUGHN, John , PAN, Long
CPC classification number: C01F7/56 , A61K8/26 , A61K8/28 , A61K8/44 , A61K2800/592 , A61K2800/80 , A61Q15/00 , C01F7/002 , C01P2002/86 , C01P2002/87
Abstract: A composition comprising an aluminum chlorohydrate salt, the aluminum chlorohydrate salt having at least 50 mole % Al 30 polyhydroxyoxoaluminum cation of all polyhydroxyoxoaluminum cations detectable by quantitative 27 Al NMR within the aluminum chlorohydrate salt, and a buffer. The composition can optionally include zirconium. Also disclosed are a method of making an aluminum salt using an increased molar concentration of a starting aluminum salt with a buffer, a method of reducing perspiration with the aluminum chlorohydrate salt, and a method of treating water with the aluminum chlorohydrate salt.
Abstract translation: 一种包含氯化铝水合物盐的组合物，该水合氯化铝盐具有至少50摩尔％的所有聚羟基氧化铝阳离子的Al30聚羟基氧化铝阳离子，可通过铝水合盐内的定量27 Al NMR和缓冲液检测。 该组合物可以任选地包括锆。 还公开了使用起始铝盐与缓冲剂的摩尔浓度增加的方法，用氯化铝水合物盐减少汗水的方法以及用氯化铝水盐处理水的方法。
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公开(公告)号：WO2013158077A1
公开(公告)日：2013-10-24
申请号：PCT/US2012/033926
申请日：2012-04-17
Applicant: COLGATE-PALMOLIVE COMPANY , YUAN, Shaotang , PAN, Long , VAUGHN, John , PAPPAS, Iraklis , MASTERS, James
Inventor： YUAN, Shaotang , PAN, Long , VAUGHN, John , PAPPAS, Iraklis , MASTERS, James
CPC classification number: A61K8/26 , A61K8/28 , A61K2800/80 , A61Q15/00 , C01F7/002 , C01F7/56 , C01G25/006
Abstract: A method of making aluminum salt compositions using a combination of a basic organic buffer with a source of alkaline earth metal ions. This selection of basic organic buffer provides for a lower alkaline earth metal salt content in the composition made by the method.
Abstract translation: 一种使用碱性有机缓冲液与碱土金属离子源的组合制备铝盐组合物的方法。 碱性有机缓冲液的选择提供了通过该方法制备的组合物中较低的碱土金属盐含量。
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公开(公告)号：WO2012148480A1
公开(公告)日：2012-11-01
申请号：PCT/US2011/066012
申请日：2011-12-20
Applicant: COLGATE-PALMOLIVE COMPANY , VAUGHN, John , PAPPAS, Iraklis , PAN, Long
Inventor： VAUGHN, John , PAPPAS, Iraklis , PAN, Long
CPC classification number: A61K8/26 , A61K8/19 , A61K8/20 , A61K8/28 , A61K8/42 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01F7/002 , C01F7/56 , C01P2002/86 , C01P2002/87
Abstract: An antiperspirant active composition comprising an aluminum salt, the aluminum salt (i) having an aluminum to chloride molar ratio of 0.3:1 to 3:1; and (ii) having a species of polyhydroxyoxoaluminum cation detectable at 76 ppm by 27 Al NMR that is present in a relative abundance on a 27 Al NMR spectrograph that is greater than any other polyhydroxyoxoaluminum cation detectable by 27 Al NMR. Also, disclosed are methods of making the antiperspirant active.
Abstract translation: 一种止汗活性组合物，其包含铝盐，所述铝盐（i）的铝与氯化物的摩尔比为0.3:1至3:1; 和（ii）具有通过27Al NMR在76ppm处可检测到的聚羟基氧化铝阳离子的种类，其在27Al NMR光谱仪上的相对丰度存在，其大于通过27Al NMR可检测的任何其它聚羟基氧代铝阳离子。 此外，公开了使止汗剂活性的方法。
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Patent Agency Ranking
公开(公告)号：EP2702007A1
公开(公告)日：2014-03-05
申请号：EP11808786.5
申请日：2011-12-20
Applicant: Colgate-Palmolive Company
Inventor： VAUGHN, John , PAPPAS, Iraklis , PAN, Long
CPC classification number: A61K8/26 , A61K8/19 , A61K8/20 , A61K8/28 , A61K8/42 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01F7/002 , C01F7/56 , C01P2002/86 , C01P2002/87
Abstract: An antiperspirant active composition comprising an aluminum salt, the aluminum salt (i) having an aluminum to chloride molar ratio of 0.3:1 to 3:1; and (ii) having a species of polyhydroxyoxoaluminum cation detectable at 76 ppm by 27Al NMR that is present in a relative abundance on a 27Al NMR spectrograph that is greater than any other polyhydroxyoxoaluminum cation detectable by 27Al NMR. Also, disclosed are methods of making the antiperspirant active.
Abstract translation: 一种止汗活性组合物，其包含铝盐，所述铝盐（i）的铝与氯化物摩尔比为0.3:1至3:1; 和（ii）具有通过27Al NMR在76ppm处可检测到的聚羟基氧化铝阳离子的种类，其在27Al NMR光谱仪上的相对丰度存在，其大于可通过27Al NMR检测的任何其它聚羟基氧代铝阳离子。 此外，公开了使止汗剂活性的方法。
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公开(公告)号：EP3068422A1
公开(公告)日：2016-09-21
申请号：EP13802151.4
申请日：2013-11-12
Applicant: Colgate-Palmolive Company
Inventor： PAN, Long , YUAN, Shaotang , PAPPAS, Iraklis , VAUGHN, John , MASTERS, James G.
CPC classification number: G01N27/44782 , A61K8/19 , A61K8/26 , A61K8/27 , A61K8/28 , A61K8/44 , A61K2800/58 , A61K2800/74 , A61K2800/805 , A61Q15/00 , D06M13/005
Abstract: Methods of estimating the suitability of a candidate antiperspirant material by measuring the zeta potential of the material.
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公开(公告)号：EP2702007B1
公开(公告)日：2018-11-14
申请号：EP11808786.5
申请日：2011-12-20
Applicant: Colgate-Palmolive Company
Inventor： VAUGHN, John , PAPPAS, Iraklis , PAN, Long
CPC classification number: A61K8/26 , A61K8/19 , A61K8/20 , A61K8/28 , A61K8/42 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01F7/002 , C01F7/56 , C01P2002/86 , C01P2002/87
Abstract: An antiperspirant active composition comprising an aluminum salt, the aluminum salt (i) having an aluminum to chloride molar ratio of 0.3:1 to 3:1; and (ii) having a species of polyhydroxyoxoaluminum cation detectable at 76 ppm by 27Al NMR that is present in a relative abundance on a 27Al NMR spectrograph that is greater than any other polyhydroxyoxoaluminum cation detectable by 27Al NMR. Also, disclosed are methods of making the antiperspirant active.
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公开(公告)号：EP2635353B1
公开(公告)日：2018-05-09
申请号：EP11782333.6
申请日：2011-10-31
Applicant: Colgate-Palmolive Company
Inventor： PAPPAS, Iraklis , VAUGHN, John , PAN, Long
CPC classification number: C01F7/56 , A61K8/26 , A61K8/28 , A61K8/44 , A61K2800/592 , A61K2800/80 , A61Q15/00 , C01F7/002 , C01P2002/86 , C01P2002/87
Abstract: An antiperspirant active composition comprising an aluminum salt, the aluminum salt (i) having an aluminum to chloride molar ratio of 0.3:1 to 3:1; and (ii) exhibiting an 27Al NMR spectrum with a species distribution including at least 90% A130 polyhydroxyoxoaluminum cation as the predominant species detectable by 27Al NMR within the aluminum salt. The composition can optionally include zirconium. Also disclosed are a method of making an antiperspirant active composition and the use of a heating step at elevated temperature to convert Al13 polyhydroxyoxoaluminum cations in the species detectable by 27Al NMR within an aqueous aluminum salt solution into Al30 polyhydroxyoxoaluminum cations in the species detectable by 27Al NMR without increasing a SEC Peak 3 area in the SEC chromatogram of the aluminum salt.
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10.发明公开COMPOSITIONS CONTAINING POLYHYDROXYOXOALUMINUM CATIONS AND MANUFACTURE THEREOF 有权含有聚羟基铝氧烷阳离子的组合物及其制造方法
公开(公告)号：EP2702008A1
公开(公告)日：2014-03-05
申请号：EP11810736.6
申请日：2011-12-20
Applicant: Colgate-Palmolive Company
Inventor： VAUGHN, John , PAPPAS, Iraklis , PAN, Long
CPC classification number: C01F7/026 , A61K8/26 , A61K8/28 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01F7/002 , C01F7/56 , C01P2002/86 , C01P2002/87
Abstract: A composition comprising a polyhydroxyoxoaluminum cation detectable at 76 ppm by
27 Al NMR that is present in a relative abundance on a
27 Al NMR spectrograph that is greater than any other polyhydroxyoxoaluminum cation detectable by
27 Al NMR. Also, disclosed are methods of making the composition.Abstract translation: 包含可通过27Al NMR在76ppm处检测到的聚羟基氧基铝阳离子的组合物，其在27Al NMR光谱仪上的相对丰度比任何其他可通过27Al NMR检测的多羟基铝阳离子都高。 还公开了制造该组合物的方法。
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