Abstract:
PROBLEM TO BE SOLVED: To provide a method of making metal oxide powder by which uniform powders having high BET surface area and narrow particle size distribution can be obtained and suitable for making the metal oxide powder in a range of quantity of kg/hr order. SOLUTION: In the method of making the metal oxide powder having at least 20 m 2 /g BET surface area by reacting aerosol with oxygen in a reaction space at a reaction temperature higher than 700°C and successively separating the resultant powder from a gaseous material, the aerosol is produced by spraying at least one kind of a starting material in a liquid form or a solution and at least one kind of a spray gas using a multi-component nozzle so that the average liquid particle diameter D 30 of the aerosol to the volume is 30-100 μm and the number of aerosol small droplets having a particle diameter larger than 100 μm is ≤10% of the total number of droplets. COPYRIGHT: (C)2006,JPO&NCIPI
Abstract:
금속화합물을포함하는에어로졸은반응기에서화염에도입되어반응기내에서반응하고, 수득된금속산화물분말은가스상물질로부터분리되며, a) 화염은연료가스와함께산소-함유가스 (1)의점화에의해형성되고, b) 에어로졸은하나이상의노즐로분무화가스및 금속화합물을함유하는용액의공동분무화에의해수득되며, c) 분무면적대 반응기단면적의비는 0.2 이상인화염분무열분해에의해금속산화물분말을제조하는방법이개시되어있다.
Abstract:
PROBLEM TO BE SOLVED: To obtain indium - tin - oxide capable of coating on plastics. SOLUTION: This indium - tin - oxide is characterized by having 1 to 200 nm of the average primary particle size, 0.1 to 300 m 2 /g of BET surface area, a cubic crystal of indium oxide, a tetragonal crystal of tin oxide, 0.03 to 0.30 mL/g of mesopore measured by a BJH method, 1.5 to 5.0 mL/g of macropore 50 to 2,000 g/L of the bulk density. This indium - tin - oxide is manufactured by mixing an indium salt solution with a tin salt solution, spraying the mixture, and thermally decomposing the sprayed mixture and used for manufacturing transparent and conductive coatings and coating films. COPYRIGHT: (C)2003,JPO
Abstract:
PROBLEM TO BE SOLVED: To prepare a cerium oxide powder suitable as a component of a dispersion for grinding a semiconductor substrate, easily incorporated and having high stability to precipitation. SOLUTION: The polycrystalline cerium oxide powder in a form of primary particle aggregate has 70-150 m 2 /g specific surface area, 5-20 nm average primary particle diameter and 20-100 nm projected average aggregate diameter. COPYRIGHT: (C)2005,JPO&NCIPI
Abstract:
PROBLEM TO BE SOLVED: To provide a method by which an anhydrous and high-purity sodium sulfide can be obtained. SOLUTION: Hydrous sodium sulfide is heated with an organic solvent incompatible with water at a temperature lower than the melting point of the hydrous sodium sulfide by 10-20 deg.C and the temperature is then slowly raised within the temperature range of 1-10 deg.C and kept at a temperature higher than the melting point of the hydrous sodium sulfide by 10-20 deg.C for 5-15 min to heat the hydrous sodium sulfide to the boiling point of the water-solvent mixture. Water of crystallization is distilled off by azeotropic distillation in a vacuum or under a reduced pressure to dry the hydrous sodium sulfide.
Abstract:
Mixed oxide powder containing indium and tin, with a proportion of indium oxide of between 90 and 98 wt.% and a BET surface area of 40 to 120 m²/g, which is in the form of aggregates having an average circumference of less than 500 nm, consists of at least 95% of an indium oxide phase and displays an oxygen content that is lower than the content that theoretically results from In2O3 and SnO2. It is produced by mixing a solution of an indium compound with a solution of a tin compound, atomising this mixture of solutions, pyrolysing the atomised mixture of solutions in a first zone of a reactor and in a second zone of the reactor, following pyrolysis, adding reducing gases to the pyrolysed mixture at one or more points in a quantity such that overall a reducing atmosphere is established in this second zone, and separating the resulting solid from the waste gases in a further, third zone, in which a reducing atmosphere likewise still prevails. It can be used for the production of transparent, electroconductive paints and coatings.
Abstract:
The invention relates to a powder comprising calcium oxide, silicon dioxide and further calcium compounds, and to the preparation thereof. In addition, a hydraulic binder based on the calcium oxide-containing powder and the use thereof in cement, concrete or mortar form part of the invention.
Abstract:
Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated and oxidized, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein as starting materials, at least one pulverulent metal and at least one metal compound, the metal and the metal component of the metal compound being different and the proportion of metal being at least 80% by weight based on the sum of metal and metal component from metal compound, together with one or more combustion gases, are fed to an evaporation zone of a reactor, where metal and metal compound are evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the starting materials and combustion gases completely.
Abstract:
Process for preparing a metal oxide powder, in which starting materials are evaporated and oxidized, wherein a metal melt in the form of droplets and one or more combustion gases are fed to the evaporation zone of a reactor, where the metal melt is evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the metal and the combustion gases completely.
Abstract:
La invención se relaciona con partículas de óxido de hierro-silicio que comprenden un núcleo y una corteza externa, el núcleo contiene las modificaciones de óxido de hierro maghemita, magnetita y hematita, y la corteza externa consiste sustancialmente o exclusivamente de dióxido de silicio amorfo y para lo cual se comprueba que a) H0.20nm/H0.25nm = 0.2, en donde H0.20nm = brillantez del anillo de difracción de Debye-Scherrer determinada por difracción de electrones con un espaciamiento del plano reticular de 0.20+/-0.02 nm, comprendiendo maghemita y magnetita, y H0.25nm = brillantez del anillo de difracción de Debye-Scherrer determinado por difracción de electrones con un espaciamiento del plano reticular de 0.25+/-0.02 nm, que comprende maghemita, magnetita y hematita, y b) el diámetro del cristalito de la hematita, determinado por difractometría de rayos X, es mayor que 120 nm. Las partículas se producen porque, en una primera zona 1, una mezcla que contiene 0-30 % de la cantidad total de compuestos de silicio, compuestos de hierro, gases combustibles y uno o más gases que contienen oxígeno se enciende y se deja reaccionar y, en una segunda zona, 70-100 % de la cantidad total de compuestos de silicio se añade a esta mezcla de reacción y, en la zona 3, el material sólido se separa de las sustancias gaseosas o vaporosas en la mezcla de reacción. La invención se relaciona además con caucho de silicona que contiene las partículas de óxido de hierro-silicio.