Method for making metal oxide powder
    1.
    发明专利
    Method for making metal oxide powder 审中-公开
    制造金属氧化物粉末的方法

    公开(公告)号:JP2006213591A

    公开(公告)日:2006-08-17

    申请号:JP2005345055

    申请日:2005-11-30

    Abstract: PROBLEM TO BE SOLVED: To provide a method of making metal oxide powder by which uniform powders having high BET surface area and narrow particle size distribution can be obtained and suitable for making the metal oxide powder in a range of quantity of kg/hr order. SOLUTION: In the method of making the metal oxide powder having at least 20 m 2 /g BET surface area by reacting aerosol with oxygen in a reaction space at a reaction temperature higher than 700°C and successively separating the resultant powder from a gaseous material, the aerosol is produced by spraying at least one kind of a starting material in a liquid form or a solution and at least one kind of a spray gas using a multi-component nozzle so that the average liquid particle diameter D 30 of the aerosol to the volume is 30-100 μm and the number of aerosol small droplets having a particle diameter larger than 100 μm is ≤10% of the total number of droplets. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 要解决的问题:提供一种制备金属氧化物粉末的方法,通过该方法可以获得具有高BET表面积和窄粒度分布的均匀粉末,并且适于使金属氧化物粉末的量为kg / 小时订单。 解决方案:在反应温度高于700℃的反应空间中通过气溶胶与氧气反应制备具有至少20m 2 / SP / g BET表面积的金属氧化物粉末的方法中, 并将所得粉末从气态物质中分离出来,通过使用多组分喷嘴将至少一种起始材料以液体形式或溶液喷射至少一种喷雾气体喷射而制成气雾剂, 气溶胶的体积的平均液体粒径D 30 为30-100μm,粒径大于100μm的气溶胶小液滴的数量为液滴总数的10%。 版权所有(C)2006,JPO&NCIPI

    화염 분무 열분해에 의한 금속 산화물 분말의 제조 방법
    2.
    发明公开
    화염 분무 열분해에 의한 금속 산화물 분말의 제조 방법 审中-公开
    火焰喷雾热解法制备金属氧化物粉末的方法

    公开(公告)号:KR20180022845A

    公开(公告)日:2018-03-06

    申请号:KR20187002240

    申请日:2016-06-28

    CPC classification number: C01G1/02 C01B13/34 C01B33/18 C01P2006/12 C01P2006/80

    Abstract: 금속화합물을포함하는에어로졸은반응기에서화염에도입되어반응기내에서반응하고, 수득된금속산화물분말은가스상물질로부터분리되며, a) 화염은연료가스와함께산소-함유가스 (1)의점화에의해형성되고, b) 에어로졸은하나이상의노즐로분무화가스및 금속화합물을함유하는용액의공동분무화에의해수득되며, c) 분무면적대 반응기단면적의비는 0.2 이상인화염분무열분해에의해금속산화물분말을제조하는방법이개시되어있다.

    Abstract translation: 含金属化合物的气溶胶引入到反应器中的火焰,在反应器中的反应,将得到的金属氧化物粉末从气态物质中分离出来,一个)的氧与燃料气体含有气体逐火焰(1)uijeom化学 形成,并且,b)将气溶胶是由含有一个或多个喷嘴的气体和金属的化合物的雾化溶液的共雾化获得的,c)中的喷射区域的用于反应器的横截面面积的金属氧化物粉末由火焰喷雾热解比0.2的比例 被披露。

    Indium - tin - oxide, method for manufacturing the same and the use
    3.
    发明专利
    Indium - tin - oxide, method for manufacturing the same and the use 审中-公开
    氧化铟锡,其制造方法和使用方法

    公开(公告)号:JP2003063823A

    公开(公告)日:2003-03-05

    申请号:JP2002177650

    申请日:2002-06-18

    Abstract: PROBLEM TO BE SOLVED: To obtain indium - tin - oxide capable of coating on plastics.
    SOLUTION: This indium - tin - oxide is characterized by having 1 to 200 nm of the average primary particle size, 0.1 to 300 m
    2 /g of BET surface area, a cubic crystal of indium oxide, a tetragonal crystal of tin oxide, 0.03 to 0.30 mL/g of mesopore measured by a BJH method, 1.5 to 5.0 mL/g of macropore 50 to 2,000 g/L of the bulk density. This indium - tin - oxide is manufactured by mixing an indium salt solution with a tin salt solution, spraying the mixture, and thermally decomposing the sprayed mixture and used for manufacturing transparent and conductive coatings and coating films.
    COPYRIGHT: (C)2003,JPO

    Abstract translation: 要解决的问题:获得能够在塑料上涂覆的铟锡氧化物。 解决方案:该铟锡氧化物的特征在于具有1至200nm的平均一次粒径,0.1至300m 2 / g的BET表面积,立方晶体的氧化铟,四方晶体的氧化锡 ,通过BJH法测量的0.03〜0.30mL / g的中孔,1.5〜5.0mL / g的大孔50〜2000g / L的体积密度。 该铟锡氧化物是通过将铟盐溶液与锡盐溶液混合,喷雾该混合物并将该喷射混合物热分解并用于制造透明导电涂层和涂膜而制造的。

    METHOD FOR PRODUCING ANHYDROUS AND HIGH-PURITY SODIUM SULFIDE

    公开(公告)号:JP2001158608A

    公开(公告)日:2001-06-12

    申请号:JP2000354680

    申请日:2000-11-21

    Applicant: DEGUSSA

    Abstract: PROBLEM TO BE SOLVED: To provide a method by which an anhydrous and high-purity sodium sulfide can be obtained. SOLUTION: Hydrous sodium sulfide is heated with an organic solvent incompatible with water at a temperature lower than the melting point of the hydrous sodium sulfide by 10-20 deg.C and the temperature is then slowly raised within the temperature range of 1-10 deg.C and kept at a temperature higher than the melting point of the hydrous sodium sulfide by 10-20 deg.C for 5-15 min to heat the hydrous sodium sulfide to the boiling point of the water-solvent mixture. Water of crystallization is distilled off by azeotropic distillation in a vacuum or under a reduced pressure to dry the hydrous sodium sulfide.

    NANOSCALE INDIUM TIN MIXED OXIDE POWDER
    6.
    发明申请
    NANOSCALE INDIUM TIN MIXED OXIDE POWDER 审中-公开
    纳米铟锡混合氧化物粉末

    公开(公告)号:WO2004080144A3

    公开(公告)日:2004-11-04

    申请号:PCT/EP2004002283

    申请日:2004-03-05

    Abstract: Mixed oxide powder containing indium and tin, with a proportion of indium oxide of between 90 and 98 wt.% and a BET surface area of 40 to 120 m²/g, which is in the form of aggregates having an average circumference of less than 500 nm, consists of at least 95% of an indium oxide phase and displays an oxygen content that is lower than the content that theoretically results from In2O3 and SnO2. It is produced by mixing a solution of an indium compound with a solution of a tin compound, atomising this mixture of solutions, pyrolysing the atomised mixture of solutions in a first zone of a reactor and in a second zone of the reactor, following pyrolysis, adding reducing gases to the pyrolysed mixture at one or more points in a quantity such that overall a reducing atmosphere is established in this second zone, and separating the resulting solid from the waste gases in a further, third zone, in which a reducing atmosphere likewise still prevails. It can be used for the production of transparent, electroconductive paints and coatings.

    Abstract translation: 含有铟和锡的混合氧化物粉末,氧化铟的比例为90-98重量%,BET表面积为40-120米2 /克,其平均周长小于500的聚集体形式 nm由至少95%的氧化铟相组成,并显示出低于理论上由In 2 O 3和SnO 2得到的含量的氧含量。 它是通过将铟化合物溶液与锡化合物溶液混合,将该溶液混合物雾化,在反应器的第一区热解溶液的雾化混合物并在反应器的第二区中, 在一个或多个点处向所述热解混合物中加入还原气体的量使得总体上在该第二区域中建立还原气氛,并且在另一个第三区域中将所得固体与废气分离,其中还原气氛同样地 仍然占上风。 它可用于生产透明导电油漆和涂料。

    PARTICULAS DE OXIDO DE HIERRO-SILICIO CON VELOCIDAD DE CALENTAMIENTO MEJORADA EN UN CAMPO MAGNETICO Y ELECTROMAGNETICO ALTERNADO.

    公开(公告)号:MX2013008898A

    公开(公告)日:2013-08-21

    申请号:MX2013008898

    申请日:2011-12-07

    Abstract: La invención se relaciona con partículas de óxido de hierro-silicio que comprenden un núcleo y una corteza externa, el núcleo contiene las modificaciones de óxido de hierro maghemita, magnetita y hematita, y la corteza externa consiste sustancialmente o exclusivamente de dióxido de silicio amorfo y para lo cual se comprueba que a) H0.20nm/H0.25nm = 0.2, en donde H0.20nm = brillantez del anillo de difracción de Debye-Scherrer determinada por difracción de electrones con un espaciamiento del plano reticular de 0.20+/-0.02 nm, comprendiendo maghemita y magnetita, y H0.25nm = brillantez del anillo de difracción de Debye-Scherrer determinado por difracción de electrones con un espaciamiento del plano reticular de 0.25+/-0.02 nm, que comprende maghemita, magnetita y hematita, y b) el diámetro del cristalito de la hematita, determinado por difractometría de rayos X, es mayor que 120 nm. Las partículas se producen porque, en una primera zona 1, una mezcla que contiene 0-30 % de la cantidad total de compuestos de silicio, compuestos de hierro, gases combustibles y uno o más gases que contienen oxígeno se enciende y se deja reaccionar y, en una segunda zona, 70-100 % de la cantidad total de compuestos de silicio se añade a esta mezcla de reacción y, en la zona 3, el material sólido se separa de las sustancias gaseosas o vaporosas en la mezcla de reacción. La invención se relaciona además con caucho de silicona que contiene las partículas de óxido de hierro-silicio.

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