公开(公告)号：EP3047260B1

公开(公告)日：2019-01-09

申请号：EP14786810.3

申请日：2014-09-18

Applicant: FLSmidth A/S

Inventor： BRUZENAK, Lukas ,  MELEG, Vladimir

IPC: G01N1/28 ,  G01N23/2005

公开(公告)号：EP3142928A1

公开(公告)日：2017-03-22

申请号：EP15725120.8

申请日：2015-05-13

Applicant: FLSmidth A/S

Inventor： MELEG, Vladimir ,  OKÉNKA, Miroslav

IPC: B65B37/20 ,  B65B1/36 ,  B65B1/38 ,  G01F13/00 ,  G01F11/18

CPC classification number: B65B37/20 ,  B08B5/02 ,  B08B5/04 ,  B08B9/023 ,  B65B2210/08 ,  G01F11/18

Abstract: Disclosed, is a dosing apparatus [1] which is configured to provide a predetermined amount of material from one vessel to another vessel. The dosing apparatus [1] may comprise a dosing head having a dosing tube [9] and a dosing rod [12] which is movable within said dosing tube [9]. The dosing rod [12] may comprise a dosing chamber [10] which may be filled with a predetermined amount of material. Also described, is a method of dosing which utilizes the dosing apparatus [1] disclosed. In some embodiments, the method may comprise providing a dosing apparatus [1], extending the dosing rod [12] with respect to the dosing tube [9], loading the dosing chamber [10] with a predetermined amount of material, and, retracting the dosing rod [12] with respect to the dosing tube [9] to close the dosing chamber [10]. One or more air and/or liquid cleaning steps may be employed, wherein a cleaning unit [17, 117] may be utilized to clean the dosing rod [12] and/or a funnel [4].

Abstract translation: 公开了一种配量装置[1]，其被配置为从一个容器向另一个容器提供预定量的材料。 计量装置[1]可以包括具有计量管[9]和计量管[12]的计量头，该计量管可在所述计量管[9]内移动。 计量杆[12]可以包括可以用预定量的材料填充的计量室[10]。 还描述了使用所公开的计量装置[1]的剂量方法。 在一些实施例中，该方法可以包括提供相对于计量管[9]延伸计量杆[12]的计量装置[1]，将计量腔[10]装入预定量的材料， 计量杆[12]相对于计量管[9]关闭给药室[10]。 可以采用一个或多个空气和/或液体清洁步骤，其中可以使用清洁单元[17,117]来清洁计量棒[12]和/或漏斗[4]。

公开(公告)号：EP3047260A2

公开(公告)日：2016-07-27

申请号：EP14786810.3

申请日：2014-09-18

Applicant: FLSmidth A/S

Inventor： BRUZENAK, Lukas ,  MELEG, Vladimir

IPC: G01N23/20 ,  G01N1/28

CPC classification number: G01N23/2005 ,  G01N1/286 ,  G01N2223/056 ,  G01N2223/307 ,  G01N2223/312 ,  G01N2223/616

Abstract: Disclosed, is a sample preparation apparatus which is configured to prepare a material sample suitable for X-ray diffraction. The apparatus comprises a dished sample holder bottom configured to fit within an annular sample holder. The dished sample holder bottom has a concave dished surface which is adapted to distribute sample material under pressing forces. A method of preparing a material sample suitable for X-ray diffraction is also disclosed. The method comprises dosing a dished sample holder bottom which is configured to fit within an annular sample holder with sample material, wherein the dished sample holder bottom preferably has a concave dished surface which is adapted to distribute sample material under pressing forces.

公开(公告)号：WO2015040123A2

公开(公告)日：2015-03-26

申请号：PCT/EP2014/069917

申请日：2014-09-18

Applicant: FLSMIDTH A/S

Inventor： BRUZENAK, Lukas ,  MELEG, Vladimir

IPC: G01N23/20

CPC classification number: G01N23/2005 ,  G01N1/286 ,  G01N2223/056 ,  G01N2223/307 ,  G01N2223/312 ,  G01N2223/616

Abstract: Disclosed, is a sample preparation apparatus (6B) which is configured to prepare a material sample (900') suitable for X-ray diffraction. The apparatus (6B) comprises a dished sample holder bottom (500) configured to fit within an annular sample holder (400). The dished sample holder bottom (500) has a concave dished surface (501) which is adapted to distribute sample material (900) under pressing forces. A method of preparing a material sample (900') suitable for X-ray diffraction is also disclosed. The method comprises dosing a dished sample holder bottom (500) which is configured to fit within an annular sample holder (400) with sample material (900), wherein the dished sample holder bottom (500) preferably has a concave dished surface (501) which is adapted to distribute sample material (900) under pressing forces. A new leveling device design tool (Fig 12) is also disclosed. The leveling tool minimizes surface contact effects by penetrating the core of the sample and providing random sample grain orientation while evenly distributing material throughout the sample holder bottom. The sample material (900) is lightly pressed, and sample material (900) is distributed within the dished sample holder bottom (500) by virtue of the concave dished surface (501).

Abstract translation: 公开了一种样品制备设备（6B），其被配置为制备适用于X射线衍射的材料样品（900'）。 设备（6B）包括配置成装配在环形样品保持器（400）内的碟形样品保持器底部（500）。 碟形样品容器底部（500）具有适于在压力下分配样品材料（900）的凹形碟形表面（501）。 还公开了一种制备适用于X射线衍射的材料样品（900'）的方法。 该方法包括给配置样品材料（900）的环形样品保持器（400）内装配碟形样品保持器底部（500），其中碟形样品保持器底部（500）优选具有凹形碟形表面（501） 其适于在压力下分配样品材料（900）。 还公开了一种新的校平装置设计工具（图12）。 通过穿透样品核心并提供随机样品晶粒取向，同时均匀分布材料到整个样品架底部，该找平工具将表面接触效应降至最低。 轻轻按压样品材料（900），并且样品材料（900）借助凹形碟形表面（501）分布在碟形样品保持器底部（500）内。

公开(公告)号：WO2015173749A1

公开(公告)日：2015-11-19

申请号：PCT/IB2015/053529

申请日：2015-05-13

Applicant: FLSMIDTH A/S

Inventor： MELEG, Vladimir ,  OKÉNKA, Miroslav

IPC: B65B37/20 ,  B65B1/36 ,  B65B1/38 ,  G01F13/00 ,  G01F11/18

CPC classification number: B65B37/20 ,  B08B5/02 ,  B08B5/04 ,  B08B9/023 ,  B65B2210/08 ,  G01F11/18

Abstract: Disclosed, is a dosing apparatus [1] which is configured to provide a predetermined amount of material from one vessel to another vessel. The dosing apparatus [1] may comprise a dosing head having a dosing tube [9] and a dosing rod [12] which is movable within said dosing tube [9]. The dosing rod [12] may comprise a dosing chamber [10] which may be filled with a predetermined amount of material. Also described, is a method of dosing which utilizes the dosing apparatus [1] disclosed. In some embodiments, the method may comprise providing a dosing apparatus [1], extending the dosing rod [12] with respect to the dosing tube [9], loading the dosing chamber [10] with a predetermined amount of material, and, retracting the dosing rod [12] with respect to the dosing tube [9] to close the dosing chamber [10]. One or more air and/or liquid cleaning steps may be employed, wherein a cleaning unit [17, 117] may be utilized to clean the dosing rod [12] and/or a funnel [4].

Abstract translation: 公开了一种配量装置[1]，其被配置为从一个容器向另一个容器提供预定量的材料。 计量装置[1]可以包括具有计量管[9]和计量杆[12]的计量头，该计量管可在所述计量管[9]内移动。 计量杆[12]可以包括可以用预定量的材料填充的计量室[10]。 还描述了一种使用所公开的给药装置[1]的剂量方法。 在一些实施例中，该方法可以包括提供相对于计量管[9]延伸计量杆[12]的计量装置[1]，将计量腔[10]装入预定量的材料， 计量杆[12]相对于计量管[9]关闭计量室[10]。 可以采用一个或多个空气和/或液体清洁步骤，其中可以使用清洁单元[17,117]来清洁计量杆[12]和/或漏斗[4]。

公开(公告)号：WO2016185023A1

公开(公告)日：2016-11-24

申请号：PCT/EP2016/061438

申请日：2016-05-20

Applicant: FLSMIDTH A/S

Inventor： KRSEK, Michal ,  MELEG, Vladimir

IPC: G01N1/28 ,  G01N23/20

CPC classification number: G01N1/286 ,  G01N23/20025

Abstract: A punch (1100) for use in a sample preparation apparatus configured to prepare a sticky material sample suitable for X-ray analysis comprising an upper surface part (1103) and a lower surface part (1104) having an outer flat ring (1101) and a pressing surface part (1102); wherein at least a portion of the punch is coated with a diamond-like carbon coating configured to reduce the amount of sticky material residue on the punch after preparation of the sticky material sample. Also disclosed are methods for preparing a non-contaminated material sample suitable for X-ray analysis.

Abstract translation: 一种用于样品制备装置的冲头（1100），其被配置为制备适于X射线分析的粘性材料样品，所述样品制备装置包括上表面部分（1103）和具有外平坦环（1101）的下表面部分（1104）和 按压表面部分（1102）; 其中所述冲头的至少一部分涂覆有金刚石状碳涂层，其被配置为在制备所述粘性材料样品之后减少所述冲头上的粘性材料残留物的量。 还公开了制备适合于X射线分析的非污染材料样品的方法。