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公开(公告)号:BR8004137A
公开(公告)日:1981-03-24
申请号:BR8004137
申请日:1980-07-03
Applicant: HOECHST AG
Inventor: SCHRODTER K , GRADL R , EHLERS K
Abstract: The present invention relates to a mixer/settler-type apparatus for continuous liquid-liquid extraction. The apparatus is comprised of a separating vessel with an inclined bottom portion and an agitator-provided mixing vessel. The mixing vessel is tightly mounted to the inclined bottom portion of the separating vessel, the latter being formed with an upper outlet and a lower outlet and having a level indicator LI for determining phase boundary surface area installed therein. The lower outlet is passed through the separating vessel near its lowermost level and the upper outlet is passed therethrough near its upper end. The level indicator LI is connected to a regulator giving adjustment instructions to a structural element permitting the phase boundary surface area to be established in the separating vessel, distinctly above the upper end of the mixing vessel.
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公开(公告)号:ZA81793B
公开(公告)日:1982-03-31
申请号:ZA81793
申请日:1981-02-06
Applicant: HOECHST AG
Inventor: HEYMER G , SCHIMMEL G , GRADL R
Abstract: The present invention relates to a process for recovering uranium from raffinate which is obtained by extracting phosphoric acid from a uranium-containing wet-process phosphoric acid with the aid of organic extractants and separating the resulting organic phosphoric acid extract from residue not taken up by the extract. To this end, the raffinate residue is subjected to thermal treatment and thereby freed from dissolved or emulsified residual extractant. Next, the raffinate is treated with a water-immiscible solvent to extract the uranium, and the extracted uranium is separated from the undissolved raffinate portion.
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公开(公告)号:ZA8003998B
公开(公告)日:1981-07-29
申请号:ZA8003998
申请日:1980-07-03
Applicant: HOECHST AG
Inventor: GRADL R , EHLERS K , SCHROEDTER K
CPC classification number: C22B3/02 , B01D11/0457 , B01D11/0484 , C01B25/462 , C22B3/0005 , Y02P10/234
Abstract: The present invention relates to a mixer/settler-type apparatus for continuous liquid-liquid extraction. The apparatus is comprised of a separating vessel with an inclined bottom portion and an agitator-provided mixing vessel. The mixing vessel is tightly mounted to the inclined bottom portion of the separating vessel, the latter being formed with an upper outlet and a lower outlet and having a level indicator LI for determining phase boundary surface area installed therein. The lower outlet is passed through the separating vessel near its lowermost level and the upper outlet is passed therethrough near its upper end. The level indicator LI is connected to a regulator giving adjustment instructions to a structural element permitting the phase boundary surface area to be established in the separating vessel, distinctly above the upper end of the mixing vessel.
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公开(公告)号:BR8007397A
公开(公告)日:1981-05-26
申请号:BR8007397
申请日:1980-11-13
Applicant: HOECHST AG
Inventor: EHLERS K , GRADL R , SCHRODTER K
IPC: C01B25/234 , C01B25/237 , C01B25/46
Abstract: The invention relates to a process for the purification of wet-processed phosphoric acid with the aid of organic solvents which are immiscible or only partially miscible with water, the sulfate ions being removed by addition of barium compounds. The purification is carried out in an n-stage extraction installation, where n is equal to or greater than 5. The barium compound is added to the phosphoric acid to be purified, and the resulting mixture is fed to the top of the extraction installation, in which the organic solvent phase is dispersed in the aqueous phase. The sulfuric acid is led in counter-current fashion to the phosphoric acid by adding it to one of the stages n=4 to at most n-1.
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公开(公告)号:BR8004138A
公开(公告)日:1981-01-21
申请号:BR8004138
申请日:1980-07-03
Applicant: HOECHST AG
Inventor: EHLERS K , GRADL R , SCHEIBITZ W , SCHRODTER K
IPC: C01B25/234 , C01B25/46
Abstract: The invention relates to the decontamination of wet-processed phosphoric acid with the use of organic solvents in a plurality of extraction zones, of which each is comprised of a mixing zone and a separating zone, the solvent being immiscible or partially miscible with water. Resulting organic phase and the aqueous phase are contacted countercurrently with respect to one another, the organic solvent phase being dispersed in the aqueous phase. To this end, the invention provides for the aqueous phase to be admitted to the mixing zone at the onset of the extraction, and for organic phase and aqueous phase to be continuously admitted in a volume ratio of at least 2.5:1 to the respective extracting zones in an overall quantity sufficient to provide, in the mixing zones of the extraction zones, a volume ratio of organic phase to aqueous phase of at most 1:1, which is maintained therein.
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公开(公告)号:ZA8100793B
公开(公告)日:1982-03-31
申请号:ZA8100793
申请日:1981-02-06
Applicant: HOECHST AG
Inventor: HEYMER G , SCHIMMEL G , GRADL R
CPC classification number: C22B60/026 , Y02P10/212
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公开(公告)号:ZA807016B
公开(公告)日:1981-11-25
申请号:ZA807016
申请日:1980-11-13
Applicant: HOECHST AG
Inventor: SCHROEDTER K , EHLERS K , GRADL R
IPC: C01B25/237 , C01B25/46 , C01B25/234 , C01B
Abstract: The invention relates to a process for the purification of wet-processed phosphoric acid with the aid of organic solvents which are immiscible or only partially miscible with water, the sulfate ions being removed by addition of barium compounds. The purification is carried out in an n-stage extraction installation, where n is equal to or greater than 5. The barium compound is added to the phosphoric acid to be purified, and the resulting mixture is fed to the top of the extraction installation, in which the organic solvent phase is dispersed in the aqueous phase. The sulfuric acid is led in counter-current fashion to the phosphoric acid by adding it to one of the stages n=4 to at most n-1.
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公开(公告)号:ZA801407B
公开(公告)日:1981-04-29
申请号:ZA801407
申请日:1980-03-11
Applicant: HOECHST AG
Inventor: GRADL R , SCHROEDTER K , EHLERS K , SCHEIBITZ W
IPC: C02F1/58 , A62D3/36 , A62D101/45 , C01B25/234 , C01B25/46 , C02F11/00 , C02F101/10 , C02F101/20 , C02F101/22 , C02F103/34 , C01B
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公开(公告)号:BR8001427A
公开(公告)日:1980-11-11
申请号:BR8001427
申请日:1980-03-11
Applicant: HOECHST AG
Inventor: SCHRODTER K , EHLERS K , GRADL R , SCHEIBITZ W
IPC: C02F1/58 , A62D3/36 , A62D101/45 , C01B25/234 , C01B25/46 , C02F11/00 , C02F101/10 , C02F101/20 , C02F101/22 , C02F103/34 , B01D11/04
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公开(公告)号:ZA8007016B
公开(公告)日:1981-11-25
申请号:ZA8007016
申请日:1980-11-13
Applicant: HOECHST AG
Inventor: SCHROEDTER K , EHLERS K , GRADL R
IPC: C01B25/234 , C01B25/46 , C01B
CPC classification number: C01B25/462 , C01B25/461
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