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公开(公告)号:SE316472B
公开(公告)日:1969-10-27
申请号:SE668565
申请日:1965-05-21
Applicant: HOECHST AG
IPC: C07C409/34 , C07C73/10
Abstract: Peroxydicarbonates of the general formula R-O-CO-O-O-CO-O-R in which R is an alkyl, chloroalkyl or alkenyl group of 1-9 carbon atoms are prepared in a continuous process by reacting a chloroformic acid ester of the general formula R-O-CO-Cl with H2O2 and an acqueous solution of an alkali metal hydroxide at -10 DEG to 30 DEG C., wherein the major part of the reaction is effected in a first reaction zone at a pH of 8-14 with intimate mixing, the dispersion obtained is transferred to an after-reaction zone in which the reaction proceeds to completion and the peroxydicarbonate obtained is taken up in a hydrogen-free, halogen-containing solvent or a hydrocarbon or terpene that is liquid under normal conditions.