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    Process for dyeing and printing textile materials containing acid groups with basic dyestuffs
    1.
    发明授权
    Process for dyeing and printing textile materials containing acid groups with basic dyestuffs 失效
    含有基础试剂的含酸组织的染色和印刷纺织材料的工艺

    公开(公告)号：US3776691A

    公开(公告)日：1973-12-04

    申请号：US3776691D

    申请日：1972-04-21

    Applicant: HOECHST AG

    Inventor： NEEB R ,  MUNDLOS E ,  MOHR R

    IPC: C09B17/04 ,  D06P3/76

    CPC classification number: C09B17/04 ,  Y10S8/927

    Abstract: Process for the dyeing and printing of textile materials made from polymers or copolymers of acrylonitrile by using dyestuffs of the general formula

    IN WHICH R1 represents an alkyl, aralkyl, aryl or heterocyclic radical which may be substituted R2 represents hydrogen or an alkyl or aralkyl radical which may be substituted, Q represents an aromatic or heterocylic radical which may be condensed with the benzene nucleus b, and X represents an anion and the benzene radicals a and b as well as the radical Q may contain further non-ionogenic substituents. The dyeings and prints thus obtained show a good fastness to light, wet processing, washing, fulling, over-dyeing, to chlorine, to perspiration and to carbonizing as well to decatizing, steaming, ironing, rubbing and to solvents.

    Abstract translation: 由丙烯腈的聚合物或共聚物制成的纺织材料的染色和印花方法通过使用通式为I的染料，其中R 1表示可被取代的烷基，芳烷基，芳基或杂环基，R 2表示氢或烷基或芳烷基， 可以被取代，Q表示可以与苯核b缩合的芳族或杂环基团，X表示阴离子，苯基a和b以及基团Q可以含有另外的非离子型取代基。 由此获得的染色和印花显示出良好的耐光牢度，湿法加工，洗涤，饱和，过度染色，氯化，排汗和碳化，以及脱脂，蒸，熨烫，摩擦和溶剂。

    Basic oxazine dyestuffs
    2.
    发明授权
    Basic oxazine dyestuffs 失效
    基本氧化INE。

    公开(公告)号：US3806504A

    公开(公告)日：1974-04-23

    申请号：US21261871

    申请日：1971-12-27

    Applicant: HOECHST AG

    Inventor： MOHR R ,  MUNDLOS E ,  OSTERMEIER J ,  HERZ L ,  NEEB R

    IPC: C09B19/00 ,  C07D87/50

    CPC classification number: C09B19/00 ,  Y10S8/927

    Abstract: BASE OXAZINE DYESTUFFS OF THE FORMULA I

    2-(R-O-),3-(R1-N(+)(-R2)=),7-(R3-N(-R4)-)-3H-PHENOXAZINE

    X(-)

    IN WHICH R STANDS FOR A LOWER ALKYL GROUP WHICH MAY BE SUBSTITUTED, R1 AND R2 EACH STANDS FOR A HYDROGEN ATOM OR A LOWER ALKYL GROUP WHICH MAY BE SUBSTITUTED AND WHICH MAY FROM TOGETHER WITH THE NITROGEN ATOM ALSO A HETEROCYCLIC RADICAL, R3 STANDS FOR A HYDROGEN ATOM OR A LOWER ALKYL GROUP WHICH MAY BE SUBSTITUTED, R4 STANDS FOR A HYDROGEN ATOM, A LOWER ALKYL GROUP WHICH MAY BE SUBSTITUTED, AN ARYL GROUP WHICH MAY BE SUBSTITUTED, OR TOGETHER WITH THE NITROGEN ATOM AND R3 OR THE BENZENE NUCLEUS R4 MAY FORM A HETEROCYCLIC RADICAL, AND X STANDS FOR AN ANION, AND THE BENZENE NUCLEUS A MAY CARRY FURTHER NONIONIC SUBSTITUTENTS OR A FUSED BENZENE NUCLEUS. THE NOVEL DYESTUFFS ARE SUITABLE FOR THE DYEING OR PRINTING OF TANNINED CELLULOSE FIBERS, SILK, LEATHER OR FULLY SYNTHETIC FIBERS, SUCH AS ACETATE RAYON, POLYAMIDE FIBERS OR ACID-MODIFIED POLYAMIDE OR POLYESTER FIBERS, ESPECIALLY OF FIBERS CONTAINING POLYACRYLONITRILE OR POLYVINYLIDENE CYANIDE. THE DYEINGS PRODUCED ON THESE FIBERS ARE MOSTLY VERY BRIGHT AND HAVE A GOOD TINCTORIAL STRENGTH AS WELL AS, IN GENERAL, GOOD FASTENESS PROPERTIES TO LIGHT AND WET PROCCROSS-DYEING, CARBONIZING, TO THE ACTION OF CHLORINE AND TO PERSPIRATION.

    Process for the dyeing or printing of textile materials made from polymers or copolymers of acrylonitrile
    3.
    发明授权
    Process for the dyeing or printing of textile materials made from polymers or copolymers of acrylonitrile 失效
    丙烯腈聚合物或共聚物对纺织材料进行染色或印花的方法

    公开(公告)号：US3713770A

    公开(公告)日：1973-01-30

    申请号：US3713770D

    申请日：1971-01-20

    Applicant: HOECHST AG

    Inventor： LOHE K ,  MUNDLOS E ,  MOHR R

    IPC: C09B11/24 ,  C09B11/26 ,  D06P3/70

    CPC classification number: C09B11/26 ,  C09B11/24 ,  Y10S8/927

    Abstract: Process for the dyeing and printing of textile materials made from polymers or copolymers of acrylonitrile by using dyestuffs of the general formula

    WHEREIN R1, R2, and R3 each stands for a hydrogen atom or an optionally substituted lower alkyl group, Z represents a carboxylic ester group, Q stands for an aromatic or heterocyclic radical bound or not bound to the benzene nucleus b, X represents an anion, and wherein each benzene nucleus a or b or the radical Q may optionally be substituted by non-ionic substituents, and which dyeings and prints show very clear and brilliant shades and have good fastness properties.

    Abstract translation: 通过使用通式为R 1，R 2和R 3的染料的丙烯腈的聚合物或共聚物制造的纺织材料的染色和印刷方法各代表氢原子或任选取代的低级烷基，Z表示羧酸酯基 Q表示与苯环b结合或未结合的芳族或杂环基团，X表示阴离子，其中每个苯核a或b或基团Q可任选被非离子取代基取代，并且其染色和 印刷品显示非常清晰和辉煌的色调并具有良好的牢度性能。

    8.
    发明专利
    未知

    公开(公告)号：DK248275A

    公开(公告)日：1975-12-05

    申请号：DK248275

    申请日：1975-06-03

    Applicant: HOECHST AG

    Inventor： BACHMANN W ,  GNABS C ,  JANECKA K ,  MUNDLOS E ,  PAPENFUHS T ,  WAESE G

    IPC: C07C65/11 ,  C07C51/00 ,  C07C51/43 ,  C07C67/00 ,  C07C

    Abstract: An improved process for isolating 2-hydroxynaphthalenecarboxylic acids from reaction mixtures of the alkali metal salts of the 2-hydroxynaphthalene with carbon dioxide had been found which comprises diluting with water the reaction mixture which contains the di-alkali metal salt of 2-hydroxynaphthalenecarboxylic acid and 2-hydroxynaphthalene, while keeping the mixture at a temperature of at least 80 DEG C, then adjusting the pH-value to about 6 to 7 by means of aqueous mineral acid, separating the lower phase at at least 80 DEG C, cooling the upper phase to about 15 DEG to 25 DEG C, separating the 2-hydroxynaphthalene, then adjusting the pH-value to about 1 to 2 by means of aqueous mineral acid and isolating the separated 2-hydroxynaphthalenecarboxylic acid. By this novel process, work intensive operations, expensive technical apparatuses which are suspectible to repairs, solvents which do not participate directly in the reaction and therewith complicated regenerations, as known from the present art, are completely avoided. It permits clear and very easy separation of the reaction products at only one and the same stage in the process and allows in advantageous manner continuous operation.

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