1.
    发明专利
    未知

    公开(公告)号:DE59007129D1

    公开(公告)日:1994-10-20

    申请号:DE59007129

    申请日:1990-10-23

    Applicant: HOECHST AG

    Abstract: In the esterification of aliphatic C2-C6-carboxylic acids with aliphatic C1-C4-alcohols, the ester formed is distilled off azeotropically together with the water of reaction. After being separated from the water of reaction in a separation cooler, the ester phase is freed from entrained acid by scrubbing with water, and water and alcohol are then removed by distilling off a small portion of the ester. In this manner, no salt-containing waste water is formed. The ester is obtained in very good yield and free of acid and alcohol.

    2.
    发明专利
    未知

    公开(公告)号:DE3935470A1

    公开(公告)日:1991-05-02

    申请号:DE3935470

    申请日:1989-10-25

    Applicant: HOECHST AG

    Abstract: In the esterification of aliphatic C2-C6-carboxylic acids with aliphatic C1-C4-alcohols, the ester formed is distilled off azeotropically together with the water of reaction. After being separated from the water of reaction in a separation cooler, the ester phase is freed from entrained acid by scrubbing with water, and water and alcohol are then removed by distilling off a small portion of the ester. In this manner, no salt-containing waste water is formed. The ester is obtained in very good yield and free of acid and alcohol.

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