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    1.
    发明专利
    未知

    公开(公告)号：DE3246416A1

    公开(公告)日：1984-06-20

    申请号：DE3246416

    申请日：1982-12-15

    Applicant: HOECHST AG

    Inventor： GRADL REINHARD DIPL CHEM DR ,  ROSZINSKI HILMAR DIPL CHEM DR

    IPC: C01B25/01 ,  C01B25/234 ,  C01B25/46

    Abstract: The disclosure relates to a process for purifying crude, concentrated wet-processed phosphoric acid. To this end, the disclosure provides: (a) for the organic solvent to be mixed with the starting product in a ratio by volume of more than 4:1 to effect in a single process step the extraction-from the crude wet-processed phosphoric acid-of a quantity of phosphoric acid necessary for 40 to 70 weight % of the P2O5 used to go into the organic phase, and for the resulting aqueous phosphoric acid raffinate to contain at most 28-32 weight % P2O5, and for the organic phosphoric acid solution to be separated from the phosphoric acid raffinate; (b) for the separated organic phosphoric acid solution to be scrubbed with a quantity of scrubbing solution corresponding at most to 5% of the volume of the phosphoric acid solution; for the scrubbing solution to be recycled into stage (a), and for purified phosphoric acid and phosphate salt solution, respectively, to be recovered in known manner from the scrubbed phosphoric acid solution; (c) for the aqueous phosphoric acid raffinate produced in stage (a) to be neutralized, if desired, after prior removal of residual solvent, for it to be subjected to treatment with an alkaline agent with the resultant formation of a purified phosphate salt solution and precipitation of a so-called neutralization sludge, and (d) for said neutralization sludge and simultaneously obtained alkali metal phosphate solution to be separated from each other, for the sludge to be mixed with finely ground phosphate ore, and for the mixture to be made into phosphate pellets for use in electrothermal phosphorus production.

    3.
    发明专利
    未知

    公开(公告)号：DE4106527A1

    公开(公告)日：1992-09-03

    申请号：DE4106527

    申请日：1991-03-01

    Applicant: HOECHST AG

    Inventor： DOPPELFELD WILHELM PETER ,  PIEPER WERNER DIPL CHEM DR ,  GIECHAU WILHELM ,  ROSZINSKI HILMAR DIPL CHEM DR

    IPC: C02F3/20

    Abstract: A device is described for introducing gas into waste waters in a gas treatment tank equipped with horizontal gas treatment boxes arranged in parallel next to each other and at a distance to each other, in the upper sides of which gas outlet orifices are arranged and the lower sides of which are open, which device is characterised in that movable rotary bodies are arranged in the gas outlet orifices 13 of the gas treatment boxes 14 and the gas outlet orifices 13 in a known manner each have at the bottom a central countersinking 12 enclosing an angle alpha of, for example, 90 to 180 DEG C and the remaining residual wall thickness 15 of the gas outlet orifice 13 of each countersinking 12 is 0.5 to 2 mm. In this case, the rotary bodies according to the invention can comprise a head part 1 and foot part 3, which are connected to a neck part 2. The head part can comprise two loops 4 and 4', the axis 8 of the loops 4 and 4' being vertical to the axis 7 of the neck part 2 and the surface of the loops 4 and 4' is inclined at an angle beta of preferably 30 to 60 DEG about the axis 8, and the foot part 3 can comprise two bows 6 and 6', which are connected to the neck part 2 and which at the neck part 2 form an angle gamma of, for example, 90 to 180 DEG to each other.

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