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    Water-insoluble azlactone dyestuffs and process for preparing them
    1.
    发明授权
    Water-insoluble azlactone dyestuffs and process for preparing them 失效
    水不溶性AZLACTONE DYESTUFFS及其制备方法

    公开(公告)号：US3847909A

    公开(公告)日：1974-11-12

    申请号：US36341673

    申请日：1973-05-24

    Applicant: HOECHST AG

    Inventor： SCHICKFLUSS R ,  STECKELBERG W

    IPC: C09B23/00 ,  C09B23/01 ,  D06P1/16

    CPC classification number: C09B23/0075

    Abstract: 1. WATER INSOLUBLE AZLACTONE DYESTUFFS OF THE FORMULA

    (4-(A-(CH=CH)N-CH=),5-(O=)-OXAZOLIN-2-YL-),(4-(B-(CH=

    CH)N-CH=),5-(O=)-OXAZOLIDIN-2-YL-)-D

    WHEREIN A AND B EACH REPRESENT PHENYL, LOWER ALKYLPHENYLENE, LOWER ALKOXY-PHENYLENE, CHLOROPHENYLENE, BROMOPHENYLENE, METHYLENEDIOXY-PHENYLENE OR NAPHTHYL, D REPRESENTS PHENYLENE, CHLOROPHENYLENE, BROMOPHENYLENE, BIPHENYLENE OR NAPTHYLENE, AND N REPRESENTS 0 OR 1.

    4.
    发明专利
    未知

    公开(公告)号：BR8104954A

    公开(公告)日：1982-04-20

    申请号：BR8104954

    申请日：1981-07-31

    Applicant: HOECHST AG

    Inventor： SCHICKFLUSS R ,  SCHUSTER C ,  SCHNEIDER M

    IPC: D06P5/00 ,  B41M5/025 ,  C09D11/02 ,  D06P1/18 ,  D06P5/13 ,  D06P5/28

    Abstract: Transfer-printing supports, which are impregnated or printed with a formulation containing a mixture of a blue disperse dyestuff which sublimes readily and has the formula in which X is hydrogen or halogen, R, R1 and R2 denote alkyl with 1 to 4 carbon atoms and R3 denotes hydrogen or alkyl with 1 to 4 carbon atoms, and yellow to red disperse dyestuffs which sublime readily, give deep and fast black dyeings on polyester materials and polyester mixed materials by the heat transfer-printing process.

    PROCESS FOR PREPARING 1-(N-B-CYANETHYLAMINO)-3-ACYLAMINOBENZENES
    5.
    发明专利
    PROCESS FOR PREPARING 1-(N-B-CYANETHYLAMINO)-3-ACYLAMINOBENZENES 未知

    公开(公告)号：CA1054634A

    公开(公告)日：1979-05-15

    申请号：CA251270

    申请日：1976-04-28

    Applicant: HOECHST AG

    Inventor： SCHICKFLUSS R

    IPC: C07C253/00 ,  B01J27/00 ,  B01J27/20 ,  B01J31/00 ,  B01J31/04 ,  C07B61/00 ,  C07C20060101 ,  C07C67/00 ,  C07C231/00 ,  C07C255/24 ,  C07C120/00

    Abstract: of the disclosure: Process for the manufacture of 1-(N-.beta.-cyanethylamino)-3-acylaminobenzenes of the formula (1) (1) in which R1 represents hydrogen, methyl or alkoxy of 1 to 4 carbon atoms, R2 represents hydrogen, alkyl from 1 to 3 carbon atoms or phenyl, R3 represents hydrogen or alkyl from 1 to 3 carbon atoms, and n represents the integer 0 or 1, which comprises reacting 1 mole of an amino of the formula (2) (2) in which R1, R2 and R3 are defined as above, with 1 to 1.75 moles of acrylonitrile between 70 and 150.degree.C in water with the addition of 1 to 30 percent by weight of an organic carboxylic acid or carbonic acid, and oxethylating the compound at the said formula (1) obtained, if n stands for the integer 0, without or after isolation, with 1 to 10 moles of ethylene oxide between 50 and 100.degree.C.

    6.
    发明专利
    未知

    公开(公告)号：BR7602626A

    公开(公告)日：1976-11-23

    申请号：BR7602626

    申请日：1976-04-28

    Applicant: HOECHST AG

    Inventor： SCHICKFLUSS R

    IPC: C07C253/00 ,  B01J27/00 ,  B01J27/20 ,  B01J31/00 ,  B01J31/04 ,  C07B61/00 ,  C07C20060101 ,  C07C67/00 ,  C07C231/00 ,  C07C255/24 ,  C07C121/16

    Abstract: Process for the manufacture of 1-(N- beta -cyanethylamino)-3-acylaminobenzenes of the formula (1) (1) in which R1 represents hydrogen, methyl or alkoxy of 1 to 4 carbon atoms, R2 represents hydrogen, alkyl from 1 to 3 carbon atoms or phenyl, R3 represents hydrogen or alkyl from 1 to 3 carbon atoms, and n represents the integer 0 or 1, which comprises reacting 1 mole of an amino of the formula (2) (2) in which R1, R2 and R3 are defined as above, with 1 to 1.75 moles of acrylonitrile between 70 DEG and 150 DEG C in water with the addition of 1 to 30% by weight of an organic carboxylic acid or carbonic acid, and oxethylating the compound at the said formula (1) obtained, if n stands for the integer 0, without or after isolation, with 1 to 10 moles of ethylene oxide between 50 DEG and 100 DEG C.

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