公开(公告)号：EP2799423A4

公开(公告)日：2015-08-12

申请号：EP12861493

申请日：2012-11-27

Applicant: KAO CORP

Inventor： NAKAI TAKESHI ,  FUJIOKA TOKU ,  AMISHIGE YASUO

IPC: C07C51/23 ,  C07B61/00 ,  C07C59/125 ,  C08G65/324 ,  C11D1/06

CPC classification number: C07C51/25 ,  B01J23/6447 ,  C07C51/23 ,  C08G65/324 ,  C11D1/06 ,  C07C59/125

公开(公告)号：ES2621254T3

公开(公告)日：2017-07-03

申请号：ES12861493

申请日：2012-11-27

Applicant: KAO CORP

Inventor： NAKAI TAKESHI ,  FUJIOKA TOKU ,  AMISHIGE YASUO

IPC: C07C51/23 ,  C07B61/00 ,  C07C59/125 ,  C08G65/324 ,  C11D1/06

Abstract: Un método para producir ácido polioxialquilen alquil éter carboxílico o una sal del mismo, donde el método comprende un proceso de reacción de oxidación de oxidar polioxialquilen alquil éter con oxígeno suministrando un gas que contiene oxígeno a una suspensión o una solución que tiene una profundidad de 200 mm o más e incluye polioxialquilen alquil éter, donde en el proceso de reacción de oxidación, en un periodo en el cual una conversión expresada mediante la Ecuación (A) es mayor que o igual al 50% y menor que el 70%, se reduce una velocidad de suministro del gas que contiene oxígeno de tal manera que una velocidad de suministro de oxígeno con respecto a un número molar total de polioxialquilen alquil éter, ácido polioxialquilen alquil éter carboxílico, y la sal del mismo se reduzca desde un intervalo mayor que 10 mol%/h y menor que o igual a 15 mol%/h hasta un intervalo mayor que o igual a 1 mol%/h y menor que o igual a 10 mol%/h, conversión (%) >= c2 * 100/(c1 + c2) (A) [donde c1 es una molaridad (mol/l) de polioxialquilen alquil éter, y c2 es una molaridad total (mol/l) de ácido polioxialquilen alquil éter carboxílico y la sal del mismo],

公开(公告)号：MY161171A

公开(公告)日：2017-04-14

申请号：MYPI2013000506

申请日：2011-08-10

Applicant: KAO CORP

Inventor： SAITO JUNNOSUKE ,  NAKAI TAKESHI

IPC: C07D301/26 ,  C07D303/22 ,  C25B1/14 ,  C25B1/22

Abstract: THE PRESENT INVENTION PROVIDES A METHOD FOR PRODUCING THE EPOXY COMPOUND, INCLUDING THE FOLLOWING STEPS 1 TO 4: STEP 1) CYCLIZING A CHLOROHYDRIN WITH AN ALKALI AGENT TO OBTAIN A COMPOSITION CONTAINING AN EPOXY COMPOUND, AN INORGANIC SALT AND WATER; STEP 2) TREATING THE INORGANIC SALT AND WATER GENERATED IN THE STEP 1 WITH A BIPOLAR MEMBRANE ELECTRO DIALYZER TO RECOVER AND COLLECT AN ALKALI AGENT AND AN ACID; STEP 3) SUPPLYING A COMPOSITION CONTAINING THE INORGANIC SALT AT A REDUCED CONCENTRATION DISCHARGED FROM THE COMPARTMENT 1 AFTER THE STEP 2 INTO THE COMPARTMENT 2 AND/OR THE COMPARTMENT 3 TO REUSE THE COMPOSITION AS AN AQUEOUS ELECTROLYTE SOLUTION IN THE STEP 2; AND STEP 4) REUSING THE ALKALI AGENT RECOVERED IN THE STEP 2 AS AN ALKALI AGENT FOR THE STEP 1.

公开(公告)号：MY160901A

公开(公告)日：2017-03-31

申请号：MYPI2012701180

申请日：2011-06-16

Applicant: KAO CORP

Inventor： NAKAI TAKESHI ,  SHIRASAWA TAKESHI

IPC: C25B3/00 ,  C07C41/03 ,  C07C43/13 ,  C07D301/02

Abstract: The present invention provides the method for producing the alkyl glycidyl ether in the bipolar membrane electrodialyzer, including applying current to the composition (A) having a heterogeneous system (oil phase/aqueous phase) containing the chlorohydrin ether at a concentration of not less than 5% by weight, water, and the electrolyte in the electrodialyzer to convert the chlorohydrin ether to the alkyl glycidyl ether through the reaction with OH generated on the bipolar membrane and simultaneously to separate and collect the C1 side product in the form of HC1 (hydrochloric acid).

公开(公告)号：JP2012021228A

公开(公告)日：2012-02-02

申请号：JP2011132810

申请日：2011-06-15

Applicant: Kao Corp ,  花王株式会社

Inventor： NAKAI TAKESHI ,  SHIRASAWA TAKESHI

IPC: C25B3/00 ,  C07B61/00 ,  C07C41/03 ,  C07C43/13 ,  C07D301/02 ,  C07D303/22

CPC classification number: C07D301/26 ,  B01D61/445 ,  C07D303/22

Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an alkylglycidyl ether not requiring a removing operation of by-produced metal salt, capable of remarkably reducing generation of waste water by utilizing water resources effectively, and further capable of producing an alkylglycidyl ether with a high yield.SOLUTION: In the method for producing an alkylglycidyl ether, a composition (A), which is composed of a heterogeneous phase system (oil phase/water phase), has a chlorohydrin ether concentration of 5 mass% or more, and contains water and an electrolyte, is introduced into an electrodialyzer that has a bipolar membrane 24 and 25 and an electric current is applied thereto, so that a chlorohydrin ether contained in the composition (A) is converted into an alkylglycidyl ether by the action of OH- that is generated by the bipolar membrane 24 and 25, while separating and recovering by-produced Cl- in the form of HCl (hydrochloric acid) at the same time.

Abstract translation: 待解决的问题：提供一种不需要除去生成的金属盐的烷基缩水甘油醚的制造方法，其能够有效地利用水资源显着地减少废水的产生，并且还能够制备烷基缩水甘油基 乙醚，产率高。 解决方案：在烷基缩水甘油醚的制造方法中，由异相体系（油相/水相）组成的组合物（A）的氯醇醚浓度为5质量％以上，含有 将水和电解质引入具有双极性膜24和25的电渗析器中，并向其施加电流，使得组合物（A）中包含的氯代醇醚通过OH-的作用转化为烷基缩水甘油醚， 其由双极性膜24和25产生，同时以HCl（盐酸）的形式分离和回收副产物Cl-。 版权所有（C）2012，JPO＆INPIT

公开(公告)号：JP2010143890A

公开(公告)日：2010-07-01

申请号：JP2008325731

申请日：2008-12-22

Applicant: Kao Corp ,  花王株式会社

Inventor： SHIRASAWA TAKESHI ,  NAKAI TAKESHI

IPC: C07D301/26 ,  B01J31/08 ,  B01J38/00 ,  C07D303/14 ,  C07D303/18

CPC classification number: Y02P20/584

Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an epoxy compound which does not require a desalting step separate from the reaction step and does not accompany a loss in yield as well. SOLUTION: The method for producing an epoxy compound comprises bringing a compound represented by formula (I) [wherein R 1 is a 1-24C alkoxy group, a hydroxy group, a halogen or hydrogen; A is an -R 2 O- group (wherein R 2 is a 2-4C alkylene group) or a -CH 2 CH(OH)CH 2 O- group; B is a -CH(OH)CH 2 X group or a -CH(X)CH 2 OH group (wherein X is a halogen); m is a number of 0-10; and n is a number of 0-2] into contact with an anion exchanger to react them, to obtain a reaction product represented by formula (II) (wherein R 1 , A, m, and n are the same as defined above). COPYRIGHT: (C)2010,JPO&INPIT

Abstract translation: 待解决的问题：提供一种环氧化合物的制备方法，其不需要与反应步骤分离的脱盐步骤，并且不伴随产率的损失。 解决方案：制备环氧化合物的方法包括使由式（I）表示的化合物[其中R 1 为1-24℃烷氧基，羟基，卤素或氢; A是一个-R 2 O-基团（其中R 2 是2-4C亚烷基）或-CH- SB 2 CH（OH ）CH 2 O-基团; B是-CH（OH）CH 2 SBR基或-CH（X）CH 2 S 2 OH基（其中X是卤素）。 m是0-10的数; 和n是0-2]的数，与阴离子交换剂接触以使其反应，得到由式（II）表示的反应产物（其中R 1，A，m和n为 与上述相同）。 版权所有（C）2010，JPO＆INPIT

公开(公告)号：JP2008255110A

公开(公告)日：2008-10-23

申请号：JP2008063020

申请日：2008-03-12

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOYA SHINGO ,  SAKUMA YASUMITSU ,  NAKAI TAKESHI ,  MINE KOJI

IPC: A61K8/37 ,  A61K8/39 ,  A61K8/42 ,  A61K8/46 ,  A61Q5/02

Abstract: PROBLEM TO BE SOLVED: To provide a pearl gloss composition which maintains strong pearl gloss and is simultaneously large in turbidity. SOLUTION: Provided are a pearl gloss composition comprising a fatty acid glycol ester, an alkyl sulfate salt, a polyoxyalkylene type nonionic surfactant and water, characterized by further containing 0.3 to 3 wt.% of a fatty acid, and a method for producing the same. COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 要解决的问题：提供一种保持强烈的珍珠光泽并同时具有大浊度的珍珠光泽组合物。 解决方案：提供包含脂肪酸二醇酯，烷基硫酸盐，聚氧化烯型非离子表面活性剂和水的珍珠光泽组合物，其特征在于还含有0.3至3重量％的脂肪酸​​，以及用于 生产相同。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2008156522A

公开(公告)日：2008-07-10

申请号：JP2006348170

申请日：2006-12-25

Applicant: Kao Corp ,  花王株式会社

Inventor： MIYAHARA TSUTOMU ,  NAKAI TAKESHI ,  KOZUKA ATSUSHI ,  NAKAJIMA MINAKO

IPC: C11B9/00

Abstract: PROBLEM TO BE SOLVED: To provide a granulating method which inhibits the volatilization of a perfume component having high volatility to reduce loss as much as possible. SOLUTION: This method for manufacturing perfume particles comprises a step of adding a perfume to a thermoplastic water-soluble binder and granulating the resulting mixture at a temperature of lower than the melting point of the water-soluble binder. Perfume particles are prepared by the manufacturing method. COPYRIGHT: (C)2008,JPO&INPIT

Abstract translation: 待解决的问题：提供抑制具有高挥发性的香料组分的挥发以尽可能减少损失的造粒方法。 解决方案：用于制造香料颗粒的方法包括将一种香料加入到热塑性水溶性粘合剂中并在低于水溶性粘合剂的熔点的温度下制粒所得混合物的步骤。 香料颗粒通过制造方法制备。 版权所有（C）2008，JPO＆INPIT

公开(公告)号：JP2007169197A

公开(公告)日：2007-07-05

申请号：JP2005367450

申请日：2005-12-21

Applicant: Kao Corp ,  花王株式会社

Inventor： NAKAI TAKESHI ,  KOZUKA ATSUSHI

IPC: A01N31/02 ,  A01G7/06 ,  A01N25/12 ,  A01N37/12 ,  A01P21/00 ,  C05G3/00

Abstract: PROBLEM TO BE SOLVED: To provide a particulate plant vitalizer having suitable form, particle size and the like for mechanical spreading, and efficiently producible by a simple method.
SOLUTION: The plant vitalizer with cover comprises a particulate obtained by forming a cover layer on a particulate (D) to be covered, which cover layer comprises a specific compound (A) having plant-vitalizing activity, an emulsifying/dispersing agent (B) and a water-soluble vehicle (C), wherein the plant vitalizer with cover comprises a particulate having a structure in which the compound (A) is dispersed in the cover layer as oil drops.
COPYRIGHT: (C)2007,JPO&INPIT

Abstract translation: 要解决的问题：提供具有用于机械扩散的合适形状，粒度等的颗粒状植物激活剂，并且可以通过简单的方法有效地生产。 解决方案：具有盖的植物促进剂包括通过在要被覆盖的颗粒（D）上形成覆盖层而获得的颗粒，该覆盖层包含具有植物活化活性的特定化合物（A），乳化分散剂 （B）和水溶性载体（C），其中具有盖的植物促进剂包括具有其中化合物（A）以油滴分散在覆盖层中的结构的颗粒。 版权所有（C）2007，JPO＆INPIT

公开(公告)号：JP2013067564A

公开(公告)日：2013-04-18

申请号：JP2011205159

申请日：2011-09-20

Applicant: Kao Corp ,  花王株式会社

Inventor： FUJIOKA TOKU ,  NAKAI TAKESHI ,  AMISHIGE YASUO

IPC: C07C51/235 ,  B01J23/644 ,  C07B61/00 ,  C07C51/47 ,  C07C59/125

CPC classification number: Y02P20/52

Abstract: PROBLEM TO BE SOLVED: To reliably remove noble metal-supporting activated carbon contained in a reaction liquid in a short time, in a method for producing a polyoxyalkylene alkyl ether carboxylate.SOLUTION: An oxygen-containing gas is brought into contact with slurry containing a polyoxyalkylene alkyl ether, a noble metal-supporting catalyst whose carrier is activated carbon, and water, whereby the polyoxyalkylene alkyl ether is oxidized to generate a polyoxyalkylene alkyl ether carboxylate. The resulting reaction liquid containing the generated polyoxyalkylene alkyl ether carboxylate is filtered using a filter medium made of a sulfonic polymer to thereby separate the noble metal-supporting catalyst contained in the reaction liquid.

Abstract translation: 要解决的问题：为了在短时间内可靠地除去反应液中所含的贵金属负载活性炭，在聚氧化烯烷基醚羧酸盐的制造方法中。 解决方案：使含氧气体与含有聚氧化烯烷基醚，载体为活性炭的贵金属负载催化剂和水的浆料接触，由此聚氧化烯烷基醚被氧化以产生聚氧化烯烷基醚 羧酸酯。 使用由磺酸聚合物制成的过滤介质过滤所得到的含有生成的聚氧化烯烷基醚羧酸酯的反应液，由此分离反应液中所含的贵金属负载催化剂。 版权所有（C）2013，JPO＆INPIT