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    NOVEL SILICON-CONTAINING POLYMER AND ITS PRODUCTION
    7.
    发明专利
    NOVEL SILICON-CONTAINING POLYMER AND ITS PRODUCTION 失效

    公开(公告)号：JPH09216949A

    公开(公告)日：1997-08-19

    申请号：JP2243696

    申请日：1996-02-08

    Applicant: MITSUI TOATSU CHEMICALS

    Inventor： ISHIKAWA JUNICHI ,  INOUE KOJI ,  IWATA KENJI ,  ITO MASAYOSHI

    IPC: C07F7/08 ,  C08G77/48 ,  C08G77/60

    Abstract: PROBLEM TO BE SOLVED: To produce a silicon-contg. polymer improved in heat resistance by reacting a specific disilane compd. with a diethynyl compd. in the presence of a basic metal oxide catalyst. SOLUTION: A silicon-contg. polymer having repeating units represented by formula III and having acetylene bonds and Si-H bonds is obtd. by reacting a disilane compd. represented by formula I (wherein R and R are each H, 1-30C alkyl, alkenyl, alkynyl, or an arom. group such as a phenyl group; R is a 1-30C alkylene, alkenylene or alkynylene, or an arom. group such as a phenylene group; and (n) is 0 or 1) with a diethynyl compd. represented by formula II (wherein R is a 1-30C alkylene, alkenylene or alkynylene, or a divalent arom. group such as a phenylene or naphthylene group; and (n) is 0 or 1) in the presence of 0.1-1mol (based on 1mol of the diethynyl compd.) of a basic metal oxide catalyst preactivated at 100-800 deg.C for 1-20hr.

    FUNCTIONALLY GRADIENT MATERIAL AND ITS PRODUCTION
    8.
    发明专利
    FUNCTIONALLY GRADIENT MATERIAL AND ITS PRODUCTION 失效

    公开(公告)号：JPH09176325A

    公开(公告)日：1997-07-08

    申请号：JP17962696

    申请日：1996-07-09

    Applicant: MITSUI TOATSU CHEMICALS

    Inventor： INOUE KOJI ,  IWATA KENJI ,  ISHIKAWA JUNICHI ,  ITO MASAYOSHI

    IPC: C08J3/00 ,  C08G77/48 ,  C08G77/60 ,  C08G79/00

    Abstract: PROBLEM TO BE SOLVED: To obtain a silicon-contg. functionally gradient material excellent in resistances to heat and combustion, and in mechanical properties. SOLUTION: This silicon-contg. functionally gradient material is obtained by treating a silicon-contg. polymeric compound of the formula (R is H, an alkyl, alkenyl, alkynyl or aromatic group; R is an alkylene, alkenylene or divalent aromatic group; R is an alkylene, alkenylene, alkynylene or divalent aromatic group) and/or its cured product in an inert gas or at reduced pressures at 200-3,500 deg.C, or by heat treatment thereof in a gaseous atmosphere containing 1-50vol.% oxygen at 50-1,000 deg.C.

    DIAMINE COMPOUND CONTAINING SILICON AND ITS PRODUCTION
    9.
    发明专利
    DIAMINE COMPOUND CONTAINING SILICON AND ITS PRODUCTION 失效

    公开(公告)号：JPH0971588A

    公开(公告)日：1997-03-18

    申请号：JP23037195

    申请日：1995-09-07

    Applicant: MITSUI TOATSU CHEMICALS

    Inventor： ISHIKAWA JUNICHI ,  INOUE KOJI ,  IWATA KENJI ,  ITO MASAYOSHI

    IPC: B01J23/02 ,  C07B61/00 ,  C07F7/10

    Abstract: PROBLEM TO BE SOLVED: To produce a new compound, useful as a raw material for polyimides as heat- and burning-resistant materials and containing acetylene and Si-H bonds. SOLUTION: This compound of formula I [R is H, a 1-30C alkyl, phenyl, etc.; R is a 1-30C alkylene, phenylene, naphthylene, etc.; R is a 1-30C alkylene, phenylene, naphthylene, etc.; (l) is a positive integer], e.g. bis(3,3'- aminophenylethyny1)silane. The compound of formula I is obtained by reacting an aminoethynyl compound of formula II with an aminosilyl compound of formula III in the presence of a basic metallic oxide catalyst.

    SILOXANE POLYMER AND ITS PRODUCTION
    10.
    发明专利
    SILOXANE POLYMER AND ITS PRODUCTION 失效

    公开(公告)号：JPH08333458A

    公开(公告)日：1996-12-17

    申请号：JP14182995

    申请日：1995-06-08

    Applicant: MITSUI TOATSU CHEMICALS

    Inventor： INOUE KOJI ,  IWATA KENJI ,  ISHIKAWA JUNICHI ,  ITO MASAYOSHI

    IPC: C08G77/50 ,  C08G77/48

    Abstract: PURPOSE: To obtain a silicon-contg. material which is excellent in resistances to heat and combustion. CONSTITUTION: This siloxane polymer has repeating units contg. acetylene bonds, Si-H bonds, and siloxane bonds and is represented by the formula (wherein R . R , R , and R are each H, a 1-30C alkyl, alkenyl, alkynyl. or arom. such as phenyl or naphthyl; R is a 1-30C divalent hydrocarbon group such as an alkylene, alkenylene, alkynylene, or arom. such as phenylene or naphthylene; l is 0 or 1; m is a positive integer; and n is 0 or a positive integer).

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