1.
    发明专利
    未知

    公开(公告)号:BR8404332A

    公开(公告)日:1985-07-30

    申请号:BR8404332

    申请日:1984-08-30

    Applicant: STAMICARBON

    Abstract: The invention relates to a process for recovering capro- actam from a residue remaining in a destillation, under reduced pressure, of impure caprolactame, obtained by rearrangement of cyclohexanone-oxime with sulphuric acid or oleum. The process consists of a destillation of the residue under reduced pressure, followed by a hydrogenation of the caprolactam containing destillate in an aqueous medium, from which hydrogenation-product caprolactam is recovered.

    PROCESS FOR THE PURIFICATION OF 2-PYRROLIDONE

    公开(公告)号:DE3166798D1

    公开(公告)日:1984-11-29

    申请号:DE3166798

    申请日:1981-05-29

    Applicant: STAMICARBON

    Abstract: In a distillation process 2-pyrrolidones obtained from succinonitrile are purified by treating the impure liquid pyrrolidone with a strong base, fractionally distilling this product to yield, as distillate, polymerization grade purified 2-pyrrolidone, mixing the 2-pyrrolidone-containing residue from the fractional distillation with water and an acid, and extracting purified 2-pyrrolidone from the water/acid mixture. The latter purified 2-pyrrolidone products are suitable for recycling to the pyrrolidone synthesis or to make other products.

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