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1.发明授权Process of preparing a mixture of a lactam and an alkali compound of this lactam 失效制备本发明乳酸酯和碱性化合物的混合物的方法
公开(公告)号：US3563980A
公开(公告)日：1971-02-16
申请号：US3563980D
申请日：1968-04-05
Applicant: STAMICARBON
Inventor： MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN , DILVA JOHANNES J DE
IPC: B01J19/18 , C07D201/14 , C08G69/18 , C07D41/08
CPC classification number: C08G69/18 , B01J19/1862 , B01J2219/0009 , B01J2219/00094 , B01J2219/00108 , B01J2219/00182 , C07D201/14
Abstract: PROCESS AND APPARTUS FOR PREPARING A CATALYST FOR THE ANIONIC POLYMERIZATION OF LACTAMS, IN WHICH A LACTAM AND A ALKALI METAL HYDROXIDE ARE CONTINOUSLY FED INTO A FIRST REACTION VESSEL THE LIQUID LEVEL IN SAID VESSEL BEING KEPT CONSTANT BY FEEDING A PORTION OF THE REACTION MIXTURE INTO A SECOND VESSEL AND THE LIQUID LEVEL IN SAID SECOND VESSEL BEING KEPT CONSTANT BY DISCHARGINGG A CONTINUOUS STREAM OF THE REACTION MIXTURE FROM SAID VESSEL. THE WATER FORMED IN THE REACTION VESSELS IS EVAPORATED BY HEATING IN VACUO AND THE VAPOUR THUS FORMED IS PASSED THROUGH A CONDENSER IN WHICH THE LACTAM IS CONDENSED AND RETURNED TO THE REACTION VESSELS.
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公开(公告)号：US3391125A
公开(公告)日：1968-07-02
申请号：US44307465
申请日：1965-03-26
Applicant: STAMICARBON
Inventor： MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN , BOONSTRA HARM J
IPC: C08G69/20
CPC classification number: C08G69/20
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3.发明授权Process for the ionogenic polymerization of omega-lactams with oxy- or thioalkynes as activators 失效用氧 - 或硫炔炔作为活化剂的ω-内酰胺的离子聚合反应的方法
公开(公告)号：US3379697A
公开(公告)日：1968-04-23
申请号：US43503565
申请日：1965-02-24
Applicant: STAMICARBON
Inventor： MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
IPC: C08G69/20
CPC classification number: C08G69/20
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4.发明授权Ionic polymerization of lactams with a derivative of a carboxylic ester of a ketoxime as promoter 失效作为促销剂的羧甲基纤维素的衍生物的LACTAMS的离子聚合
公开(公告)号：US3575937A
公开(公告)日：1971-04-20
申请号：US3575937D
申请日：1967-07-24
Applicant: STAMICARBON
Inventor： BIGOT JOHAN A , MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
CPC classification number: C08G69/20
Abstract: THE USE OF CARBOXYLIC ESTERS OF KETOXIMES, IN WHICH AN ACYL RADICAL HAS BEEN SUBSTITUTED IN THE MOLECULE FOR ONE OF THE HYDROCARBON RADICALS OF THE KETOXIME, AS PROMOTERS, USED IN CONJUNCTION WITH CATALYSTS, IN THE IONIC POLYMERIZATION OF LACTAME, IS DISCLOSED. THE USE OF SUCH PROMOTERS PERMITS RAPID POLYMERIZATION WITH HIGH YIELDS OF AMIDE POLYMERS, WHICH ARE USEFUL IN THE PRODUCTION OF MOLDED PRODUCTS.
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公开(公告)号：US3492275A
公开(公告)日：1970-01-27
申请号：US3492275D
申请日：1967-07-24
Applicant: STAMICARBON
Inventor： BIGOT JOHAN A , MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
CPC classification number: C08G69/20
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Patent Agency Ranking
公开(公告)号：US3488326A
公开(公告)日：1970-01-06
申请号：US3488326D
申请日：1966-11-01
Applicant: STAMICARBON
Inventor： BEVEREN JOHANNES VAN , MOURIK JOHANNES VAN
CPC classification number: C08G69/18
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7.发明授权
公开(公告)号：US3408335A
公开(公告)日：1968-10-29
申请号：US46301065
申请日：1965-06-10
Applicant: STAMICARBON
Inventor： MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
IPC: C07D409/04 , C08G69/20
CPC classification number: C07D409/04 , C08G69/20
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8.发明授权Process for the ionogenic or anionic polymerization of omega-lactams with dispiro alkane diones as activators 失效使用二烷基二恶烷作为活化剂的ω-内酰胺的离子或阴离子聚合方法
公开(公告)号：US3391124A
公开(公告)日：1968-07-02
申请号：US43533865
申请日：1965-02-25
Applicant: STAMICARBON
Inventor： DUYNSTEE EDUARD F J , MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
IPC: C08G69/20
CPC classification number: C08G69/20
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公开(公告)号：US3379698A
公开(公告)日：1968-04-23
申请号：US44309765
申请日：1965-03-26
Applicant: STAMICARBON
Inventor： BIGOT JOHAN A , MOURIK JOHANNES VAN , BEVEREN JOHANNES VAN
IPC: C08G69/20
CPC classification number: C08G69/20
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公开(公告)号：DE1645474A1
公开(公告)日：1970-10-29
申请号：DE1645474
申请日：1966-10-31
Applicant: STAMICARBON
Inventor： BEVEREN JOHANNES VAN , MOURIK JOHANNES VAN
Abstract: 1,147,160. Moulded anionic lactam polymers. STAMICARBON N.V. 28 Oct., 1966 [3 Nov., 1965], No. 48530/66. Heading B5A. [Also in Division C3] A lactam is anionically polymerized at 175 to 210‹ C. using a catalyst but no promoter to obtain a liquid polymer which remains liquid when cooled to 140 to 170‹ C. and a promoter is then mixed with the cooled liquid polymer and the mixture is poured into a mould heated at 140‹ to 170‹ C. wherein it is further polymerized to a solid polymer. Various catalysts and promoters are mentioned. It is stated that the moulds may be made of material with which the monomer-catalyst mixture would be too reactive e.g. epoxy resins. Fillers or dyes may be mixed with the liquid polymer before moulding. In the examples caprolactam is polymerized using KOH as catalyst and dicaprolactam ether as promoter (1) in a cylindrical glass mould and (2) a two part disc-shaped brass mould.
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