Process for production of benzene phosphonic dihalide
    2.
    发明公开
    Process for production of benzene phosphonic dihalide 失效
    生产苯膦二卤化物的方法

    公开(公告)号:EP0010368A1

    公开(公告)日:1980-04-30

    申请号:EP79302006.6

    申请日:1979-09-26

    Inventor: Shim, Kyung Sup

    CPC classification number: C07F9/42

    Abstract: Benzene phosphonic dihalide is produced by oxygenation of phenyl phosphonous dihalide according to the following reaction:
    wherein X is Cl or Br.
    The reaction is conducted at a temperature from about 0°C to about 200°C. Charcoal is added to the reaction mixture when impure phenyl phosphonous dihalide is used as a starting material. The product has high purity and is stable at high temperatures. It can be used as an intermediate to prepare flame retardants, insecticides, pesticides and plasticisers.

    Abstract translation: 苯膦二卤化物是通过苯基二卤化膦的氧化根据以下反应制备的:其中X是Cl或Br。 该反应在约0℃至约200℃的温度下进行。 当不纯的苯基二卤化膦用作原料时,将木炭加入到反应混合物中。 该产品纯度高,在高温下稳定。 它可以用作制备阻燃剂,杀虫剂,杀虫剂和增塑剂的中间体。

    Improved process for the production of insoluble sulfur
    7.
    发明公开
    Improved process for the production of insoluble sulfur 失效
    Verfahren zur Herstellung vonunlöslichemSchwefel。

    公开(公告)号:EP0053832A1

    公开(公告)日:1982-06-16

    申请号:EP81110244.1

    申请日:1981-12-08

    Inventor: Shim, Kyung Sup

    CPC classification number: C01B17/12

    Abstract: Process for the preparation of insoluble sulfur product comprising the steps of vaporizing sulfur, mixing the vaporized sulfur with from about 1 x 10 -6 % to about 5% hydrogen sulfide, in the essential absence of hydrocarbon oil, quenching the vaporized sulfur in a quenching medium and separating the insoluble sulfur product from the quenching medium.

    Abstract translation: 用于制备不溶性硫产物的方法,包括在基本不存在烃油的情况下蒸发硫,将蒸发的硫与约1×10 -6%至约5%的硫化氢混合,骤冷汽化的 硫在淬灭介质中并将不溶性硫产物与淬灭介质分离。

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