Method for preparing p-hydroxycinnamate by using ionic liquid for catalytic lignin depolymerization

    公开(公告)号:US10807940B2

    公开(公告)日:2020-10-20

    申请号:US16642959

    申请日:2017-11-21

    Abstract: The present invention discloses a method for preparing p-hydroxycinnamate by using an ionic liquid for catalytic lignin depolymerization comprising: 1) preparation of a halogen metal-based ionic liquid: preparing the halogen metal-based ionic liquid by reacting an alkylimidazole chloride with a metal chloride by heating the same to 30° C. to 80° C. with stirring; and 2) catalytic depolymerization of lignin: mixing the halogen metal-based ionic liquid and lignin with an alcohol, and after N2 replacement, heating the solution to 140° C. to 200° C. and reacting the solution for 4-8 h while stirring to prepare high value-added chemicals with p-hydroxycinnamate as a main product. The present invention has advantages of a simple process, mild conditions, environmental kindness, and high selectivity for a main product. The ionic liquid is simple in preparation, has a good atom economy, and is recyclable. Under optimal conditions, the yield of p-hydroxycinnamate can reach 40-80 mg/g.

    SiC inverted plasma cutting power supply

    公开(公告)号:US10807184B2

    公开(公告)日:2020-10-20

    申请号:US16082972

    申请日:2017-03-13

    Abstract: The present invention provides an SiC inverted plasma cutting power supply, which is characterized in that: the SiC inverted plasma cutting power supply comprises a main circuit and a closed-loop control circuit; the main circuit comprises a sequentially connected noise suppression module, a power-frequency rectification and filtering module, an SiC inverter module, a power transformer, an SiC rectification and smoothing module and a non-contact arc initiation module, wherein the noise suppression module is connected to an alternating-current input power supply, and the SiC rectification and smoothing module and the non-contact arc initiation module are respectively connected to a load; the closed-loop control circuit comprises a man-machine interaction module, a DSC controller, a failure diagnosis and protection module, an SiC high-frequency drive module and a load electrical signal detection module. The power supply has high inverting frequency, small size, light weight, lower raw material consumption, high energy efficiency, an obvious energy saving effect and excellent dynamic characteristics, and can be applied on both a low-power occasion and medium and high power cutting occasions in a stable and reliable manner.

    Zero-valent iron pillared montmorillonite repair material, and preparation method therefor and application thereof

    公开(公告)号:US10780418B2

    公开(公告)日:2020-09-22

    申请号:US16466299

    申请日:2017-11-23

    Abstract: A zero-valent iron pillared montmorillonite repair material relates to the field of environmental functional materials. A preparation method thereof is mainly to obtain the zero-valent iron pillared montmorillonite repair material by reducing hydroxyl-iron pillared montmorillonite at high temperature in a mixed atmosphere of hydrogen and nitrogen, and mainly includes: (1) preparation of Na-montmorillonite; (2) preparation of a polyhydroxy-iron pillared solution; (3) preparation of hydroxy-iron pillared montmorillonite; and (4) obtaining the zero-valent iron pillared montmorillonite repair material by means of high-temperature reduction-calcination in the mixed atmosphere of hydrogen and nitrogen. The zero-valent iron pillared montmorillonite repair material can be used for removing degradation-resistant organic pollutants, and degrading organics into small molecular organics by means of peroxymonosulfate (PMS).

    AUTOMATIC OBSTACLE AVOIDANCE OPTIMIZATION METHOD FOR CONNECTING LINE OF GRAPHICAL PROGRAMMING SOFTWARE

    公开(公告)号:US20200286268A1

    公开(公告)日:2020-09-10

    申请号:US16607106

    申请日:2017-11-15

    Abstract: Disclosed is an automatic obstacle avoidance optimization method for a connecting line of graphical programming software. A breadth-first search method is adopted to search an optimal connecting line path, and a result is displayed in a front-end interface. In a generated connecting line, a user can drag the connecting line with a mouse to regulate a position of the connecting line. At the time, the mouse is viewed as an unavoidable point, that is, the connecting line starts from a starting point of the connecting line to the unavoidable point and then reaches an end point of the connecting line. By means of the method, high instantaneity requirements of the user can be met, and when the user drags the connecting line with the mouse, a new connecting line is generated in real time without a stuck phenomenon. In addition, the optimality of the connecting line can be guaranteed, when a scene of a front-end programming control is changed, the connecting line can generate a new connecting line path according to a new scene in real time, and the optimality is kept.

    HIGH-STRETCHABLE HIGH-SENSITIVE FLEXIBLE FORCE-SENSITIVE SENSING FIBER AND PREPARATION METHOD THEREFOR

    公开(公告)号:US20200255981A1

    公开(公告)日:2020-08-13

    申请号:US16616974

    申请日:2017-11-27

    Abstract: A high-stretchable high-sensitive flexible force-sensitive sensing fiber and a preparation method therefor comprising the specific preparation method is as follows: uniformly and synergistically dispersing a one-dimensional (1D) nanowire/nanotube and a two-dimensional (2D) conductive sheet layer in a thermoplastic elastomer solution; formulating a uniform dispersion solution of a certain concentration; and using a wet spinning process to prepare an elastic composite fiber with a highly oriented 1D/2D hybrid network. The above-described composite fiber is placed in a metal precursor solution to fully swell, and then placed in reductive steam for reduction, to reduce metal precursors to zero-dimensional (0D) metal nanoparticles, thereby preparing a flexible force-sensitive sensing fiber based on a 0D/1D/2D three-dimensional collaborative network.

    Method for Improving Blood Compatibility of Material Surface by Using Controllable Grafting Technique

    公开(公告)号:US20200255951A1

    公开(公告)日:2020-08-13

    申请号:US16305923

    申请日:2016-12-08

    Abstract: The present invention discloses a method for improving the blood compatibility of a material surface by using a controllable grafting technique. The method involves placing a monomer NVP, an RAFT reagent and a solvent acetonitrile in a container, adding an initiator AIBN, mixing the same uniformly, removing oxygen with liquid nitrogen, making the same react in an oil bath; after polymerization, adding liquid nitrogen to quench and stop the reaction, thus obtaining PVP-COOH; mixing the PVP-COOH with DCC and NHS; adding dry dichloromethane to the mixture in a nitrogen atmosphere, adding mercaptoethylamine, and making the same react in darkness at room temperature; obtaining a crude sample; dissolving the crude sample in water, and performing dialysis with deoxygenated water in darkness, and then obtaining HS-PVP by freeze-drying. An Au—S bond chemisorption method is used to controllably graft an anti-protein high-molecular polymer onto an Au surface.

    An Anionic Imide Material Having Ferromagnetism At Room Temperature And The Use Thereof

    公开(公告)号:US20200247802A1

    公开(公告)日:2020-08-06

    申请号:US16496394

    申请日:2018-07-25

    Abstract: The anionic imide material is obtained by preparing a solution or a suspension of an imide compound, then reducing and drying the same; the anionic material comprises anions of an imide compound, the anions being at least one selected from the following formula I or formula II; in formula I or II: n=1, 2, or 3; R1, R2 are respectively selected from at least one of H, amino, carboxyl, hydroxy, thiol, and pyridyl groups; X1-X4 are respectively an electron withdrawing group, and specifically selected from one of H, F, Cl, Br, CN, and NO2 groups. The anionic material of the present invention has a Curie temperature larger than room temperature and ferromagnetism, and is an organic magnetic material; it may be used for preparing an organic magnetic material and/or an organic magnetic device.

    Tea massage oil, preparation method therefor and application thereof

    公开(公告)号:US10702468B2

    公开(公告)日:2020-07-07

    申请号:US16334364

    申请日:2017-11-21

    Inventor: Yong Ye Qian Yang

    Abstract: The present invention, belonging to the field of daily skin care products, discloses a tea massage oil, a preparation method therefor and an application thereof. The tea massage oil is prepared from the following raw materials in parts by weight: 40-87 parts of ethyl-esterified tea oil, 5-15 parts of oregano oil, 2-12 parts of melaleuca alternifolia oil, 2-10 parts of pumpkin seed oil, 2-10 parts of prickly pear seed oil, 1-10 parts of passion fruit seed oil, and 1-5 parts of nano germanium oxide. The method comprises: evenly mixing the ethyl-esterified tea oil, the oregano oil, the melaleuca alternifolia oil, the pumpkin seed oil, the prickly pear seed oil, the passion fruit seed oil, and the nano germanium oxide, so as to obtain the tea massage oil. The tea massage oil can eliminate fatigue, achieve a men's health-care function, remove scars, and achieve a far-infrared skin activating function.

    Lead-free easy-cutting high-strength corrosion-resistant silicon-brass alloy and the preparation method and use thereof

    公开(公告)号:US10697045B2

    公开(公告)日:2020-06-30

    申请号:US15573774

    申请日:2016-12-15

    Abstract: The present invention relates to a lead-free easy-cutting high-strength corrosion-resistant silicon-brass alloy and the preparation method and use thereof. The mass percent composition of the alloy is: 56˜60% Cu, 38˜42% Zn, 0.003˜0.01% B, 0.03˜0.06% Ti, and 1.0˜1.5% Si and 0.5˜0.9% Al or 0.5˜0.8% Si and 1˜1.5% Al, and the zinc equivalent of all components is between 48% and 50%. In the present invention, the phase composition and the distribution state of the alloy can be regulated by controlling the contents of Si and Al elements, as well as by adding a B and Ti composite grain refiner, in order to obtain a copper alloy with the advantages of excellent comprehensive performance of strength, process ability and dezincification resistance, a high production yield, and low costs, which can replace lead brass and bismuth brass for plumbing, bathroom and a variety of corrosion-resistant parts, and has a bright prospect of popularization and application.

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