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    Fatty acid mixtures of improved low-temperature stability which comprise comb polymers, and their use in fuel oils
    121.
    发明授权
    Fatty acid mixtures of improved low-temperature stability which comprise comb polymers, and their use in fuel oils 有权
    包含梳状聚合物的改进的低温稳定性的脂肪酸混合物及其在燃料油中的应用

    公开(公告)号：US06596037B2

    公开(公告)日：2003-07-22

    申请号：US09993847

    申请日：2001-11-16

    Applicant: Matthias Krull ,  Werner Reimann

    Inventor： Matthias Krull ,  Werner Reimann

    IPC: C10L118

    CPC classification number: C10L10/08 ,  C10L1/143

    Abstract: The invention relates to low-temperature-stabilized fatty acid mixtures comprising A) from 10 to 99.99% by weight of fatty acid mixtures comprising: A1) from 1 to 99% by weight of at least one saturated mono- or dicarboxylic acid having 6 to 50 carbon atoms, A2) from 1 to 99% by weight of at least one unsaturated mono- or dicarboxylic acid having 6 to 50 carbon atoms, and B) from 0.01 to 90% by weight of copolymers comprising: B1) from 40 to 60 mol % of bivalent structural units of the formula  where X═O or N—R1, in which a and b=0 or 1 and a+b=1, and B2) from 60 to 40 mol % of bivalent structural units of the formula —H2C—CR2R3—  B2 and, if desired, B3) from 0 to 20 mol % of bivalent structural units derived from polyolefins, where the polyolefins can be derived from monoolefins having 3 to 5 carbon atoms, and in which a) R1 is an alkyl or alkenyl radical having from 10 to 40 carbon atoms or an alkoxyalkyl radical having from 1 to 100 alkoxy units and from 1 to 30 carbon atoms in the alkyl radical, and b) R3 is a radical of the formula OCOR4 or COOR4, in which R4 is C1-C24-alkyl, and c) the number of carbon atoms in the polyolefin molecules on which the structural units B3) are based is from 35 to 350, and d) R2 is hydrogen or methyl, and to the use of these mixtures for improving the lubrication properties of low-sulfur middle distillates.

    Abstract translation: 本发明涉及低温稳定的脂肪酸混合物，其包含A）10至99.99重量％的脂肪酸​​混合物，其包含：A1）1至99重量％的至少一种具有6至50个的饱和单羧酸或二羧酸 碳原子，A2）1至99重量％的至少一种具有6至50个碳原子的不饱和单羧酸或二羧酸，和B）0.01至90重量％的共聚物，其包含：B1）40至60摩尔％ 其中X = O或N-R1的二价结构单元，其中a和b = 0或1和a + b = 1，B2）为60至40摩尔％的二价结构单元，如果 所需的B3）0至20摩尔％的衍生自聚烯烃的二价结构单元，其中聚烯烃可以衍生自具有3至5个碳原子的单烯烃，并且其中a）R 1是具有10至40个的烷基或烯基 碳原子或烷基中具有1至100个烷氧基单元和1至30个碳原子的烷氧基烷基，b ）R3是式OCOR4或COOR4的基团，其中R4是C1-C24-烷基，c）结构单元B3）所基于的聚烯烃分子中的碳原子数为35〜350，以及 d）R2是氢或甲基，以及使用这些混合物来改善低硫中间馏分的润滑性能。

    Mixtures of carboxylic acids, their derivatives and hydroxyl-containing polymers and their use for improving the lubricating effect of oils
    122.
    发明授权
    Mixtures of carboxylic acids, their derivatives and hydroxyl-containing polymers and their use for improving the lubricating effect of oils 失效
    羧酸，其衍生物和含羟基聚合物的混合物及其用于改善油的润滑效果的用途

    公开(公告)号：US06592638B2

    公开(公告)日：2003-07-15

    申请号：US09811307

    申请日：2001-03-16

    Applicant: Matthias Krull ,  Werner Reimann

    Inventor： Matthias Krull ,  Werner Reimann

    IPC: C10L118

    CPC classification number: C10L10/08 ,  C10L1/143 ,  C10L1/18

    Abstract: The invention relates to additives for improving lubricating properties of fuel oils, comprising A) 10-95% by weight of at least one oil-soluble amphiphile which comprises nitrogen- or oxygen-containing groups substituted by alkyl, alkenyl, hydroxyalkyl or aromatic radicals, and B) 5-90% by weight of at least one copolymer which contains B1) from 0.5 to 15 mol % of structural units which are derived from olefinically unsaturated compounds which have at least one free hydroxyl group, and B2) from 85 to 99.5 mol % of structural units which are derived from ethylene, and, if required, B3) from 0 to 20 mol % of further structural units selected from the group consisting of (meth)acrylic acid, (meth)acrylates, vinyl esters, vinyl ethers and alkenes, and the copolymer has an average molar mass Mw of from 500 to 100,000 g/mol and an OH number of from 5 to 500 mg KOH/g.

    Abstract translation: 本发明涉及用于改善燃料油的润滑性能的添加剂，其包括：A）10-95重量％的至少一种油溶性两亲物，其包含被烷基，链烯基，羟烷基或芳族基团取代的含氮或含氧基团，和B ）5-90重量％的至少一种共聚物，其含有B 1）0.5至15摩尔％的衍生自具有至少一个游离羟基的烯属不饱和化合物的结构单元，和B 2）85-99.5摩尔％的结构 衍生自乙烯的单元，如果需要，B3）0至20摩尔％的选自（甲基）丙烯酸，（甲基）丙烯酸酯，乙烯基酯，乙烯基醚和烯烃的其它结构单元，以及 共聚物的平均摩尔质量Mw为500〜100,000g / mol，OH值为5〜500mgKOH / g。

    Use of hydroxyl-containing copolymers for the preparation of fuel oils having improved lubricity
    123.
    发明授权
    Use of hydroxyl-containing copolymers for the preparation of fuel oils having improved lubricity 失效
    使用含羟基的共聚物来制备具有改善的润滑性的燃料油

    公开(公告)号：US06391071B1

    公开(公告)日：2002-05-21

    申请号：US09591236

    申请日：2000-06-09

    Applicant: Matthias Krull ,  Markus Kupetz

    Inventor： Matthias Krull ,  Markus Kupetz

    IPC: C10L118

    CPC classification number: C10L10/08 ,  C10L1/195 ,  C10L1/1955 ,  C10L1/1963 ,  C10L1/1973 ,  C10L1/236

    Abstract: The present invention relates to the use of oil-soluble copolymers which comprise A) from 5 to 80 mol-% of structural units derived from olefinically unsaturated compounds containing at least one free hydroxyl group, B) from 5 to 95 mol-% of structural units derived from olefinically unsaturated compounds carrying a hydrocarbon radical having at least 6 carbon atoms, and, if desired, C) from 0 to 40 mol-% of further structural units selected from the group consisting of acrylic acid, acrylates, vinyl esters, vinylethane and alkenes, with the proviso that the structural units mentioned under C) are different from the structural units mentioned under A) and B), and have a mean molecular weight Mw of from 500 to 100,000 g/mol and an OH number of from 10 to 300 mg of KOH/g, for improving the lubricity and cold flow properties of middle distillates having a sulfur content of less than 0.5% by weight.

    Abstract translation: 本发明涉及油溶性共聚物的用途，该共聚物包含A）5至80mol％的衍生自含有至少一个游离羟基的烯属不饱和化合物的结构单元，B）5至95mol％的结构单元 衍生自携带具有至少6个碳原子的烃基的烯属不饱和化合物，如果需要，C）0至40摩尔％的选自丙烯酸，丙烯酸酯，乙烯酯，乙烯基乙烷和 烯烃，条件是C）中提到的结构单元不同于A）和B）中提及的结构单元，并且具有500至100,000g / mol的平均分子量Mw和10至 300mg KOH / g，用于改善硫含量小于0.5重量％的中间馏分的润滑性和冷流动性。

    Process for improving the cold-flow properties of fuel oils
    124.
    发明授权
    Process for improving the cold-flow properties of fuel oils 有权
    改进燃油的冷流特性的方法

    公开(公告)号：US6110238A

    公开(公告)日：2000-08-29

    申请号：US235723

    申请日：1999-01-22

    Applicant: Matthias Krull ,  Werner Reimann

    Inventor： Matthias Krull ,  Werner Reimann

    IPC: C10L1/192 ,  C10L1/14 ,  C10L1/195 ,  C10L1/196 ,  C10L1/197 ,  C10L10/18 ,  C10L1/18

    CPC classification number: C10L1/195 ,  C10L1/143 ,  C10L1/1973

    Abstract: A process for improving the cold flow properties of fuel oils comprising the addition to fuel oil of an additive comprising copolymers of lower olefins and vinyl esters and a terpolymer of 4-methylpentene-1 and an additive composition comprising copolymers of lower olefins and vinyl esters and a terpolymer of 4-methylpentene-1.

    Abstract translation: 一种用于改进燃料油的冷流动性能的方法，其包括添加到包含低级烯烃和乙烯基酯的共聚物的添加剂的燃料油和4-甲基戊烯-1的三元共聚物和包含低级烯烃和乙烯基酯的共聚物的添加剂组合物的方法，以及 4-甲基戊烯-1的三元共聚物。

    Additive for improving the flow properties of mineral oils and mineral oil distillates
    125.
    发明授权
    Additive for improving the flow properties of mineral oils and mineral oil distillates 有权
    添加剂用于改善矿物油和矿物油馏分的流动性能

    公开(公告)号：US6010989A

    公开(公告)日：2000-01-04

    申请号：US148933

    申请日：1998-09-04

    Applicant: Matthias Krull ,  Werner Reimann

    Inventor： Matthias Krull ,  Werner Reimann

    IPC: C10L1/192 ,  C09K3/00 ,  C10L1/14 ,  C10L1/16 ,  C10L1/18 ,  C10L1/182 ,  C10L1/185 ,  C10L1/19 ,  C10L1/197 ,  C10L1/198 ,  C10L1/22 ,  C10L10/18 ,  C10M145/10

    CPC classification number: C10L1/143 ,  C10L1/1616 ,  C10L1/1824 ,  C10L1/1852 ,  C10L1/1855 ,  C10L1/1857 ,  C10L1/19 ,  C10L1/1905 ,  C10L1/191 ,  C10L1/195 ,  C10L1/1966 ,  C10L1/1973 ,  C10L1/1981 ,  C10L1/1985 ,  C10L1/221 ,  C10L1/2222 ,  C10L1/2225 ,  C10L1/224 ,  C10L1/2364 ,  C10L1/238

    Abstract: The invention relates to an additive for improving the flow properties of paraffin-containing mineral oils and mineral oil distillates, comprising a mixture of at least one ethylene/vinyl ester copolymer or terpolymer and at least one paraffin dispersant, wherein said mixture contains ethers and/or esters as solubilizers, wherea) the ethers conform to the formula 1R--O--R' (1) in which R is a linear or branched alkyl or alkenyl group having 4 to 30 carbon atoms, and R' is a linear or branched alkyl or alkenyl group having 1 to 30 carbon atoms,b) the esters are derived from monobasic or polybasic carboxylic acids having 4 to 30 carbon atoms (acid radical) and from monohydric or polyhydric alcohols having 1 to 30 carbon atoms (alcohol radical), orc) the ethers and/or esters are cyclic, with a ring size of from 6 to 30 carbon atoms.The invention furthermore relates to a process for improving the flow properties of mineral oils and mineral oil distillates which comprises adding the novel additive thereto.

    Abstract translation: 本发明涉及用于改善含链烷烃的矿物油和矿物油馏出物的流动性质的添加剂，其包括至少一种乙烯/乙烯基酯共聚物或三元共聚物和至少一种链烷烃分散剂的混合物，其中所述混合物含有醚和/ 或酯作为增溶剂，其中a）醚符合式1的RO-R'（1）其中R是具有4至30个碳原子的直链或支链烷基或烯基，R'是直链或支链烷基 或具有1至30个碳原子的烯基，b）酯衍生自具有4至30个碳原子的一元或多元羧酸（酸基）和具有1至30个碳原子的一元或多元醇（醇基），或 c）醚和/或酯是环状的，环的大小为6至30个碳原子。 本发明还涉及一种用于改善矿物油和矿物油馏出物的流动性质的方法，其包括向其中加入新的添加剂。

    Alkenylaminoalkane-1,1-diphosphonic acid derivatives and copolymers thereof with unsaturated carboxylic acids
    129.
    发明授权
    Alkenylaminoalkane-1,1-diphosphonic acid derivatives and copolymers thereof with unsaturated carboxylic acids 失效
    烯基氨基烷烃-1,1-二膦酸衍生物及其与不饱和羧酸的共聚物

    公开(公告)号：US5302677A

    公开(公告)日：1994-04-12

    申请号：US37256

    申请日：1993-03-26

    Applicant: Matthias Krull ,  Christoph Naumann ,  Herrmann Hoffmann

    Inventor： Matthias Krull ,  Christoph Naumann ,  Herrmann Hoffmann

    IPC: C02F5/14 ,  C07F9/40 ,  C08F30/02 ,  C08F230/02 ,  C09K3/00 ,  C11D3/37

    CPC classification number: C08F230/02 ,  C02F5/14 ,  C07F9/405 ,  C11D3/3784

    Abstract: The invention relates to alkenylaminoalkane-1,1-diphosphonic acid derivatives of the formula I ##STR1## in which R.sup.1 to R.sup.5, a, b, and Z have the meaning given in the description and to processes for their preparation. The invention furthermore relates to copolymers comprising 0.1-50 mol %, preferably 1-15 mol %, of at least one alkenylaminoalkane-1,1-diphosphonate unit of the formula I and 99.9-50 mol %, preferably 99-85 mol %, of at least one carboxylic acid unit of the formula IIR.sup.6 R.sup.7 C=CR.sup.8 Y (II)in which R.sup.6, R.sup.7, R.sup.8 and Y have the meaning given in the description and to processes for their preparation. These copolymers are used as scale inhibitors, as alkaline earth metal and heavy metal complexing agents and/or sequestering agents and as builders or co-builders in detergents.

    Abstract translation: 本发明涉及式I（I）的链烯基氨基烷烃-1,1-二膦酸衍生物，其中R1至R5，a，b和Z具有说明书中给出的含义及其制备方法。 本发明还涉及包含0.1-50mol％，优选1-15mol％的至少一种式I的链烯基氨基烷烃-1,1-二膦酸酯单元和99.9-50mol％，优选99-85mol％的共聚物， 的至少一种式IIR 6 R 7 C = CR 8 Y（II）的羧酸单元，其中R 6，R 7，R 8和Y具有说明书中给出的含义及其制备方法。 这些共聚物用作阻垢剂，作为碱土金属和重金属络合剂和/或螯合剂，以及作为洗涤剂中的助洗剂或助洗剂。

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