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    Device for generating high pressures and temperatures
    142.
    发明授权
    Device for generating high pressures and temperatures 失效
    用于产生高压和高温的装置

    公开(公告)号：US3895894A

    公开(公告)日：1975-07-22

    申请号：US35373873

    申请日：1973-04-23

    Applicant: KRUPP GMBH

    Inventor： BIERMANN KLAUS ,  BURBACH JURGEN ,  GIMPEL HORST ,  ZIRPINS BURCKHARD

    IPC: B01J3/06 ,  B29C11/00 ,  B29F5/00

    CPC classification number: B01J3/065

    Abstract: A device for generating high pressures and temperatures, in which in the pressure chamber of a high strength metallic pressure container, a charge of material laterally surrounded by electrically insulating material by means of two piston rams movable in opposite direction with regard to each other and sealed relative to the pressure container is subjected to pressure while being electrically heated. The pressure container comprises at least two axially aligned metallic ring members of high strength hard metal which define a pressure chamber, while between the rings and between the rings and a matrix surrounding the rings, pressure resistant electrically insulating material is provided. Outside the pressure chamber, sealing means of plastically deformable strong metallic material are provided between the piston rams and the rings.

    Abstract translation: 一种用于产生高压和高温的装置，其中在高强度金属压力容器的压力室中，由电绝缘材料横向包围的材料的电荷通过相对于彼此相反方向可移动的两个活塞凸起而密封 相对于压力容器在电加热的同时承受压力。 压力容器包括高强度硬金属的至少两个轴向排列的金属环构件，其限定了压力室，同时在环之间和环之间以及围绕环的基体之间提供耐压电绝缘材料。 在压力室外面，在活塞杆和环之间提供可塑性变强的金属材料的密封装置。

    Mass of polycrystalline cubic system boron nitride and composites of polycrystalline cubic system boron nitride and other hard materials, and processes for manufacturing the same
    144.
    发明授权
    Mass of polycrystalline cubic system boron nitride and composites of polycrystalline cubic system boron nitride and other hard materials, and processes for manufacturing the same 失效
    多晶CIBIC系统的硼酸盐和多晶硅系统的复合物和其他硬质材料的制造及其制造方法

    公开(公告)号：US3852078A

    公开(公告)日：1974-12-03

    申请号：US21156471

    申请日：1971-12-23

    Applicant: WAKATSUKI M ,  ICHINOSE K ,  AOKI T ,  MORI R

    Inventor： ICHINOSE K ,  MORI R ,  AOKI T ,  WAKATSUKI M

    IPC: B01J3/06 ,  C04B35/5831 ,  C04B35/52

    CPC classification number: C04B35/5831 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/067 ,  B01J2203/0685

    Abstract: This invention gives bonded or compact bodies of polycrystalline cubic system boron nitride and substantially uniform composites of polycrystalline cubic system boron nitride and other hard materials, for example, metal borides, such as titanium boride and zirconium boride, covalent or metallic cabides, such as boron carbide, silicon carbide, titanium, carbide, tungsten carbide and chromium carbide, metal nitrides, such as titanium nitride, tantalum nitride, silicon nitride and aluminum nitride, metal oxides, such as alumina and silica, complex oxide such as garnet and agate, and diamond. Further, this invention provides a process of obtaining the bonded body of these materials which comprises subjecting hexagonal system boron nitride powder, or a mixture of hexagonal system boron nitride powder and cubic system boron nitride crystal powder or powders of the above-mentioned hard materials to high temperatures and high pressures.

    Abstract translation: 本发明提供了多晶立方氮化硼和多晶立方氮化硼和其它硬质材料的基本上均匀的复合材料的结合体或致密体，例如金属硼化物，例如硼化钛和硼化锆，共价或金属催化剂，例如硼 碳化物，碳化硅，钛，碳化物，碳化钨和碳化铬，金属氮化物，例如氮化钛，氮化钽，氮化硅和氮化铝，金属氧化物如氧化铝和二氧化硅，复合氧化物如石榴石和玛瑙，以及 钻石。 此外，本发明提供了获得这些材料的接合体的方法，其包括将六方晶系氮化硼粉末或六方晶系氮化硼粉末和立方体系氮化硼晶体粉末或上述硬质材料的粉末的混合物 高温高压。

    Method of bonding diamond with refractory cermet material
    146.
    发明授权
    Method of bonding diamond with refractory cermet material 失效
    将金刚石与耐火材料接合的方法

    公开(公告)号：US3785093A

    公开(公告)日：1974-01-15

    申请号：US3785093D

    申请日：1970-12-21

    Applicant: VERESCHAGIN L ,  KONYAFV J ,  DOVBNYA A ,  ASANNURI A ,  PALY P ,  POLYAKOV E ,  STEPANOVICH A ,  GEVORKOV G ,  OBLASTI L

    Inventor： VERESCHAGIN L ,  KONYAFV J ,  STEPANOVICH A ,  ASANNURI A ,  DOVBNYA A ,  POLYAKOV E ,  OBLASTI L ,  PALY P ,  GEVORKOV G

    IPC: B01J3/06 ,  B24D3/08 ,  B24D3/06 ,  B24D3/14

    CPC classification number: B24D3/08 ,  B01J3/062 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/0685

    Abstract: The diamond and cement materials to be sintered are placed in a hermetic graphite sheathing which is, in turn, arranged inside a sheathing of some low-melting metal. The latter is to be made from a metal whose melting point is lower than the temperature at which diamond will be sintered with the cermet material. The filled-up graphite sheathing is placed into a high-pressure reaction chamber and heated up until the low-melting metal gets soft. Thereafter the temperature and the pressure are raised until they are adequate for diamond to be sintered with cermet material. The softened sheathing of the low-melting material is a hydrostatic medium which provides for a uniform distribution of pressure and temperature over the entire volume of materials being sintered.

    Abstract translation: 将待烧结的金刚石和水泥材料放置在密封石墨护套中，其又布置在一些低熔点金属的护套内。 后者由熔点低于金刚石与金属陶瓷材料烧结的温度的金属制成。 将填充的石墨护套放入高压反应室中并加热直到低熔点金属变软。 此后，温度和压力升高直到它们足以使金刚石与金属陶瓷材料烧结。 低熔点材料的软化护套是静压介质，其在整个烧结材料的体积上提供均匀的压力和温度分布。

    Method and device for providing high pressure and high temperature
    148.
    发明授权
    Method and device for providing high pressure and high temperature 失效
    用于提供高压和高温的方法和装置

    公开(公告)号：US3695797A

    公开(公告)日：1972-10-03

    申请号：US3695797D

    申请日：1970-08-26

    Applicant: UK NI KONSHUKTORSKO T I SINT S

    Inventor： BAKUL VALENTIN NIKOLAEVICH ,  PRIKHNA ALEXEI IOSIFOVICH ALEX ,  SHULZHENKO ALEXANDR ALEXANDROV ,  GERASIMOVICH ALEXEI VLADIMIROV

    IPC: B01J3/06 ,  B30B11/32

    CPC classification number: B01J3/065 ,  Y10S425/026

    Abstract: A die pair for use in high temperature high pressure apparatus for use in the synthesis of super hard materials such as diamonds, cubic boron nitride or the like in which the dies include an annular step structure on confronting cooperating faces of the dies to afford over an extended period of time stable, repetitive temperatures in the order of thousands of degrees centigrade and pressures in the order of 60 thousand atmospheres; the confronting die faces having recesses forming a pressure chamber and step structure cooperating with a deformable container of a thermo-and-electro-insulating material such as lithographic stone etc. which deforms as heated and has pressure applied thereto to form an annular sealing ''''burr'''' of a greater volume than an outer surrounding annular slot filled with a porous plastic, electro-insulating material such as ''''technical rubber'''' etc.; the deformable container being of a volume to fill the space both inwardly and outwardly of the material being treated up to the confronting edge of annular surrounding steps; the outer steps having radial, transverse slots; staggered in confronting relation; for readily accommodating the porous plastic outer seal.

    Abstract translation: 用于合成超硬材料如金刚石，立方氮化硼等的高温高压装置中的模具对，其中模具包括在模具的配合面上面的环状台阶结构，以提供超过 延长的时间段稳定，重复温度在数千摄氏度，压力在6万个大气压的数量级; 相对的模具面具有形成压力室的凹部和与诸如平版印刷石等的热电绝缘材料的可变形容器配合的阶梯结构，其在加热时变形并施加压力以形成环形密封“毛刺 “比填充有多孔塑料的外围环形槽更大的体积，诸如”技术橡胶“之类的电绝缘材料; 所述可变形容器具有一个体积，以便将被处理的材料的内部和外部填充到环形围绕步骤的相对边缘; 所述外部台阶具有径向横向狭槽; 交错对立; 用于容易地容纳多孔塑料外部密封件。

    High-pressure device
    150.
    发明授权
    High-pressure device 失效
    高压设备

    公开(公告)号：US3642412A

    公开(公告)日：1972-02-15

    申请号：US3642412D

    申请日：1969-09-30

    Applicant: ADAMANT LAB PROPRIETARY LTD

    Inventor： POPE NOEL C ,  KEMPIS EDWARD B ,  O'DONOVAN KEVIN H J

    IPC: B01J3/06 ,  B29C3/00

    CPC classification number: B01J3/065 ,  B30B11/004 ,  Y10S425/026

    Abstract: This invention relates to high-pressure dies normally used for use in the synthesis of diamonds. The die comprises a die ring having a through cavity within which there is formed a pressure chamber that is lined with a pyrophyllite sleeve. Respectively entering the ends of the sleeve are two plungers. These plungers are capable of sliding in the sleeve until near the end of their compressive strokes so that little or no axial pressure is applied to the ends of the sleeve.

    Abstract translation: 本发明涉及通常用于合成钻石的高压模具。 模具包括具有通孔的模具环，在该模腔中形成有与叶蜡石套筒相衬的压力室。 分别进入套筒的端部是两个柱塞。 这些柱塞能够在套筒中滑动直到接近其压缩冲程的结束，使得很少或没有轴向压力施加到套筒的端部。

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