Abstract:
A method allows analyzing and describing the reflective properties of a three-dimensionally structured original surface. The topology of the original surface is determined and the topological data are stored in the form of a depth map in a first data record and evaluated with respect to the influence of the data on the reflective properties. Each surface element is assigned a reflective value in accordance with the evaluation and the value is stored in a second data record and made available to other machining or inspection systems. There, the reflection values of the second data record are divided into classes and the depth values of the first data record, assigned to the classified reflection values, are varied in accordance with the classification. Finally, the changed depth values are employed as parameters for electronically controlling a tool in order to machine the artificially produced surface.
Abstract:
The invention relates to a method of distributing a fluid. According to the invention, the following elements are connected simultaneously to a valve (1) which comprises multiple inlets and outlets and which is equipped with a check valve, namely: a fluid sampling and injecting device, such as a syringe (2); a gas (e.g. air) supply conduit; a supply conduit for the liquid to be distributed; and a discharge conduit (6). The inventive method consists in: drawing in the liquid to be distributed in order to transfer same to the sampling and injecting device (2), injecting the liquid into the discharge conduit (6), drawing in the gas in order to transfer same to the sampling and injecting device (2), and injecting the gas into the discharge conduit (6) in order to push the remaining liquid into the discharge conduit (6). The invention also relates to a device and kit for implementing said method.
Abstract:
A Josephson junction is disclosed which includes a substrate of a single crystal having a substantially flat surface, a wiring pattern of an oxide superconductor formed on the flat surface of the substrate, and an altered region formed having a width of 300 nm or less and formed in the wiring pattern to intersect the wiring pattern, the crystal orientations of the wiring pattern on both sides of the altered region being equal to each other. The Josephson junction may be prepared by a process including the steps of: (a) coating a surface of a substrate of a single crystal with a normal metal to form a protecting layer over the surface of the substrate; (b) irradiating a predetermined portion of the protecting layer with a focused ion beam so that an irradiated portion is formed in the substrate; (c) removing the protecting layer from the substrate; and (d) forming a wiring pattern of an oxide superconductor on the surface of the substrate from which the protecting layer has been removed such that the wiring pattern crosses the irradiated portion of the substrate, thereby forming an altered portion in the wiring pattern at a position above the irradiated portion.
Abstract:
Inexpensive product consisting of porous carbon, with a pore structure which is suitable for retaining electrode parts which can be used in particular for a use as an electrode material for a lithium-sulphur secondary battery, and a method comprising the following method steps: (a) providing a template consisting of inorganic material which contains spherical nanoparticles and pores, (b) infiltrating the pores of the template with a precursor for carbon of a first variety, (c) carbonizing so as to form an inner layer on the nanoparticles with a first microporosity, (d) infiltrating the remaining pores of the template with a precursor substance for carbon of a second variety, (e) carbonizing the precursor substance, wherein an outer layer with a second microporosity which is lower than the first microporosity is produced on the inner layer, and (f) removing the template so as to form the carbon product with layer composite structure, comprising an inner layer consisting carbon with a first, relatively high microporosity, which has a free surface facing a cavity, and an outer layer consisting of carbon with a second, relatively low microporosity, which has a free surface facing away from the cavity.
Abstract:
For use as electrode material for a lithium battery, porous templates are impregnated with a carbon feedstock that can be graphitized. This frequently results in only a low thickness of the deposited, graphite-like layer, such that generally several such infiltration and carbonation processes must be carried out consecutively. In order to provide a cost-effective product which is made of porous carbon and has high porosity and a low surface, according to the invention a method comprises the following method steps: (a) preparing a porous carbon structure having a large specific surface, (b) infiltrating the carbon structure with a precursor substance for carbon that can be graphitized, (c) carbonizing the precursor substance to form the carbon product having a low specific surface, wherein preparing the carbon structure according to method step (a) comprises the following: (I) preparing a template containing pores, (II) infiltrating the pores of the template with a solution that contains a precursor of carbon that cannot be graphitized, (III) carbonizing the precursor forming the carbon structure having the first specific surface, and (IV) removing the template.
Abstract:
A known method for producing a porous carbon body comprises providing a template of inorganic template material which comprises interconnected pores, providing a precursor substance for carbon, infiltrating the pores of the template with the precursor substance, carbonizing the precursor substance and removing the template with formation of the porous carbon product. Starting therefrom, to provide a method which allows a cost-effective production of a porous carbon structure also with thick wall thicknesses, it is suggested according to the invention that precursor substance particles of fusible material and template particles are provided and a powder mixture is formed from the particles, and that the powder mixture is heated before or during carbonization according to method step (d) in such a manner that precursor substance melt penetrates into the pores of the template particles.
Abstract:
Build-up granulation and compaction granulation methods are generally known for producing granules from porous inorganic material. In order to allow a cost-efficient yet also reproducible production of porous granules having a more pronounced hierarchical pore structure, the invention relates to a method comprising the following steps: (a) supplying a feedstock flow to a reaction zone in which the feedstock is converted to material particles by means of pyrolysis or hydrolysis, (b) depositing the material particles on a deposition surface (1a) forming a soot layer (5), (c) thermally hardening the soot layer (5) to form a porous soot plate (5a), and (d) comminuting the soot plate (5a) to form porous granules (13).
Abstract:
In order to provide an inexpensive product composed of a porous carbon provided with electrochemical active material, said product being suitable particularly for use as a cathode or anode material for a secondary battery, a process comprising the following process steps is proposed: (a) producing a template from inorganic material by gas phase deposition, said template comprising a framework of pores and nanoparticles joined to one another, (b) coating the template framework with an electrochemical active material or a precursor thereof, (c) infiltrating the pores of the template with a precursor substance for carbon, (d) carbonizing the precursor substance to form a carbon layer, (f) removing the template.
Abstract:
In a known process for drawing a quartz glass strand, SiO2 particles are fed to a melting crucible and softened therein to form a quartz glass mass, and the softened quartz glass mass is pulled vertically downward as a quartz glass strand via a drawing nozzle which is provided in the bottom region of the melting crucible and has a gap-like drawing nozzle opening. In order, on the basis thereof, to make it easier to reproducibly produce a quartz glass strand with a minor deviation from the nominal wall thickness profile, and in particular to avoid irregularly occurring indentations and protrusions of the wall thickness profile, it is proposed according to the invention that the wall thickness profile of the quartz glass strand is detected, and that the drawing nozzle is heated by means of a plurality of heating elements which are distributed around the drawing nozzle opening and can be electrically actuated independently of one another, and that the quartz glass mass is locally heated by means of the heating elements within the gap-like drawing nozzle opening depending on measurement results of the wall thickness profile.
Abstract:
A known method for producing a porous carbon product comprises producing a monolithic template from inorganic matrix material having pores connected to each other, infiltrating the pores of the template with carbon or a carbon precursor substance forming a green body framework containing carbon surrounded by matrix material and calcining the green body framework forming the porous carbon product. In order to provide a method proceeding herefrom which permits cost-effective production of a product from porous carbon, according to the invention the production of the template comprises a soot separation process in which a hydrolyzable or oxidable starting compound of the matrix material is supplied to a reaction zone, therein converted to matrix material particles by hydrolysis or pyrolysis, the matrix material particles are agglomerated or aggregated and formed to the template.